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71. 发明申请

US20070112156A1 Linear perfluoropolyethers having an improved thermooxidative stability 有权
标题翻译：具有改善的热氧化稳定性的线性全氟聚醚
公开(公告)号：US20070112156A1
公开(公告)日：2007-05-17
申请号：US11648549
申请日：2007-01-03
申请人： Pier Guarda , Giuseppe Marchionni
发明人： Pier Guarda , Giuseppe Marchionni
IPC分类号： B32B27/00
CPC分类号： C08G65/007 , Y10T428/3154
摘要： Linear perfluoropolyethers of formula: T-O(CF2O)n(CF2CF2O)m(CF2CF2CF2O)r(CF2CF2CF2CF2O)s-T1 (I)wherein n, m, r, s are integers such that the polymer number average molecular weight is comprised between 700 and 100,000 and the n/(n+m+r+s) ratio ranges from 0.05 to 0.40, and respective preparation process by addition of a peroxidic perfluoropolyether of formula (III): T4-O(CF2O)n′(CF2CF2O)m′(O)h-T5 (III)having a PO from 1.8 to 4, to a perfluoropolyether oil preheated at a temperature comprised between 150° C. and 250° C. and subsequent exhaustive fluorination of the obtained compound.
摘要翻译：线性全氟聚醚，其结构如下：<？in-line-formula description =“In-line formula”end =“lead”？>（CF 2 O 2）n（CF （CF 2）2 CF 2 O 2（CF 2）2 CF 2，（CF 2）2 CF 2 CF 2 CH 2 CF 2 R 2 CF （I）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中n， m，r，s是整数，使得聚合物数均分子量在700和100,000之间，n /（n + m + r + s）的比例为0.05至0.40，各自的制备方法通过加入过氧化物式（III）的全氟聚醚：<？in-line-formula description =“In-line Formulas”end =“lead”？> T （O）n'（CF 2）2 O 2）（O）H（O）对于全氟聚醚油进行预热的“=”在线公式“末端=”尾“→具有1.8至4的PO，在包含的温度下在150℃和250℃之间，随后彻底氟化所得化合物。

72. 发明申请

US20060281640A1 Fluorinated lubricants 审中-公开
标题翻译：氟化润滑剂
公开(公告)号：US20060281640A1
公开(公告)日：2006-12-14
申请号：US11448670
申请日：2006-06-08
申请人： Patrizia Maccone , Giuseppe Marchionni
发明人： Patrizia Maccone , Giuseppe Marchionni
IPC分类号： C10M169/00
CPC分类号： C10M169/041 , C10M107/38 , C10M147/04 , C10M2213/04 , C10M2213/043 , C10N2220/021 , C10N2220/022 , C10N2230/08 , C10N2240/06 , C10N2240/30
摘要： Fluorinated lubricants comprising “pour point depressant” additives of structure: X1—O(CF2O)n(CF2CF2O)m(CF2CF2CF2O)p(CF2CF2CF2CF2O)q—X2 (I)wherein X1, X2, have formula —(CF2)zCF3 wherein z is an integer from 0 to 3; n is an integer between 1 and 200; m is an integer between 0 and 200; p, q are integers between 0 and 10; (p+q)/(p+q+m+n)≦0.05; m/n≦0.7; the number average molecular weight of (I) is between 1,000 and 10,000.
摘要翻译：包含“倾点下降剂”添加剂结构的氟化润滑剂：<？in-line-formula description =“In-line formula”end =“lead”？> X 1 -O （CF 2）（CF 2）（CF 2）O（CH 2）n（CH 2）（CF 2）2 CF 2 O 2（CF 2）2 CF 2（CF 2）2 CF 2 （CF 2）2 CF 2 O 2 Q 2 -X 2（I）<β在线公式描述 =“内联式”末端=“尾”→其中X 1，X 2，具有式 - （CF 2 H 2）其中z是0-3的整数;其中z是0-3的整数; n是1和200之间的整数; m是0和200之间的整数; p，q是0和10之间的整数; （p + q）/（p + q + m + n）<= 0.05; m / n <= 0.7; （I）的数均分子量在1,000和10,000之间。

