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61. 发明授权

US06720112B2 Lithium cell based on lithiated transition metal titanates 失效
标题翻译：锂电池基于锂化过渡金属钛酸盐
公开(公告)号：US06720112B2
公开(公告)日：2004-04-13
申请号：US09969440
申请日：2001-10-02
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey L. Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey L. Swoyer
IPC分类号： H01M448
CPC分类号： H01M4/485 , C01G23/003 , C01G31/006 , C01G45/006 , C01G49/009 , C01G51/42 , C01G53/42 , C01P2002/32 , C01P2002/72 , C01P2002/76 , C01P2002/77 , C01P2004/41 , C01P2006/40 , C01P2006/60 , H01M4/136 , H01M4/5825 , H01M4/587 , H01M10/0525 , H01M10/446
摘要： An electrochemical active material contains a lithiated zirconium, titanium, or mixed titanium/zirconium oxide. The oxide can be represented by the formula LiM′M″XO4, where M′ is a transition metal, M″ is an optional three valent non-transition metal, and X is zirconium, titanium, or a combination of the two. Preferably, M′ is nickel, cobalt, iron, manganese, vanadium, copper, chromium, molybdenum, niobium, or combinations thereof. The active material provides a useful composite electrode when combined with a polymeric binder and electrically conductive material. The active material can be made into a cathode for use in a secondary electrochemical cell. Rechargeable batteries may be made by connecting a number of such electrochemical cells.
摘要翻译：电化学活性材料含有锂化锆，钛或混合的钛/锆氧化物。氧化物可以由式LiM'M'XO4表示，其中M'是过渡金属，M“是任选的三价非过渡金属，X是锆，钛或两者的组合。优选地，M'是镍，钴，铁，锰，钒，铜，铬，钼，铌或其组合。当与聚合物粘合剂和导电材料组合时，活性材料提供有用的复合电极。活性材料可以制成用于二次电化学电池的阴极。可以通过连接多个这样的电化学电池来制造可充电电池。

62. 发明授权

US06720110B2 Lithium-containing phosphates, method of preparation, and uses thereof 有权
标题翻译：含锂磷酸盐，制备方法及其用途
公开(公告)号：US06720110B2
公开(公告)日：2004-04-13
申请号：US09776843
申请日：2001-02-05
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M458
CPC分类号： H01M10/0525 , C01B25/45 , H01M4/0459 , H01M4/5825 , H01M10/05 , H01M2004/027 , H01M2004/028
摘要： The invention provides an electrochemical cell which comprises a first electrode and a second electrode which is a counter electrode to said first electrode. The first electrode comprises a phosphorous compound of the nominal general formula Li3E′aE″b(PO4)3, desirably at least one E is a metal; and preferably, Li3M′M″(PO4)3. E′ and E″ are the same or different from one another. Where E′ and E″ are the same, they are preferably metals having more than one oxidation state. Where E′ and E″ are different from one another, they are preferably selected from the group of metals where at least one of E′ and E″ has more than one oxidation state.
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和作为与所述第一电极相对的电极的第二电极。第一电极包括标称通式为Li 3 E''E'b（PO 4）3的磷化合物，理想的是至少一个E是金属; 优选Li 3 M'M“（PO 4）3。 E'和E“彼此相同或不同。当E'和E“相同时，它们优选为具有多于一种氧化态的金属。其中E'和E“彼此不同，它们优选选自E'和E”中的至少一个具有多于一个氧化态的金属组。

