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71. 发明授权

US06977307B2 Water soluble or water dispersible fluorochemical silanes for rendering substrates oil and water repellent 失效
标题翻译：水溶性或水分散性含氟硅烷，用于使基质油和憎水剂
公开(公告)号：US06977307B2
公开(公告)日：2005-12-20
申请号：US10053001
申请日：2002-01-17
申请人： Rudolf J. Dams
发明人： Rudolf J. Dams
IPC分类号： C09K3/18 , B05D3/04 , B05D3/10 , B05D5/08 , C04B33/34 , C07F7/04 , C07F7/12 , C07F7/18 , C08F20/22 , C08F20/24 , C08F20/38 , C08F220/22 , C08F220/24 , C08F220/38 , C08G81/02
CPC分类号： C04B41/4933 , B05D5/083 , C03C17/30 , C04B41/009 , C04B41/84 , C07F7/1804 , C04B41/502 , C04B33/00
摘要： A water soluble or water dispersible fluorochemical silane represented by the general formula (I): X-MfnMhmMar-G wherein X represents the residue of an initiator or hydrogen; Mf represents units derived from one or more fluorinated monomer; Mh represents units derived from one or more non-fluorinated monomer; Ma represents units having a silyl group; G is a monovalent organic group comprising the residue of a chain transfer agent; n represents a value of 1 to 100; m represents a value of 0 to 100; and r represents a value of 0 to 100; and n+m+r is at least 2; with the proviso that at least one of the following conditions is fulfilled: (a) G contains a silyl group of the formula (III): wherein Y1, Y2 and Y3 each independently represents an alkyl group, an aryl group or a hydrolyzable group and at least one of Y1, Y2 and Y3 represents a hydrolyzable water solubilising group; or (b) r is at least 1 and at least one of Y4, Y5 and Y6 represents a hydrolyzable water solubilizing group.
摘要翻译：由通式（I）表示的水溶性或水分散性含氟硅烷：<？in-line-formula description =“In-line Formulas”end =“lead”？> XM _{n m m =“In-line Formulas”end =“tail”？>其中X表示引发剂或氢的残基; M代表来自一种或多种氟化单体的单元; M h H表示衍生自一种或多种非氟化单体的单元; M ^{a表示具有甲硅烷基的单元; G是包含链转移剂残基的一价有机基团; n表示1〜100的数值。 m表示0〜100的值。 r表示0〜100的值。 n + m + r为2以上; 条件是满足以下条件中的至少一个：（a）G包含式（III）的甲硅烷基：其中Y 1，Y 2和 Y 3各自独立地表示烷基，芳基或可水解基团，Y 1，Y 2和Y 2中的至少一个， SUP> 3 表示可水解水增溶基团; 或（b）r为至少1且Y 4，Y 5和Y 6以及Y 6中的至少一个表示可水解的水溶性基团。}}

72. 发明授权

US06525127B1 Alkylated fluorochemical oligomers and use thereof in the treatment of fibrous substrates 有权
标题翻译：烷基化氟化物低聚物及其在处理纤维基材中的用途
公开(公告)号：US06525127B1
公开(公告)日：2003-02-25
申请号：US09708372
申请日：2000-11-08
申请人： Chetan P. Jariwala , James D. Eggleston , Michael A. Yandrasits , Rudolf J. Dams
发明人： Chetan P. Jariwala , James D. Eggleston , Michael A. Yandrasits , Rudolf J. Dams
IPC分类号： C08K502
CPC分类号： C07C323/52 , C14C9/00 , D06M13/156 , D06M13/236 , D06M13/256 , D06M13/265 , D06M15/277 , D06M15/53 , D06M2200/11 , D06M2200/12
摘要： This invention provides a method of treating fibrous substrates, such as leather, by contacting the substrate with a fluorochemical compound comprising: a fluorochemical oligomeric portion comprising an aliphatic backbone with a plurality of pendant fluoroaliphatic groups, each fluoroaliphatic group having a fully fluorinated terminal group and each independently linked to a carbon atom of the aliphatic backbone through an organic linking group; an aliphatic moiety; and a linking group which links the fluorochemical oligomeric portion to the aliphatic moiety. The fluorochemical compounds provide desirable oil, water and stain repellency to fibrous substrates.
摘要翻译：本发明提供了一种处理纤维基材如皮革的方法，该方法是使基材与含氟化合物接触，该含氟化合物包含：含氟脂肪族主链与多个侧链氟代脂族基团的氟化合物低聚部分，每个氟脂族基团具有完全氟化的端基，各自独立地通过有机连接基团连接到脂族主链的碳原子上; 脂肪族部分; 以及将氟化物低聚部分连接到脂肪族部分的连接基团。含氟化合物对纤维基质提供了所需的油，水和防污性。

