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1. 发明授权

US08147709B2 Compositions comprising 3,3,3-trifluoropropyne 有权
标题翻译：包含3,3,3-三氟丙炔的组合物
公开(公告)号：US08147709B2
公开(公告)日：2012-04-03
申请号：US12437014
申请日：2009-05-07
申请人： Barry Asher Mahler , Mario Joseph Nappa , Jeffrey P. Knapp
发明人： Barry Asher Mahler , Mario Joseph Nappa , Jeffrey P. Knapp
IPC分类号： C09K5/04
CPC分类号： C09K5/00 , B01J27/125 , B01J37/26 , C07C17/25 , C07C17/354 , C07C21/18 , C07C21/22 , C08J9/146 , C08J9/149 , C09K3/30 , C09K5/045 , C09K2205/12 , C09K2205/126 , C07C19/08
摘要： Disclosed are compositions comprising HFC-245eb and at least one additional compound selected from the group consisting of HFO-1234ze, HFC-245fa, HFC-236cb, HFC-236ea, HFC-236fa, HFC-227ea, HFC-227ca, HFO-1225yc, HFO-1225zc, HFO-1225ye, methane, ethane, propane, HFC-23, HFC-143a, HFC-134, HFC-134a, FC-1216, HFO-1234yf, HFC-254eb, HFO-1243zf, and HFC-254fb. Compositions comprising HFC-245eb are useful in processes to make HFO-1234yf. Also disclosed are compositions comprising HFO-1234yf and at least one additional compound selected from the group consisting of HFO-1234ze, HFC-254eb, HFC-254fb, HFO-1243zf, HFCHFC-245eb, HFC-245fa, HFC-245cb, HFC-236cb, HFC-236ea, HFC-236fa, HFC-227ea, HFC-227ca, HFO-1225yc, HFO-1225zc, HFO-1225ye, methane, ethane, propane, HFC-23, HFC-134, HFC-134a, HFO-1132a and FC-1216. Compositions comprising HFO-1234yf are useful as heat transfer compositions for use in refrigeration, air-conditioning and heat pump systems.
摘要翻译：公开了包含HFC-245eb和至少一种选自HFO-1234ze，HFC-245fa，HFC-236cb，HFC-236ea，HFC-236fa，HFC-227ea，HFC-227ca，HFO-1225yc ，HFO-1225zc，HFO-1225ye，甲烷，乙烷，丙烷，HFC-23，HFC-143a，HFC-134，HFC-134a，FC-1216，HFO-1234yf，HFC-254eb，HFO-1243zf和HFC- 254fb。包含HFC-245eb的组合物可用于制备HFO-1234yf的方法。还公开了包含HFO-1234yf和至少一种选自HFO-1234ze，HFC-254eb，HFC-254fb，HFO-1243zf，HFCHFC-245eb，HFC-245fa，HFC-245cb，HFC- 236cb，HFC-236ea，HFC-236fa，HFC-227ea，HFC-227ca，HFO-1225yc，HFO-1225zc，HFO-1225ye，甲烷，乙烷，丙烷，HFC-23，HFC-134，HFC-134a， 1132a和FC-1216。包含HFO-1234yf的组合物可用作用于制冷，空调和热泵系统的热转印组合物。

2. 发明申请

US20080051612A1 PROCESSES FOR SEPARATION OF FLUOROOLEFINS FROM HYDROGEN FLUORIDE BY AZEOTROPIC DISTILLATION 有权
标题翻译：通过AZOOTROPIC蒸馏从氟化氢中分离氟化物的方法
公开(公告)号：US20080051612A1
公开(公告)日：2008-02-28
申请号：US11844403
申请日：2007-08-24
申请人： JEFFREY P. KNAPP , BARRY ASHER MAHLER , DONALD J. TOTON
发明人： JEFFREY P. KNAPP , BARRY ASHER MAHLER , DONALD J. TOTON
IPC分类号： C07C17/383
CPC分类号： C07C17/38 , C01B7/196 , C07C17/25 , C07C17/383 , C07C17/386 , C07C21/18 , C07C21/185 , C07C19/08
摘要： The present disclosure relates to a process for separating a fluoroolefin from a mixture comprising hydrogen fluoride and fluoroolefin, comprising azeotropic distillation both with and without an entrainer. In particular are disclosed processes for separating any of HFC-1225ye, HFC-1234ze, HFC-1234yf or HFC-1243zf from HF.
摘要翻译：本公开涉及一种从包含氟化氢和氟代烯烃的混合物中分离氟烯烃的方法，包括具有和不具有夹带剂的共沸蒸馏。特别公开了从HF分离HFC-1225ye，HFC-1234ze，HFC-1234yf或HFC-1243zf中的任何一种的方法。

