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71. 发明申请

US20110092699A1 PROCESS FOR PRODUCING AMIDE OR LACTAM 有权
标题翻译：生产酰胺或乳酸菌的方法
公开(公告)号：US20110092699A1
公开(公告)日：2011-04-21
申请号：US12997287
申请日：2009-06-10
申请人： Takahiro Iwahama , Tatsuya Nakano
发明人： Takahiro Iwahama , Tatsuya Nakano
IPC分类号： C07D201/04
CPC分类号： C07D201/04 , C07D223/10 , Y02P20/52
摘要： A process produces an amide or lactam by subjecting an oxime compound to rearrangement in a solvent in the presence of: at least one catalyst selected from the group consisting of an aromatic compound (A1) containing a leaving group bound to a carbon atom constituting the aromatic ring, the aromatic ring including, as a constitutive atom thereof, a heteroatom or including, as a constitutive atom thereof, a carbon atom bound to an electron-withdrawing group, and a compound (A2) containing a structure of Formula (1): -G-LA (1) wherein G represents P, N, S, B or Si atom; and LA represents a leaving group, wherein G is bound to one or more atoms or groups in addition to LA; and a co-catalyst including a halogen-containing organic acid, to give the corresponding amide or lactam, wherein, when the aromatic compound (A1) alone is used as the catalyst, the solvent is at least one solvent selected typically from hydrocarbon solvents. The production process can yield amides or lactams simply in high yields without causing large amounts of by-products such as ammonium sulfate.
摘要翻译：一种方法是通过使肟化合物在溶剂中进行重排来生成酰胺或内酰胺：在至少一种选自包含与构成芳香族的碳原子结合的离去基团的芳族化合物（A1）的催化剂的存在下，芳环包括作为其组成原子的杂原子或其包含作为其组成原子的与吸电子基团结合的碳原子，和包含式（1）结构的化合物（A2）： -G-LA（1）其中G表示P，N，S，B或Si原子; 并且LA表示离去基团，其中除了LA之外，G与一个或多个原子或基团结合; 和包含含卤素的有机酸的助催化剂，得到相应的酰胺或内酰胺，其中当单独使用芳族化合物（A1）作为催化剂时，溶剂是通常选自烃溶剂的至少一种溶剂。生产过程可以简单地以高产率产生酰胺或内酰胺，而不会引起大量副产物如硫酸铵。

72. 发明授权

US07615656B2 Cycloaliphatic polyepoxy compounds and preparation thereof 失效
标题翻译：环脂族聚环氧化合物及其制备
公开(公告)号：US07615656B2
公开(公告)日：2009-11-10
申请号：US11819615
申请日：2007-06-28
申请人： Takashi Kubo , Tatsuya Nakano , Takahiro Iwahama
发明人： Takashi Kubo , Tatsuya Nakano , Takahiro Iwahama
IPC分类号： C07D303/06
CPC分类号： C08G59/24 , C07D303/16 , C07D303/40
摘要： Is disclosed a cycloaliphatic polyepoxy compound represented by following Formula (1): wherein Y represents a linkage group or a single bond; and HAs each represent hydrogen atom at the junction between cyclohexane ring and oxirane ring, and the cyclohexane rings may each further have one or more substituents in addition to the groups shown in the formula. The cycloaliphatic polyepoxy compound contains stereoisomers in such proportions as to have a ratio A/B of 1.8 or more, wherein “A” and “B” are integrated intensities of signals of protons at the junction between cyclohexane ring and oxirane ring as determined by 1H-NMR spectroscopy of the compound, in which “A” represents the integrated intensity of a signal observed at a lower magnetic field, and “B” represents the integrated intensity of a signal observed at a higher magnetic field.
摘要翻译：公开了由下式（1）表示的脂环族聚环氧化合物：其中Y表示连接基团或单键; 并且HAs各自表示环己烷环和环氧乙烷环之间的连接处的氢原子，除了式中所示的基团之外，环己烷环还可以具有一个或多个取代基。脂环族聚环氧化合物含有比例A / B为1.8以上的立体异构体，其中“A”和“B”是环己烷环与环氧乙烷环之间的连接处质子信号的积分强度，由1H 化合物的-NMR光谱，其中“A”表示在较低磁场下观察到的信号的积分强度，“B”表示在较高磁场下观察到的信号的积分强度。