73. 发明授权

US06462228B1 Process for preparation of fluorinated sulfinates 失效
标题翻译：氟化亚硫酸盐的制备方法
公开(公告)号：US06462228B1
公开(公告)日：2002-10-08
申请号：US09582121
申请日：2000-09-25
申请人： Rudolf J. Dams
发明人： Rudolf J. Dams
IPC分类号： C07C20500
CPC分类号： C07C313/04 , C08F14/18 , C08F2/16
摘要： A process for preparation of a fluorinated sulfinate product by reacting a mixture comprising: (1) water; (2) dehalogenating and sulfinating reagent: and (3) fluoroaliphatic sulfonyl fluoride represented by the formula: Rf—[SO2F]n; and (4) at least one of the material selected from the group consisting of: (i) fluorinated surfactant, or (ii) organic cosolvent comprising, as the major component by weight of the organic solvent, alcohol having a boiling point of less than 110° C. at 760 torr; by heating the reaction mixture to a temperature between about 50° C. and 100° C. until the desired product yield is achieved. Also provided is a process of using the fluorinated sulfinate product as an initiation system for a free radical polymerization process, such as that used to prepare fluoropolymers.
摘要翻译：一种制备氟化亚磺酸盐产物的方法，该方法是使包含以下物质的混合物：（1）水; （2）脱卤和硫化试剂：和（3）由式Rf- [SO2F] n表示的氟代脂族磺酰氟; 和（4）选自以下的材料中的至少一种：（i）氟化表面活性剂或（ii）有机共溶剂，其包含作为主要组分的有机溶剂的重量，沸点小于 110℃，760托; 通过将反应混合物加热至约50℃至100℃的温度，直到达到所需的产物收率。还提供了使用氟化亚磺酸盐产物作为自由基聚合方法的引发体系的方法，例如用于制备含氟聚合物的方法。

74. 发明授权

US5852148A Perfluoroalkyl halides and derivatives 失效
公开(公告)号：US5852148A
公开(公告)日：1998-12-22
申请号：US794828
申请日：1997-02-04
申请人： Frederick E. Behr , Rudolf J. Dams , Johan E. DeWitte , Donald F. Hagen
发明人： Frederick E. Behr , Rudolf J. Dams , Johan E. DeWitte , Donald F. Hagen
IPC分类号： C07C17/00 , C07C17/25 , C07C51/285 , C08G18/08 , C08G18/09 , C08G18/28 , C08G18/80 , C08F18/20
CPC分类号： C08G18/8077 , C07C17/00 , C07C17/25 , C07C51/285 , C08G18/0866 , C08G18/095 , C08G18/2885 , Y10T428/31855
摘要： Novel mixtures of perfluoroalkyl halides and derivatives thereof are described. These mixtures contain some compounds with a straight perfluoroalkyl group and some with a branched perfluoroalkyl group. Methods of preparation and use are also described.