73. 发明授权

US06982173B2 PFPEs having at least an alkylether end group and respective preparation process 有权
标题翻译：具有至少烷基醚端基的PFPE和各自的制备方法
公开(公告)号：US06982173B2
公开(公告)日：2006-01-03
申请号：US10179977
申请日：2002-06-26
申请人： Giuseppe Marchionni , Mario Visca
发明人： Giuseppe Marchionni , Mario Visca
IPC分类号： G01N33/00
CPC分类号： C08G65/007 , C08G65/334 , C08G65/337 , C09K5/10 , Y10T436/200833 , Y10T436/206664
摘要： Perfluoropolyethers having structural formula R1O—(CF2O)n—(CF2CF2O)mR2 (I) wherein: R1 is —CH3 or —C2H5; R2 is equal to R1 or —CF2H n is 0 or an integer from 1 to 100; m is an integer from 1 to 100 or, when R2 is —CF2H, m can also be 0; the oxyfluoro-alkylene units —(CF2CF2O)— and —(CF2O)— are statistically distributed along the polymer chain.
摘要翻译：具有结构式<？in-line-formula description =“In-line Formulas”的全氟聚醚结束=“lead”→R 1 O-（CF 2 O）（CF 2）2 R 2（I）其中R 1，R 2，R 2，R 2，？in-line-formula description =“In-line formula”end =“tail”？>其中：R 1是-CH 3或-C 2 5 5; R 2等于R 1或-CF 2 H n是0或1至100的整数; m为1至100的整数，或当R 2为-CF 2 H时，m也可为0; 氧氟基亚烷基单元 - （CF 2 2 CF 2 O） - 和 - （CF 2 O） - 沿着聚合物链统计分布。

74. 发明申请

US20050197469A1 Peroxidic perfluoropolyethers 有权
标题翻译：过氧化全氟聚醚
公开(公告)号：US20050197469A1
公开(公告)日：2005-09-08
申请号：US11063976
申请日：2005-02-24
申请人： Giuseppe Marchionni , Pier Guarda
发明人： Giuseppe Marchionni , Pier Guarda
IPC分类号： C07C407/00 , C07C409/20 , C07C409/42 , C08G65/00 , C08G65/30 , C08G65/32 , C08G65/332 , C08G65/334 , C07C409/44 , C07C409/24 , C08G59/14
CPC分类号： C08G65/32 , C08G65/007
摘要： Peroxidic perfluoropolyethers having formula: X1—O(CF2O)n1(CF2CF2O)m1(CF2(CF2)zCF2O)p1(O)h—X2 (I)wherein: X1 and X2, equal to or different from each other, are chain end groups selected among —CF2COF, —COF, —SO2F; n1, m1, p1 and h are integers such that the number average molecular weight is in the range 700-100,000; z=1 or 2; with the proviso that: the m1/n1 ratio is between 0.2 and 10; the p1/(n1+m1) ratio is lower than 0.05; the h/(n1+m1+p1) ratio is such that the PO content, defined as grams of active oxygen/100 g of compound, is in the range 0.8-4.5, preferably 1.4-3.8; the perfluorooxyalkylene units being statistically distributed along the polymeric chain.
摘要翻译：具有下式的过氧化全氟聚醚：<？in-line-formula description =“In-line Formulas”end =“lead”？> X 1 -O（CF 2 O）（CF 2）2（CF 2）2（CF 2）（CF 2）（CF 2）（O） > 2 <？in-line-formula description =“In-line Formulas”end =“tail”？>其中：X 1和X 2 < SUB>，彼此相同或不同，为选自-CF 2 COF，-COF，-SO 2 F的链端基; n1，m1，p1和h是数均分子量在700-100,000范围内的整数; z = 1或2; 条件是：m1 / n1比在0.2和10之间; p1 /（n1 + m1）比低于0.05; h /（n1 + m1 + p1）的比例使得定义为活性氧克数/ 100g化合物的PO含量在0.8-4.5，优选1.4-3.8的范围内; 全氟氧化烯单元沿着聚合物链统计分布。