63. 发明授权

US06702961B2 Preparation of lithium-containing materials 有权
标题翻译：含锂材料的制备
公开(公告)号：US06702961B2
公开(公告)日：2004-03-09
申请号：US10461842
申请日：2003-06-13
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M458
CPC分类号： H01M4/5825 , C01B25/37 , C01B25/45 , C01G21/00 , C01G31/00 , C01G39/00 , C01P2006/40 , H01M4/13 , H01M4/131 , H01M4/136 , H01M4/1391 , H01M4/1397 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/582 , H01M6/40 , H01M10/052 , H01M10/0525 , H01M10/0566 , Y10T29/10 , Y10T156/1002
摘要： The invention provides novel lithium-mixed metal materials which, upon electrochemical interaction, release lithium ions, and are capable of reversibly cycling lithium ions. The invention provides a rechargeable lithium battery which comprises an electrode formed from the novel lithium-mixed metal materials. Methods for making the novel lithium-mixed metal materials and methods for using such lithium-mixed metal materials in electrochemical cells are also provided. The lithium-mixed metal materials comprise lithium and at least one other metal besides lithium. Preferred materials are lithium-mixed metal phosphates which contain lithium and two other metals besides lithium.
摘要翻译：本发明提供新的锂混合金属材料，其在电化学相互作用时释放锂离子，并且能够可逆地循环锂离子。本发明提供一种可再充电锂电池，其包括由新型锂混合金属材料形成的电极。还提供了制备新的锂复合金属材料的方法和在电化学电池中使用这种锂混合金属材料的方法。锂混合金属材料除锂之外还包含锂和至少一种其它金属。优选的材料是除了锂之外还含有锂和另外两种金属的锂混合金属磷酸盐。

64. 发明授权

US06387568B1 Lithium metal fluorophosphate materials and preparation thereof 有权
标题翻译：锂金属氟磷酸盐材料及其制备
公开(公告)号：US06387568B1
公开(公告)日：2002-05-14
申请号：US09559861
申请日：2000-04-27
申请人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
发明人： Jeremy Barker , M. Yazid Saidi , Jeffrey Swoyer
IPC分类号： H01M458
CPC分类号： H01M4/136 , C01B25/455 , H01M4/58 , H01M4/5825 , H01M10/0525 , H01M2004/028
摘要： The invention provides new and novel lithium-metal-fluorophosphates which, upon electrochemical interaction, release lithium ions, and are capable of reversibly cycling lithium ions. The invention provides a rechargeable lithium battery which comprises an electrode formed from the novel lithium-metal-fluorophosphates. The lithium-metal-fluorophosphates comprise lithium and at least one other metal besides lithium.
摘要翻译：本发明提供了新的和新型的锂 - 金属 - 氟磷酸盐，其在电化学相互作用时释放锂离子，并且能够可逆地循环锂离子。本发明提供一种可充电锂电池，其包括由新型锂金属 - 氟磷酸盐形成的电极。除了锂之外，锂金属 - 氟磷酸盐还包含锂和至少一种其它金属。

65. 发明授权

US06203946B1 Lithium-containing phosphates, method of preparation, and uses thereof 有权
公开(公告)号：US06203946B1
公开(公告)日：2001-03-20
申请号：US09204944
申请日：1998-12-03
申请人： Jeremy Barker , M. Yazid Saidi
发明人： Jeremy Barker , M. Yazid Saidi
IPC分类号： H01M458
CPC分类号： H01M10/0525 , C01B25/45 , H01M4/0459 , H01M4/5825 , H01M10/05 , H01M2004/027 , H01M2004/028
摘要： The invention provides an electrochemical cell which comprises a first electrode and a second electrode which is a counter electrode to said first electrode. The first electrode comprises a phosphorous compound of the nominal general formula Li3E′aE″b(PO4)3, desirably at least one E is a metal; and preferably, Li3M′M″(PO4)3. E′ and E″ are the same or different from one another. Where E′ and E″ are the same, they are preferably metals having more than one oxidation state. Where E′ and E″ are different from one another, they are preferably selected from the group of metals where at least one of E′ and E″ has more than one oxidation state.