75. 发明授权

US5631306A Foamable composition containing unsaturated perfluorochemical blowing agent 失效
标题翻译：含不饱和全氟化合物发泡剂的可发泡组合物
公开(公告)号：US5631306A
公开(公告)日：1997-05-20
申请号：US511415
申请日：1995-08-04
申请人： Rudolf J. Dams , Richard M. Flynn , Koen Focquet , John G. Owens
发明人： Rudolf J. Dams , Richard M. Flynn , Koen Focquet , John G. Owens
IPC分类号： C08J9/14
CPC分类号： C08J9/148 , C08J9/143 , C08J9/149
摘要： Foamable compositions comprise (a) at least one normally liquid, unsaturated perfluorochemical blowing agent compound selected from the group consisting of perfluoroolefin compounds, e.g., perfluoro(4-methylpent-2-ene), perfluoroaromatic compounds, e.g., hexafluorobenzene, and perfluorocycloolefin compounds, e.g., perfluorocyclohexene, the perfluoroolefin compounds optionally containing one or more catenary heteroatoms; and (b) at least one foamable polymer or the precursors of at least one foamable polymer. The compositions are useful in preparing polymeric, e.g., polyurethane, foams.
摘要翻译：可发泡组合物包含（a）至少一种通常为液体的不饱和全氟化合物发泡剂化合物，其选自全氟烯烃化合物，例如全氟（4-甲基戊-2-烯），全氟芳族化合物如六氟苯和全氟环烃化合物，例如全氟环己烯，任选地含有一个或多个链状杂原子的全氟烯烃化合物; 和（b）至少一种可发泡聚合物或至少一种可发泡聚合物的前体。该组合物可用于制备聚合物，例如聚氨酯泡沫。

76. 发明授权

US5276175A Isocyanate derivatives comprising flourochemical oligomers 失效
标题翻译：包含荧光化学低聚物的异氰酸酯衍生物
公开(公告)号：US5276175A
公开(公告)日：1994-01-04
申请号：US679633
申请日：1991-04-02
申请人： Rudolf J. Dams , Johan E. De Witte
发明人： Rudolf J. Dams , Johan E. De Witte
IPC分类号： B01F17/52 , C08F8/30 , C08F14/18 , C08F214/18 , C08G18/62 , C08G18/73 , C08G18/77 , C09K3/18 , D06M13/398 , D06M13/432 , D06M15/277 , D06M15/576 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , D06M101/16 , D06M101/30 , D06M101/32 , D06M101/34 , D21H19/16 , C07C263/00
CPC分类号： D06M13/432 , C08G18/6279 , D06M13/398 , D06M15/576 , Y10T428/3154 , Y10T428/31942 , Y10T428/31949 , Y10T428/31964 , Y10T428/31971 , Y10T428/31993
摘要： Fluorochemical compositions comprising fluorinated compounds, wherein the fluorinated compound comprises fluorochemical oligomeric portion, an organic moiety, and a group that can impart soft hand, stain release, water repellency, or a durable property when the compound is applied to a fibrous substrate, wherein the fluorochemical oligomeric portion is bonded to the organic moiety through an isocyanate-derived linking group. Also disclosed are fluorochemical compositions in the form of fluorochemical liquid dispersions and methods for preparing substrates treated with such compositions. Substrates so treated exhibit particularly durable and abrasion-resistant oil and water repellent properties. Intermediates in the preparation of the fluorochemical compositions are also disclosed. Some of the intermediates are useful as emulsifiers in fluorochemical liquid dispersions.
摘要翻译：含氟化合物的氟化合物组合物，其中所述氟化化合物包含氟化合物低聚部分，有机部分，以及当将化合物施用于纤维质基材时可赋予柔软的手感，脱色性，防水性或耐久性的基团，其中含氟低聚部分通过异氰酸酯衍生的连接基团与有机部分结合。还公开了含氟化合物液体分散体形式的氟化合物组合物和用这些组合物处理的底物的方法。如此处理的基材表现出特别耐用和耐磨损的防水和防水性能。还公开了制备氟化合物组合物的中间体。一些中间体可用作含氟液体分散体中的乳化剂。

77. 发明授权

US09902836B2 Fluoropolyether elastomer compositions having low glass transition temperatures 有权
公开(公告)号：US09902836B2
公开(公告)日：2018-02-27
申请号：US14009929
申请日：2012-03-13
申请人： Steven G. Corveleyn , Miguel A. Guerra , Rudolf J. Dams , Tom Opstal
发明人： Steven G. Corveleyn , Miguel A. Guerra , Rudolf J. Dams , Tom Opstal
IPC分类号： C08K5/14 , C08K5/06 , C08G65/00 , C08L71/00
CPC分类号： C08K5/14 , C08G65/007 , C08G2650/48 , C08L71/00
摘要： A curable composition is provided. The curable composition has at least one functionalized fluoropolyether and at least one radical curing system. Further provided are fluoroelastomer compositions having a glass transition temperature of less than −40° C. and shaped articles comprising fluoroelastomers having glass transition temperatures of less than −40° C. obtained by curing the curable compositions. Also described are methods of making fluoroelastomer compositions having glass transition temperatures of less than −40° C.