75. 发明授权

US06403539B1 Perfluoropolyether lubricant containing sulphonylfluoride groups 有权
标题翻译：含氟磺酰氟基团的全氟聚醚润滑剂
公开(公告)号：US06403539B1
公开(公告)日：2002-06-11
申请号：US09631880
申请日：2000-08-02
申请人： Giuseppe Marchionni , Ugo De Patto
发明人： Giuseppe Marchionni , Ugo De Patto
IPC分类号： C10M10738
CPC分类号： C08G65/007 , C10M107/38 , C10M2221/02
摘要： Perfluoropolyether lubricants containing sulphonylfluoride groups pending along the perfluoropolyether chain and having the following formula: wherein: T are end groups selected from —CF2X (X═F,CF3Cl), —C3F7, —COF, —CF(CF3)COF, —CF2COF, —CF2COCF3; d,e,f,h are integers; a,b,c can be zero or integers; said units are statistically distributed along the chain, being a+b+c+d+e+f+h such that the number average molecular weight ranges from 500 to 5×105, preferably from 1,000 to 50,000.
摘要翻译：包含沿着全氟聚醚链悬浮的磺酰氟化物基团的全氟聚醚润滑剂并具有下式：其中：T是选自-CF 2 X（X = F，CF 3 Cl），-C 3 F 7，-CF，-CF（CF 3）COF，-CF 2 COF， -CF 2 COCF 3; d，e，f，h为整数; a，b，c可以为零或整数; 所述单元沿着链统计分布，为+ b + c + d + e + f + h，使得数均分子量为500〜5×10 5，优选为1,000〜50,000。

76. 发明授权

US06020298A Solvent cleaning agents including additives of the formula R.sub.f -CFX-L containing perfluoroalkylenic units 失效
标题翻译：包括含有全氟亚烷基单元的式Rf-CFX-L的添加剂的溶剂清洗剂
公开(公告)号：US06020298A
公开(公告)日：2000-02-01
申请号：US71807
申请日：1998-05-04
申请人： Rossella Silvani , Gianfranco Spataro , Giuseppe Marchionni
发明人： Rossella Silvani , Gianfranco Spataro , Giuseppe Marchionni
IPC分类号： C11D7/50 , C11D3/24 , C11D3/20 , C11D3/43
CPC分类号： C11D7/5018
摘要： Use of solvents capable of removing oily substances without solubilizing them, consisting of hydrofluoropolyethers having the general formulaHF.sub.2 CO(CF.sub.2 O).sub.n (CF.sub.2 CF.sub.2 O).sub.m CF.sub.2 Hwherein n and m are integers comprised between 0 and 20, excluding when m and n are contemporaneously 0, and having boiling point from 30.degree. to 200.degree. C. and having a molar ratio 0/C comprised between 0.5-1.
摘要翻译：使用能够除去油状物质而不溶解的溶剂，由具有通式HF 2 CO（CF 2 O）n（CF 2 CF 2 O）m CF 2 H的氢氟聚醚组成，其中n和m为0和20之间的整数，不包括当m和n同时为0时，以及沸点为30〜200℃，摩尔比0 / C为0.5-1。

77. 发明授权

US5354922A Perfluoropolyoxyalkylene endowed with a high viscosity and a low peroxide oxygen content, and process for preparing them 失效
标题翻译：全氟聚氧化烯具有高粘度和低过氧氧含量，以及制备它们的方法
公开(公告)号：US5354922A
公开(公告)日：1994-10-11
申请号：US871991
申请日：1992-04-22
申请人： Giuseppe Marchionni , Anna M. Staccione , Pier A. Guarda
发明人： Giuseppe Marchionni , Anna M. Staccione , Pier A. Guarda
IPC分类号： C07C41/05 , C07C43/12 , C07C407/00 , C07C409/20 , C08G18/50 , C08G63/682 , C08G65/00 , C07C409/00
CPC分类号： C08G65/007 , C08G18/5015 , C08G63/682
摘要： Peroxy perfluoropolyoxyalkylenes are prepared with high yields by carrying out the photo-oxidation of tetrafluoroethylene with molecular oxygen, by means of ultraviolet radiations, operating in the presence of pentafluorochloroethane as a solvent for tetrafluoroethylene.Thus, it is possible to obtain peroxy perfluoropolyoxyalkylenes having a viscosity at 20.degree. C. ranging from 300,000 to 8,000,000 cSt and endowed with a peroxide content not higher than 4.Such perfluoropolyoxyalkylenes provide, through chemical reduction, perfluoropolyoxyalkylenes endowed with a functionality higher than 1.9 and at the same time with a high molecular weight.
摘要翻译：过氧全氟聚氧化烯以高产率制备，通过在五氟氯乙烷作为四氟乙烯溶剂的存在下进行紫外辐射进行四氟乙烯与分子氧的光氧化反应。因此，可以获得在20℃下具有30万至8,000,000cSt的粘度并具有不高于4的过氧化物含量的过氧全氟聚氧化烯。这种全氟聚氧化烯通过化学还原提供赋予功能高于1.9的全氟聚氧化烯同时具有高分子量。