3. 发明授权

US06458249B2 Process for purifying perfluorinated products 失效
标题翻译：净化全氟化产物的方法
公开(公告)号：US06458249B2
公开(公告)日：2002-10-01
申请号：US09189322
申请日：1998-11-09
申请人： Ralph Newton Miller , Chien-Ping Chai Kao , Barry Asher Mahler
发明人： Ralph Newton Miller , Chien-Ping Chai Kao , Barry Asher Mahler
IPC分类号： B01D334
CPC分类号： C07C19/08 , B01D3/36 , C01B21/083 , C01B21/0835 , C01B21/0837 , C01P2006/80 , C07C17/38
摘要： Nitrogen trifluoride (NF3) containing less than 10 parts-per-million molar impurities, e.g., tetrafluoromethane (PFC-14), is disclosed. Azeotropic and extractive distillation processes using entraining agents for separating NF3 and PFC-14 from each other and from mixtures with other electronics industry materials are disclosed.
摘要翻译：公开了含有少于10ppm摩尔杂质的三氟化氮（NF 3），例如四氟甲烷（PFC-14）。公开了使用夹带剂将NF 3和PFC-14彼此分离的混合物和与其它电子工业材料的混合物的共沸和萃取蒸馏方法。

4. 发明授权

US06221830B1 Purification process for hexafluoroethane products 失效
标题翻译：六氟乙烷产品净化过程
公开(公告)号：US06221830B1
公开(公告)日：2001-04-24
申请号：US08842843
申请日：1997-04-17
申请人： Ralph Newton Miller , Mark Richard Deschere , Barry Asher Mahler , Olagappan Muthu
发明人： Ralph Newton Miller , Mark Richard Deschere , Barry Asher Mahler , Olagappan Muthu
IPC分类号： B01D334
CPC分类号： C07C19/08 , C01B7/0712 , C01B7/196 , C07C17/38 , C07C17/386 , Y02P20/582
摘要： The disclosure relates to removing impurities from hexafluoroethane (CF3CF3), also known as Perfluorocarbon 116 (PFC-116) or Fluorocarbon 116 (FC-116), by using azeotropic distillation such that an overhead product consisting essentially of HCl-hexafluoroethane is formed, optionally combined with a phase separation step to break the HCl-hexafluoroethane azeotropic or azeotrope-like composition thereby permitting recovery of substantially pure hexafluoroethane. Unreacted hydrogen fluoride (HF) may be removed from hexafluoroethane during the above azeotropic distillation with HCl or alternatively by an azeotropic distillation wherein an HF-hexafluoroethane azeotropic or azeotrope-like composition exits overhead and substantially pure HF exits in the bottoms stream.
摘要翻译：本公开涉及通过共沸蒸馏从六氟乙烷（CF 3 CF 3）（也称为全氟化碳116（PFC-116）或氟碳116（FC-116））除去杂质，从而形成基本上由HCl-六氟乙烷组成的塔顶馏出物结合相分离步骤以破坏HCl-六氟乙烷共沸或类共沸组合物从而允许回收基本上纯的六氟乙烷。在HCl的上述共沸蒸馏过程中，可以从六氟乙烷中除去未反应的氟化氢（HF），或者通过共沸蒸馏除去六氟乙烷，其中HF-六氟乙烷共沸或类共沸组合物离开塔顶馏出物，基本上纯的HF在塔底物流中离开。

5. 发明授权

US5874657A Process for the purification of 1,1-difluoroethane 失效
标题翻译： 1,1-二氟乙烷纯化方法
公开(公告)号：US5874657A
公开(公告)日：1999-02-23
申请号：US959869
申请日：1997-10-29
申请人： Ralph Newton Miller , Barry Asher Mahler
发明人： Ralph Newton Miller , Barry Asher Mahler
IPC分类号： C07C17/386 , C07C19/08 , C07C17/38
CPC分类号： C07C17/386
摘要： The present invention relates to processes for separating 1,1-difluoroethane (HFC-152a) from vinyl chloride by using extractive distillation with an extractive agent selected from the aliphatic hydrocarbons, chlorocarbons and alcohols.
摘要翻译：本发明涉及通过利用选自脂族烃，氯代烃和醇的萃取剂萃取蒸馏从氯乙烯中分离1,1-二氟乙烷（HFC-152a）的方法。