73. 发明授权

US07476706B2 Method for producing polyorganosiloxane particles and for producing silica particles 有权
标题翻译：聚有机硅氧烷粒子的制造方法和二氧化硅粒子的制造方法
公开(公告)号：US07476706B2
公开(公告)日：2009-01-13
申请号：US10538755
申请日：2004-02-24
申请人： Taro Suzuki , Junji Kawashima , Tatsuya Nakano
发明人： Taro Suzuki , Junji Kawashima , Tatsuya Nakano
IPC分类号： C08G77/06 , C08L83/12
CPC分类号： C08G77/14 , C01B33/18 , C01P2004/51 , C01P2004/53 , C01P2004/61 , C08G77/20 , G02F1/13392
摘要： The present invention provides a method for producing polyorganosiloxane particles through the step of hydrolyzing and condensing a silicon compound having a non-hydrolyzable group and a hydrolyzable alkoxyl group bonded to its silicon atom in the presence of a catalyst and thereby forming seed particles of polyorganosiloxane particles to obtain a seed-particles-containing solution and the step of adding a particle-diameter-growing aqueous solution containing the same silicon compound or a hydrolyzate thereof to the above seed-particles-containing solution to grow the above seed particles, the method comprising the step of obtaining the seed-particles-containing solution, in which particles are measured for a particle diameter continuously or at intervals of a constant time period and terminating the reaction at a time when an intended particle diameter is reached.
摘要翻译：本发明提供一种通过在催化剂存在下水解和缩合具有不可水解基团的硅化合物和与其硅原子键合的可水解烷氧基并从而形成聚有机硅氧烷颗粒的种子颗粒的步骤来生产聚有机硅氧烷颗粒的方法得到含有种子颗粒的溶液和将含有相同硅化合物或其水解产物的粒径生长水溶液加入到上述种子颗粒溶液中以生长上述种子颗粒的步骤，该方法包括获得含有种子颗粒的溶液的步骤，其中连续地或以恒定时间段的间隔测量颗粒，并在达到预期的粒径的时候终止反应。

74. 发明申请

US20080234455A1 Vinyl ether compounds and polymerizable compositions 失效
标题翻译：乙烯基醚化合物和可聚合组合物
公开(公告)号：US20080234455A1
公开(公告)日：2008-09-25
申请号：US12076625
申请日：2008-03-20
申请人： Takahiro Iwahama , Tatsuya Nakano , Keizo Inoue , Hiroto Miyake , Tsukasa Yoshida , Mitsuru Ohno , Yoshinori Funaki
发明人： Takahiro Iwahama , Tatsuya Nakano , Keizo Inoue , Hiroto Miyake , Tsukasa Yoshida , Mitsuru Ohno , Yoshinori Funaki
IPC分类号： C08F24/00 , C07D303/02 , C07D305/00
CPC分类号： C07D303/22 , C07D305/06 , C08F24/00
摘要： Disclosed is an oxetane-containing vinyl ether compound including one or more aromatic or non-aromatic carbocycles and/or two or more vinyl ether structures, such as a compound of Formula: wherein Ring Z1 is non-aromatic carbocycle; Ra is vinyl group of Formula: wherein each of R1, R2, and R3 is hydrogen or C1-C4 alkyl; Wa is single bond or organic group having a valence of (m+1); X1 is, for example, hydrocarbon; “m” and “q” are each 1 or 2; and “p” is 0 to 5. Also disclosed is an alicyclic epoxy-containing vinyl ether compound of Formula: wherein Ring Z2 is non-aromatic carbocycle; Rb is vinyl group of Formula: wherein R4, R5 and R6 are each hydrogen or C1-C4 alkyl; Wb is single bond or organic group having a valence of (r+1); Rc and Rd are hydrogen or alkyl; and “r” and “s” are 1 or 2.
摘要翻译：公开了包含一种或多种芳族或非芳族碳环和/或两个或多个乙烯基醚结构的含氧杂环丁烷的乙烯基醚化合物，例如下式的化合物：其中环Z 1是非 - 芳香碳环 R a是乙烯基，其中R 1，R 2和R 3各自为氢或C 1 -C 4烷基; 化合物是单键或化合价（m + 1）的有机基团。 X 1是例如烃; “m”和“q”分别为1或2; 并且“p”为0至5.还公开了下式的脂环族环氧基乙烯基醚化合物：其中Z 2是非芳族碳环; R b是下式的乙烯基：其中R 4，R 5和R 6各自是氢或C 1 -C 1-4烷基; W是单键或化合价（r + 1）的有机基团。 R d和R d是氢或烷基; “r”和“s”为1或2。