78. 发明授权

US5155282A Perfluoropolyethers having brominated end groups and fluoroelastomers obtained therefrom 失效
标题翻译：具有溴化端基的全氟聚醚和由其获得的含氟弹性体
公开(公告)号：US5155282A
公开(公告)日：1992-10-13
申请号：US605421
申请日：1990-10-30
申请人： Giuseppe Marchionni , Gian T. Viola , Giulio Tommasi , Raffaele Ferro , Gianna Cirillo
发明人： Giuseppe Marchionni , Gian T. Viola , Giulio Tommasi , Raffaele Ferro , Gianna Cirillo
IPC分类号： C08G65/00 , C08L21/00 , C08L27/12
CPC分类号： C08L21/00 , C08G65/005 , C08L27/12
摘要： New perfluoropolyethers comprising repeating units chosen from among ##STR1## statistically distributed along the chain, having a controlled molecular weight and brominated end groups, prepared starting from the product of the photochemical oxidation of C.sub.2 F.sub.4, and/or C.sub.3 F.sub.6, containing peroxidic oxygen, and subsequent treatment in liquid phase with bromine, at temperatures ranging from -40.degree. to 130.degree. C. in the presence of ultraviolet radiations, said new perfluoropolyethers derivatives being useful as additives in rubber mixes vulcanizable with peroxides, in amounts of 0.01 to 5 parts by w per 100 parts by weight of elastomer, optionally in combination with non brominated perfluoropolyethers, to improve the processability in the extrusion and the detachability of the vulcanized articles from the molding.
摘要翻译：新的全氟聚醚包含选自沿着链统计分布的具有受控分子量和溴化末端基团的重要单元的重复单元，其由含有过氧化氧的C2F4的光化学氧化产物和/或C3F6产物制备，随后所述新的全氟聚醚衍生物在紫外线辐射的存在下在-40℃至130℃的温度范围内用溴液相处理，所述新的全氟聚醚衍生物可用作可硫化为过氧化物的橡胶混合物中的添加剂，其量为0.01至5重量份每100重量份弹性体，任选地与非溴化全氟聚醚组合，以改善硫化制品的挤出加工性和脱模性。

79. 发明授权

US5149842A Process for preparing peroxide perfluoropolyethers 失效
标题翻译：制备过氧化全氟丙烯的方法
公开(公告)号：US5149842A
公开(公告)日：1992-09-22
申请号：US613483
申请日：1990-10-31
申请人： Dario Sianesi , Antonio Marraccini , Giuseppe Marchionni
发明人： Dario Sianesi , Antonio Marraccini , Giuseppe Marchionni
IPC分类号： C08G65/00
CPC分类号： C08G65/007
摘要： A process is disclosed for preparing peroxidic perfluoropolyethers comprising perfluoroalkylenoxy units having at least two carbon atoms, characterized in that one or more perfluoroolefins, except tetrafluoroethylene used alone, are reacted with oxygen in the liquid phase at a temperature not exceeding 50.degree. C. and in the presence of one or more compounds having one or more F-X bonds, in which X is selected from the group consisting of F, O and Cl.

80. 发明授权

US5144092A Perfluoropolyethers and processes for their preparation 失效
标题翻译：全氟聚醚及其制备方法
公开(公告)号：US5144092A
公开(公告)日：1992-09-01
申请号：US664858
申请日：1991-03-05
申请人： Antonio Marraccini , Antonio Pasquale , Anna M. Staccione , Giuseppe Marchionni
发明人： Antonio Marraccini , Antonio Pasquale , Anna M. Staccione , Giuseppe Marchionni
IPC分类号： C08G65/00 , C08G65/321 , C08G65/329
CPC分类号： C08G65/329 , C08G65/007 , C08G65/321
摘要： The invention relates to new peroxide perfluoropolyethers having formula: ##STR1## wherein: A and B are end groups,X represents a (R'O).sub.m R" group where R' is selected from the class consisting of ##STR2## and R" is a perfluoroalkyl group; the value of "m" ranging from 0 to 6. The invention relates also to processes for preparing said perfluoropolyethers and other classes of non peroxide perfluoropolyethers derived therefrom.

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