6. 发明申请

US20150225316A1 REACTOR FOR LIQUID PHASE FLUORINATION REACTIONS 有权
标题翻译：液相荧光反应器的反应器
公开(公告)号：US20150225316A1
公开(公告)日：2015-08-13
申请号：US14618500
申请日：2015-02-10
申请人： Daniel C. MERKEL , Barry Asher MAHLER , Hsueh Sung TUNG , Mario Joseph NAPPA
发明人： Daniel C. MERKEL , Barry Asher MAHLER , Hsueh Sung TUNG , Mario Joseph NAPPA
IPC分类号： C07C17/087 , C07C17/25
CPC分类号： C07C17/087 , B01J19/18 , B01J19/1868 , C07C17/20 , C07C17/206 , C07C17/25 , C07C19/10
摘要： The present invention relates to a hydrofluorinating process which comprises reacting a fluoroolefin with hydrogen fluoride in the liquid phase in the presence of a hydrofluorination catalyst in the reaction zone of a reactor, said reactor comprised of a reactor body having a length to diameter ratio of about 2:1 or greater; a stirred reaction zone containing said hydrofluorination catalyst, which may be prepared in situ, at least one inlet for supplying said hydrogen fluoride and fluoroolefin to the reaction zone and at least one outlet for recovering said fluoroalkane, said stirrer disposed in the reaction zone and comprising a plurality of blades fixedly attached to shaft drivable by a motor, said blades extending from about the bottom of the reaction zone to about the top of the reaction zone and said shaft extending on a longitudinal axis from the bottom of the reactor to the top of the reactor, said stirrer being rotated at a speed sufficient to promote a swirling of the liquid to effect the occurrence of hydrofluorination reaction and minimize overfluorination. The present invention also relates to said hydrofluorination reactor.
摘要翻译：本发明涉及一种氢氟化方法，其包括在反应器的反应区中在氟化氢催化剂存在下，在液相中使氟烯烃与氟化氢反应，所述反应器包括长径比为约 2：1或更大; 包含可以原位制备的所述氢氟化催化剂的搅拌反应区，至少一个用于将所述氟化氢和氟代烯烃供应到反应区的入口和用于回收所述氟烷烃的至少一个出口，所述搅拌器设置在反应区中并且包含多个叶片固定地附接到由马达驱动的轴上，所述叶片从反应区域的底部延伸到反应区域的顶部，并且所述轴线在纵向轴线上从反应器底部延伸到顶部反应器，所述搅拌器以足以促进液体旋转的速度旋转以实现氢氟化反应的发生并使过度氟化最小化。本发明还涉及所述氢氟化反应器。

7. 发明申请

US20100012900A1 NON-IGNITABLE GASEOUS COMPOSITION COMPRISING DIFLUOROMETHANE AND TETRAFLUOROETHYLENE 有权
标题翻译：包含二氟甲磺酸和四氟乙烯的非点燃气体组合物
公开(公告)号：US20100012900A1
公开(公告)日：2010-01-21
申请号：US12439565
申请日：2007-09-04
申请人： Barry Asher Mahler
发明人： Barry Asher Mahler
IPC分类号： C09K3/00
CPC分类号： C07C19/08 , C07C17/42 , C07C21/185
摘要： The present disclosure relates to non-ignitable gaseous compositions comprising difluoromethane and tetrafluoroethylene. When the pressure is at least 150 psig, the molar percentage of tetrafluoroethylene in the non-ignitable gaseous composition is no more than 111.6−0.124X. When the pressure is less than 150 psig, the molar percentage of tetrafluoroethylene in the non-ignitable gaseous composition is no more than 102−0.06X. X is the pressure in the unit of psig.The present disclosure also provides processes for making such non-ignitable gaseous compositions.Also disclosed are azeotropic compositions of TFE and HFC-32.
摘要翻译：本发明涉及包含二氟甲烷和四氟乙烯的不可燃气体组合物。当压力至少为150psig时，不燃点气体组合物中四氟乙烯的摩尔百分数不超过111.6-0.124X。当压力小于150psig时，不燃性气体组合物中四氟乙烯的摩尔百分比不大于102-0.06X。 X是以psig为单位的压力。本公开还提供了制备这种不可燃气体组合物的方法。还公开了TFE和HFC-32的共沸组合物。