75. 发明授权

US07368615B2 Catalyst comprising a cyclic imide compound and process for producing organic compounds using the catalyst 有权
标题翻译：包含环状酰亚胺化合物的催化剂和使用该催化剂生产有机化合物的方法
公开(公告)号：US07368615B2
公开(公告)日：2008-05-06
申请号：US11242779
申请日：2005-10-05
申请人： Yasutaka Ishii , Tatsuya Nakano , Shinya Nagano , Naoto Okuyama
发明人： Yasutaka Ishii , Tatsuya Nakano , Shinya Nagano , Naoto Okuyama
IPC分类号： C07C13/00
CPC分类号： C07C51/313 , B01J31/006 , B01J31/0209 , B01J31/0247 , B01J31/0271 , B01J31/2208 , B01J2231/70 , B01J2531/845 , C07C29/50 , C07C45/33 , C07C45/39 , C07C51/265 , C07C201/02 , C07C201/08 , C07C2601/14 , C07D209/48 , C07C49/403 , C07C49/04 , C07C63/06 , C07C55/12 , C07C55/14 , C07C203/08 , C07C205/05 , C07C31/125 , C07C35/08
摘要： A catalyst includes a cyclic imide compound having an N-substituted cyclic imide skeleton represented by following Formula (I): wherein X is an oxygen atom or a hydroxyl group, and having a solubility parameter of less than or equal to 26 [(MPa)1/2] as determined by Fedors method. The catalyst may further comprise a metallic compound. By allowing (A) a compound capable of forming a radical to react with (B) a radical scavenging compound in the presence of the catalyst, an addition or substitution reaction product between the compound (A) and the compound (B) or a derivative thereof can be obtained.
摘要翻译：催化剂包括具有由下式（I）表示的N-取代的环状酰亚胺骨架的环状酰亚胺化合物：其中X是氧原子或羟基，溶解度参数小于或等于26 [（MPa）通过Fedors方法测定的^{1/2。催化剂还可以包含金属化合物。通过使（A）能够形成自由基的化合物与（B）自由基清除化合物在催化剂存在下反应的化合物（A）和化合物（B）之间的加成或取代反应产物或衍生物可以得到。}

76. 发明授权

US07038064B2 Process for producing hydroxylactones 失效
标题翻译：制备羟基内酯的方法
公开(公告)号：US07038064B2
公开(公告)日：2006-05-02
申请号：US10332049
申请日：2001-07-18
申请人： Yasutaka Ishii , Tatsuya Nakano , Keizo Inoue
发明人： Yasutaka Ishii , Tatsuya Nakano , Keizo Inoue
IPC分类号： C07D307/32 , C07D309/30
CPC分类号： C07D307/935 , C07D307/32 , C07D309/30
摘要： A process of the present invention produces a hydroxylactone by subjecting an unsaturated carboxylic acid having a double bond not conjugated to a carboxyl group or an ester thereof to (i) a reaction with hydrogen peroxide in the presence of a metallic compound containing a metallic element selected from W, Mo, V and Mn or (ii) a reaction with a peroxide containing the metallic element to thereby yield a corresponding hydroxylactone having a hydroxyl group combined with one of carbon atoms constituting the double bond and being cyclized at the other carbon atom position. The metallic compound may be one selected from oxides, oxoacids and salts thereof. The unsaturated carboxylic acid includes, for example, β,γ-unsaturated carboxylic acids, γ,δ-unsaturated carboxylic acids, and δ,ε-unsaturated carboxylic acids. The process can produce hydroxylactones in high yields at low cost.
摘要翻译：本发明的方法通过使具有未与羧基键合的双键的不饱和羧酸或其酯与（ⅰ）在含有选自金属元素的金属化合物存在下与过氧化氢反应来制备羟基内酯由W，Mo，V和Mn反应，或者（ii）与含有金属元素的过氧化物反应，得到具有与构成双键的碳原子结合的羟基的相应羟基内酯，并在另一个碳原子位置环化。金属化合物可以是选自氧化物，含氧酸及其盐中的一种。不饱和羧酸包括例如β，γ-不饱和羧酸，γ，δ-不饱和羧酸和δ-不饱和羧酸。该方法可以以低成本高产率生产羟基内酯。