78. 发明授权

US09701889B2 Methods for treating siliciclastic hydrocarbon-bearing formations with fluorinated amine oxides 有权
公开(公告)号：US09701889B2
公开(公告)日：2017-07-11
申请号：US13979747
申请日：2012-01-13
申请人： Rudolf J. Dams , Yong K. Wu , Steven J. Martin , Douglas E. Johnson
发明人： Rudolf J. Dams , Yong K. Wu , Steven J. Martin , Douglas E. Johnson
IPC分类号： E21B43/16 , C09K8/584 , C09K8/565 , C09K8/575 , C09K8/80 , C07C291/04 , C07C311/05
CPC分类号： C09K8/584 , C07C291/04 , C07C311/05 , C09K8/565 , C09K8/575 , C09K8/5751 , C09K8/80 , E21B43/16
摘要： A method of treating a siliciclastic, hydrocarbon-bearing formation includes contacting the hydrocarbon-bearing formation with a composition comprising solvent and a fluorinated amine oxide. The method can provide siliciclastic, hydrocarbon-bearing formations treated according to the method.

79. 发明授权

US09624422B2 Methods for treating carbonate hydrocarbon-bearing formations with fluorinated amine oxides 有权
公开(公告)号：US09624422B2
公开(公告)日：2017-04-18
申请号：US13996143
申请日：2011-12-20
申请人： Rudolf J. Dams , Yong K. Wu , Steven J. Martin
发明人： Rudolf J. Dams , Yong K. Wu , Steven J. Martin
IPC分类号： C09K8/60 , E21B43/25 , C09K8/035 , C09K8/506 , C09K8/575 , C09K8/584 , C09K8/68 , C09K8/80 , C09K8/88
CPC分类号： C09K8/60 , C09K8/035 , C09K8/506 , C09K8/5751 , C09K8/584 , C09K8/604 , C09K8/68 , C09K8/80 , C09K8/88 , E21B43/25
摘要： A method of treating a carbonate hydrocarbon-bearing formation is disclosed. The method includes contacting the hydrocarbon-bearing formation with a composition comprising solvent and a fluorinated amine oxide. Carbonate hydrocarbon-bearing formations treated according to the method are also disclosed.

80. 发明申请

US20140066572A1 FLUOROPOLYETHER ELASTOMER COMPOSITIONS HAVING LOW GLASS TRANSITION TEMPERATURES 有权
标题翻译：具有低玻璃化转变温度的氟聚乙烯弹性体组合物
公开(公告)号：US20140066572A1
公开(公告)日：2014-03-06
申请号：US14009929
申请日：2012-03-13
申请人： Steven G. Corveleyn , Miguel A. Guerra , Rudolf J. Dams , Tom Opstal
发明人： Steven G. Corveleyn , Miguel A. Guerra , Rudolf J. Dams , Tom Opstal
IPC分类号： C08K5/14
CPC分类号： C08K5/14 , C08G65/007 , C08G2650/48 , C08L71/00
摘要： A curable composition is provided. The curable composition has at least one functionalized fluoropolyether and at least one radical curing system. Further provided are fluoroelastomer compositions having a glass transition temperature of less than −40° C. and shaped articles comprising fluoroelastomers having glass transition temperatures of less than −40° C. obtained by curing the curable compositions. Also described are methods of making fluoroelastomer compositions having glass transition temperatures of less than −40° C.
摘要翻译：提供可固化组合物。可固化组合物具有至少一种官能化氟聚醚和至少一种自由基固化体系。还提供了玻璃化转变温度低于-40℃的含氟弹性体组合物和通过固化可固化组合物获得的包含玻璃化转变温度低于-40℃的含氟弹性体的成型制品。还描述了制备玻璃化转变温度低于-40℃的含氟弹性体组合物的方法。

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