66. 发明授权

US5869207A Stabilized electrochemical cell 失效
标题翻译：稳定电化学电池
公开(公告)号：US5869207A
公开(公告)日：1999-02-09
申请号：US762081
申请日：1996-12-09
申请人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
发明人： M. Yazid Saidi , Chariclea Scordilis-Kelley , Jeremy Barker
IPC分类号： C01G45/00 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/0567 , H01M10/36
CPC分类号： H01M4/505 , C01G45/1221 , C01G45/1242 , H01M10/0567 , H01M4/62 , C01P2006/40 , H01M10/0525
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention, for the first time, effectively overcomes problems which arise between the interaction of cell components and contaminate water retained in a cell. Such contaminate water reacts with the electrolyte which comprises a salt of lithium in a solvent. Solubilizing of the salt in solution with attendant interaction between the salt and water causes formation of hydrogen-containing acids. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn.sub.2 O.sub.4). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen-containing acids thereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法第一次有效地克服了细胞成分的相互作用和污染细胞中残留的水之间产生的问题。这种污染水与包含锂在溶剂中的盐的电解质反应。溶解盐中的盐与盐和水之间伴随的相互作用引起含氢酸的形成。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上是LiMn 2 O 4）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢酸反应从而中和酸的至少一部分，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。

67. 发明授权

US5824120A Electrically conductive adhesion promoters for current collectors 失效
标题翻译：用于集电器的导电粘合促进剂
公开(公告)号：US5824120A
公开(公告)日：1998-10-20
申请号：US634752
申请日：1996-04-10
申请人： Porter H. Mitchell , M. Yazid Saidi
发明人： Porter H. Mitchell , M. Yazid Saidi
IPC分类号： H01M4/13 , H01M4/62 , H01M4/66 , H01M4/60
CPC分类号： H01M4/13 , H01M4/667 , H01M4/04 , H01M4/621 , H01M4/668 , Y10T29/49108 , Y10T29/49114
摘要： A method of preparing an electrochemical cell wherein the composite electrode material adheres to the metal current collector to create good electrical contact is provided. The electrode/current collector comprises a current collector, a layer of an electrically conductive adhesion promoter formed on at least one surface of the current collector which comprises an electrically conductive material and an adhesive polymer; and a composite electrode selected from the group consisting of composite cathode and composite anode, wherein the thickness of said electrically conductive adhesive promoter is sufficient to bind the composite electrode to said current collector.
摘要翻译：提供了一种制备电化学电池的方法，其中复合电极材料粘附到金属集电器以产生良好的电接触。电极/集电器包括集电器，形成在集电器的至少一个表面上的导电粘合促进层，其包括导电材料和粘合剂聚合物; 以及选自复合阴极和复合阳极的复合电极，其中所述导电粘合剂助剂的厚度足以将复合电极结合到所述集电器。

68. 发明授权

US5789110A Cathode-active material blends comprising Li.sub.x Mn.sub.2 O.sub.4 (0<x.ltoreq.2) 失效
标题翻译：包含LixMn2O4（0
公开(公告)号：US5789110A
公开(公告)日：1998-08-04
申请号：US723241
申请日：1996-09-27
申请人： Mohamed-Yazid Saidi , Jeremy Barker , Eileen S. Saidi
发明人： Mohamed-Yazid Saidi , Jeremy Barker , Eileen S. Saidi
IPC分类号： H01M4/131 , H01M4/133 , H01M4/36 , H01M4/48 , H01M4/485 , H01M4/50 , H01M4/505 , H01M4/52 , H01M4/525 , H01M4/58 , H01M4/587 , H01M10/0525 , H01M10/0565 , H01M10/058 , H01M10/36
CPC分类号： H01M4/485 , H01M10/0525 , H01M10/058 , H01M4/364 , H01M4/505 , H01M4/525 , H01M4/5825 , H01M4/587 , H01M10/0565 , H01M4/131 , H01M4/133 , Y02T10/7011
摘要： A solid secondary lithium electrochemical cell comprises a physical mixture of Li.sub.x n.sub.2 O.sub.4 (spinel) (0
摘要翻译：固体二次锂电化学电池包括Lixn2O4（尖晶石）（0