77. 发明授权

US07034184B2 Process for producing azine compounds and oxime compounds 失效
标题翻译：制备吖嗪化合物和肟化合物的方法
公开(公告)号：US07034184B2
公开(公告)日：2006-04-25
申请号：US10379604
申请日：2003-03-06
申请人： Yasutaka Ishii , Tatsuya Nakano
发明人： Yasutaka Ishii , Tatsuya Nakano
IPC分类号： C07C241/02 , C07C241/04 , C07C249/04
CPC分类号： C07C249/16 , C07C249/04 , C07C2601/14 , Y02P20/55 , C07C251/42 , C07C251/88
摘要： A process comprising allowing a peroxide compound represented by following Formula (2): wherein Ra, Rb, Rc and Rd are the same or different and are each a hydrogen atom or a hydrocarbon group, and wherein Ra and Rb, Rc and Rd may be combined to form a ring together with the adjacent carbon atom, respectively, to react with ammonia and water to yield an azine compound represented by following Formula (3): wherein Ra, Rb, Rc and Rd have the same meanings as defined above, or oxime compounds represented by following Formulae (4a) and/or (4b): wherein Ra, Rb, Rc and Rd have the same meanings as defined above, in the presence of a nitrogen-containing cyclic compound constitutively having a skeleton represented by following Formula (A) in its ring: wherein X is one of an oxygen atom and an —OR group, and wherein R is one of a hydrogen atom and a hydroxyl-protecting group. This process can produce an oxime compound or an azine compound useful as a material for oxime compounds from low-cost materials by easy and simple procedures.
摘要翻译：一种方法，其包括使下述式（2）表示的过氧化物：其中R a，R b，R b，R c， d相同或不同，各自为氢原子或烃基，并且其中R a，R b，R b，R c，可以将组合物和R d分别与相邻的碳原子一起形成环，与氨和水反应，得到由下式（3）表示的吖嗪化合物：其中R < 其中R a，R b，R d和R d具有与上述相同的含义，或由下式表示的肟化合物：按照下式（4a）和/或（4b）：其中R a，R b，R c，R d和R d，在具有由下式（A）表示的骨架的含氮环状化合物的环中存在下述式中，X表示氧原子和-OR基中的一个，和其中R为o ne的氢原子和羟基保护基团。该方法可以通过简单和简单的方法产生用作低成本材料的肟化合物的肟化合物或吖嗪化合物。

78. 发明授权

US06998491B2 Catalyst comprising a cyclic imide compound 失效
标题翻译：包含环状酰亚胺化合物的催化剂
公开(公告)号：US06998491B2
公开(公告)日：2006-02-14
申请号：US10092554
申请日：2002-03-08
申请人： Yasutaka Ishii , Tatsuya Nakano , Shinya Nagano , Naoto Okuyama
发明人： Yasutaka Ishii , Tatsuya Nakano , Shinya Nagano , Naoto Okuyama
IPC分类号： C07D207/00 , B07J31/02
CPC分类号： C07C51/313 , B01J31/006 , B01J31/0209 , B01J31/0247 , B01J31/0271 , B01J31/2208 , B01J2231/70 , B01J2531/845 , C07C29/50 , C07C45/33 , C07C45/39 , C07C51/265 , C07C201/02 , C07C201/08 , C07C2601/14 , C07D209/48 , C07C49/403 , C07C49/04 , C07C63/06 , C07C55/12 , C07C55/14 , C07C203/08 , C07C205/05 , C07C31/125 , C07C35/08
摘要： A catalyst includes a cyclic imide compound having an N-substituted cyclic imide skeleton represented by following Formula (I): wherein X is an oxygen atom or a hydroxyl group, and having a solubility parameter of less than or equal to 26 [(MPa)1/2] as determined by Fedors method. The catalyst may further comprise a metallic compound. By allowing (A) a compound capable of forming a radical to react with (B) a radical scavenging compound in the presence of the catalyst, an addition or substitution reaction product between the compound (A) and the compound (B) or a derivative thereof can be obtained.
摘要翻译：催化剂包括具有由下式（I）表示的N-取代的环状酰亚胺骨架的环状酰亚胺化合物：<化学式id =“CHEM-US-00001”num =“000