8. 发明授权

US06303838B1 Separating 1,1,1,3,3-pentafluoropropane from hydrogen fluoride 有权
标题翻译：从氟化氢分离1,1,1,3,3-五氟丙烷
公开(公告)号：US06303838B1
公开(公告)日：2001-10-16
申请号：US09509859
申请日：2000-03-31
申请人： Sara W. Boehmer , Barry Asher Mahler , Ralph Newton Miller
发明人： Sara W. Boehmer , Barry Asher Mahler , Ralph Newton Miller
IPC分类号： C07C1738
CPC分类号： C07C17/38 , C07C19/08
摘要： Disclosed are processes for separating 1,1,1,3,3-pentafluoropropane (HFC-245fa) from hydrogen fluoride (HF) by distillation, wherein hydrocarbons, chloroflurocarbons, hydrochlorofluorocarbons and fluorocarbons are used as entraining agents. The processes comprise: contacting a first mixture comprising HFC-245fa and HF with an entraining agent selected from the group consisting of hydrocarbons, chlorofluorocarbons, hydrochlorofluorocarbons and fluorocarbons to form a second mixture, distilling the second mixture and thereby separating the HFC-245fa from HF and entraining agent, and recovering HFC-245fa substantially-free of HF.
摘要翻译：公开了通过蒸馏从氟化氢（HF）分离1,1,1,3,3-五氟丙烷（HFC-245fa）的方法，其中使用烃，氯氟烃，氢氯氟烃和碳氟化合物作为夹带剂。该方法包括：使包含HFC-245fa和HF的第一混合物与选自碳氢化合物，氯氟烃，氢氯氟烃和碳氟化合物的夹带剂接触以形成第二混合物，蒸馏第二混合物，从而将HFC-245fa与HF分离和夹带剂，并回收基本上不含HF的HFC-245fa。

9. 发明授权

US5830325A Separating and removing 1, 1, 1-trifluoroethane by using azeotropic distillation 失效
标题翻译：通过共沸蒸馏分离和除去1,1,1-三氟乙烷
公开(公告)号：US5830325A
公开(公告)日：1998-11-03
申请号：US625579
申请日：1996-03-28
申请人： Barry Asher Mahler , Ralph Newton Miller
发明人： Barry Asher Mahler , Ralph Newton Miller
IPC分类号： C07C17/386 , C07C19/08 , C07C19/10 , B01D3/36
CPC分类号： C07C19/10 , C07C17/386 , C07C19/08
摘要： The disclosure relates to separating 1,1,1-trifluoroethane (HFC-143a from fluorocarbon impurities by using extractive distillation with an extractive agent comprising an alcohol. Examples of suitable extractive agents comprise at least one member from the group of methanol, butanol, ethanol, propanol, their isomers and cyclic compounds thereof, among others.
摘要翻译：本公开内容涉及通过采用萃取剂将醇（HFC-143a）从氟碳杂质中分离出来，所述萃取剂包括醇。合适的萃取剂的实例包括至少一种甲醇，丁醇，乙醇，丙醇，它们的异构体和环状化合物等。

10. 发明授权

US5772852A Separating HCI and halocarbons 失效
标题翻译：分离HCI和卤代烃
公开(公告)号：US5772852A
公开(公告)日：1998-06-30
申请号：US499101
申请日：1995-07-06
申请人： Barry Asher Mahler , Vinci Martinez Felix , Ralph Newton Miller
发明人： Barry Asher Mahler , Vinci Martinez Felix , Ralph Newton Miller
IPC分类号： B01D3/36 , C01B7/01 , C01B7/07 , C07C17/38 , C07C19/08 , C07C19/10 , C07C19/12
CPC分类号： C01B7/0712 , C07C17/38 , C07C19/08 , C07C19/10 , C07C19/12
摘要： A process for separating HCl from pentafluoroethane, chloropentafluoroethane, chlorotrifluoroethane, trifluoromethane, and other fully saturated and unsaturated fluorocarbons, chlorofluorocarbons and chlorocarbons.
摘要翻译：从五氟乙烷，氯五氟乙烷，三氟氯乙烷，三氟甲烷和其他完全饱和和不饱和碳氟化合物，氯氟烃和氯代烃分离HCl的方法。

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