69. 发明授权

US5770018A Method for preparing lithium manganese oxide compounds 失效
标题翻译：锰酸锂化合物的制备方法
公开(公告)号：US5770018A
公开(公告)日：1998-06-23
申请号：US630303
申请日：1996-04-10
申请人： M. Yazid Saidi
发明人： M. Yazid Saidi
IPC分类号： C01G45/00 , H01M4/133 , H01M4/1393 , H01M4/50 , H01M4/505 , H01M4/62 , H01M10/0525 , H01M10/36 , C07C1/00 , C01D1/00 , C01G45/12
CPC分类号： H01M4/505 , C01G45/1242 , H01M4/623 , C01P2002/32 , C01P2002/77 , C01P2006/40 , H01M10/0525 , H01M4/133 , H01M4/1393 , H01M4/625
摘要： The present invention provides a method of preparing an intercalation compound of the nominal general formula Li.sub.x Mn.sub.2 O.sub.4, where x is greater than 0 and less than 2, which comprises providing a manganese compound and a lithium compound and mixing such compounds in proportion which provides the desired amount of x demonstrated by the nominal general formula. The mixed compounds are then irradiated with electromagnetic radiation, desirably microwave frequency or infrared radiation whereby manganese, lithium, and oxygen combine to form the Li.sub.x Mn.sub.2 O.sub.4 having the desired quantity x of lithium. It is desired that the heating by radiation be conducted in air. Preferably, the radiation is microwave radiation and such radiation is at a frequency which causes atomic bonds to vibrate within at least a portion of the precursor compounds and/or the solvent contained in the mixture.
摘要翻译：本发明提供了制备标称通式为LixMn 2 O 4的嵌入化合物的方法，其中x大于0且小于2，其包括提供锰化合物和锂化合物，并将这些化合物按比例混合，提供所需量的x通过标称通用方程式证明。然后用电磁辐射，理想的微波频率或红外辐射照射混合的化合物，由此锰，锂和氧结合形成具有所需量x的锂的LixMn2O4。希望通过辐射进行加热在空气中进行。优选地，辐射是微波辐射，并且这种辐射的频率使得原子键在至少一部分前体化合物和/或混合物中包含的溶剂中振动。

70. 发明授权

US5759715A Lithium ion batteries containing pre-lithiated electrodes 失效
标题翻译：锂离子电池含有预锂化电极
公开(公告)号：US5759715A
公开(公告)日：1998-06-02
申请号：US723195
申请日：1996-09-27
申请人： Jeremy Barker , Mohamed-Yazid Saidi , Jeffrey L. Swoyer , Feng Gao
发明人： Jeremy Barker , Mohamed-Yazid Saidi , Jeffrey L. Swoyer , Feng Gao
IPC分类号： H01M2/16 , H01M4/48 , H01M4/58 , H01M10/40
CPC分类号： H01M10/0566 , H01M10/05 , H01M10/0525 , H01M10/0569 , H01M4/133 , H01M4/485 , H01M4/587 , H01M4/623 , H01M4/667 , H01M2/1613 , H01M2/1653 , H01M2300/0025 , H01M2300/004 , H01M2300/0082 , H01M2300/0085 , H01M4/131 , H01M4/505 , H01M4/661 , H01M4/663
摘要： The invention provides an electrochemical cell which is at least partially charged and which comprises a first electrode having an active material in particle form consisting essentially of at least partially lithiated graphite. The lithiated graphite particles are prepared by chemically or electrochemically inserting lithium ions into the particles prior to assembly of the cell. A second electrode which is a counter electrode to the first electrode has an active material consisting essentially of vanadium oxide.
摘要翻译：本发明提供了至少部分带电的电化学电池，其包括具有主要由至少部分锂化石墨组成的颗粒形式的活性材料的第一电极。在组装电池之前，通过化学或电化学地将锂离子插入颗粒中来制备锂化石墨颗粒。作为与第一电极相对的电极的第二电极具有主要由氧化钒组成的活性材料。

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