79. 发明授权

US06576787B1 Hydroxymethyl-group-containing alicyclic compound and process for producing the same 失效
标题翻译：含有羟基甲基的脂环化合物及其制备方法
公开(公告)号：US06576787B1
公开(公告)日：2003-06-10
申请号：US09647880
申请日：2000-10-06
申请人： Tatsuya Nakano , Hiroshi Shimojitosyo
发明人： Tatsuya Nakano , Hiroshi Shimojitosyo
IPC分类号： C07C6952
CPC分类号： C07C69/72 , C07C31/137 , C07C35/37 , C07C35/40 , C07C43/315 , C07C45/45 , C07C45/71 , C07C49/323 , C07C49/345 , C07C49/35 , C07C69/013 , C07C69/54 , C07C2602/10 , C07C2603/24 , C07C2603/68 , Y02P20/55
摘要： Hydroxymethyl-group-containing alicyclic compounds that are useful for making photosensitive resins and other functional polymers. Processes for producing the hydroxymethyl-group-containing alicyclic compounds. Polymerizable alicyclic compounds. The alicyclic moieties in all of these compounds may be a polycyclic ring such as a perhydroindene ring, a decalin ring, a perhydrofluorene ring, a perhydroanthracene ring, a perhydrophenanthrene ring, a tricyclo[5.2.1.02.6]decane ring, a perhydroacenaphthene ring, or a perhydrophenalene ring.
摘要翻译：可用于制备光敏树脂和其它官能聚合物的含羟基甲基的脂环族化合物。制备含羟甲基的脂环族化合物的方法。可聚合脂环族化合物。所有这些化合物中的脂环部分可以是多环，例如全氢茚环，十氢化萘环，全氢芴环，全氢蒽环，全氢菲环，三环[5.2.1.02.6]癸烷环，全氢苊环，或全氢化苯环。

80. 发明授权

US06468487B1 Nitration or carboxylation catalysts 失效
标题翻译：硝化或羧化催化剂
公开(公告)号：US06468487B1
公开(公告)日：2002-10-22
申请号：US09142089
申请日：1999-02-19
申请人： Yasutaka Ishii , Tatsuya Nakano , Satoshi Sakaguchi
发明人： Yasutaka Ishii , Tatsuya Nakano , Satoshi Sakaguchi
IPC分类号： B01J800
CPC分类号： C07C45/36 , B01J31/006 , B01J31/0247 , B01J31/2208 , B01J2231/70 , B01J2531/16 , B01J2531/72 , B01J2531/842 , B01J2531/845 , C07B41/08 , C07B43/02 , C07C51/10 , C07C67/12 , C07C69/757 , C07C205/04 , C07C205/05 , C07C205/06 , C07C205/18 , C07C205/55 , C07C211/35 , C07C211/37 , C07C215/42 , C07C229/50 , C07C233/10 , C07C233/14 , C07C233/23 , C07C233/41 , C07C233/52 , C07C233/58 , C07C233/62 , C07C235/40 , C07C235/82 , C07C237/24 , C07C265/10 , C07C271/24 , C07C2603/74 , C07C49/78 , C07C61/29 , C07C61/135
摘要： In the presence of an imide compound (e.g., N-hydroxyphthalimide) shown by the following formula (1): wherein R1 and R2 represent a hydrogen atom, a halogen atom, an alkyl group, an aryl group and a cycloalkyl group, and R1 and R2 may bond together to form a double bond, or an aromatic or non-aromatic ring, and Y is an O or OH, and n denotes 1 to 3; a substrate is allowed to contact with at least one reactant selected from (i) a nitrogen oxide and (ii) a mixture of carbon monoxide and oxygen to be introduced with at least one functional group selected from a nitro group and a carboxyl group. The nitrogen oxide includes, for example, a compound represented by the formula NxOy (e.g., N2O3, NO2). The substrate includes, for example, a compound having a methine carbon atom (e.g., adamantane), a compound having a methyl group or a methylene group at an adjacent moiety of an aromatic ring. According to such reaction, the substrate can be efficiently nitrated or carboxylated even in a mild or moderate condition.
摘要翻译：在下式（1）所示的酰亚胺化合物（例如，N-羟基邻苯二甲酰亚胺）存在下，其中R 1和R 2表示氢原子，卤素原子，烷基，芳基和环烷基，R 1 并且R 2可以键合在一起形成双键，或芳族或非芳香族环，Y是O或OH，n表示1至3;使底物与至少一种选自（i ）氮氧化物和（ii）一氧化碳和氧气的混合物与至少一种选自硝基和羧基的官能团一起引入。氮氧化物包括例如由式N x O y表示的化合物（例如，N 2 O 3，NO 2）。底物包括例如具有次甲基碳原子的化合物（例如金刚烷），在芳环的相邻部分具有甲基或亚甲基的化合物。根据这种反应，即使在温和或中等条件下，底物也能被有效地硝化或羧化。

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