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51. 发明授权

US07645494B2 Pre-plating surface treatments for enhanced galvanic-corrosion resistance 失效
标题翻译：预镀表面处理以提高电镀耐腐蚀性
公开(公告)号：US07645494B2
公开(公告)日：2010-01-12
申请号：US12056798
申请日：2008-03-27
申请人： Richard Wu , James Cornie , Stephen Cornie , Hank Breit , Larry Ballard , Richard R. Malen , Prabhat Kumar , John Shields , Robert Desberg
发明人： Richard Wu , James Cornie , Stephen Cornie , Hank Breit , Larry Ballard , Richard R. Malen , Prabhat Kumar , John Shields , Robert Desberg
IPC分类号： C23C14/02 , B05D3/00 , B05D3/04 , C23F1/00
CPC分类号： C23C2/02 , C23C4/02 , C23C26/00 , C23C28/321 , C23C28/322 , C23C28/345 , C25D5/34 , C25D5/54 , H05K1/056 , Y10T428/12625 , Y10T428/12736 , Y10T428/24132 , Y10T428/249927 , Y10T428/30 , Y10T428/31678
摘要： The invention relates to a method that involves (a) removing graphite from at least one surface of a metal graphite composite material; (b) chemically cleaning or plasma etching the surface of the metal graphite composite material; (c) applying a metal-containing material to the surface of the chemically cleaned or plasma etched metal graphite composite material, and thereby forming an intermediate layer; (d) applying a metal coating on the intermediate layer, and thereby forming a composite material. The invention also relates to a composite material comprising (a) a metal graphite composite substrate having at least one surface that is substantially free of graphite; (b) a metal-containing intermediate layer located on a surface of the substrate; and (c) a metal coating on the intermediate layer.
摘要翻译：本发明涉及一种方法，涉及（a）从金属石墨复合材料的至少一个表面去除石墨; （b）化学清洗或等离子体蚀刻金属石墨复合材料的表面; （c）将金属含有材料施加到化学清洁或等离子体蚀刻的金属石墨复合材料的表面上，从而形成中间层; （d）在中间层上涂覆金属涂层，从而形成复合材料。本发明还涉及一种复合材料，其包括（a）具有至少一个基本上不含石墨的表面的金属石墨复合基材; （b）位于所述基板的表面上的含金属的中间层; 和（c）中间层上的金属涂层。

52. 发明申请

US20090202871A1 METAL-COATED CARBON SURFACES FOR USE IN FUEL CELLS 有权
标题翻译：用于燃料电池的金属包覆碳表面
公开(公告)号：US20090202871A1
公开(公告)日：2009-08-13
申请号：US12361120
申请日：2009-01-28
申请人： Rathindra N. Bose , Anima B. Bose
发明人： Rathindra N. Bose , Anima B. Bose
IPC分类号： H01M8/00 , B32B15/04 , C25D3/50 , C25D3/46 , C25D3/48
CPC分类号： C25B11/0405 , C25D3/46 , C25D3/48 , C25D3/50 , C25D5/54 , H01M4/8605 , H01M4/8807 , H01M4/885 , H01M4/8853 , H01M4/92 , H01M4/923 , H01M8/086 , H01M2008/1095 , Y10T428/12049
摘要： A method of coating a carbon article with a metal by reductively electropolymerizing the metal via cyclic voltammetry on the carbon article, thereby forming a metal coating on the carbon article and the polymerized metal-coated carbon article made by the method. A polymerized metal-coated carbon article having a carbon article and a metal coating disposed on an exterior surface of the carbon article, the coating being present in an amount less than about 0.1 mg/cm2. A method of using a fuel cell by forming a fuel cell with a polymerized metal-coated carbon article as a working electrode and reducing oxygen, thereby providing power to a vehicle. A fuel cell including a polymerized metal-coated carbon article as a working electrode.
摘要翻译：通过在碳制品上循环伏安法将金属还原电解聚合，从而在碳制品上形成金属涂层和通过该方法制备的聚合金属涂覆的碳制品，来涂覆金属制品的方法。一种具有碳制品和设置在碳制品的外表面上的金属涂层的聚合金属涂覆的碳制品，涂层以小于约0.1mg / cm 2的量存在。一种燃料电池的使用方法，该燃料电池通过形成具有聚合的金属涂覆的碳制品作为工作电极并且还原氧的燃料电池，由此向车辆提供动力。一种燃料电池，其包括聚合的金属涂覆的碳制品作为工作电极。

53. 发明申请

US20090159452A1 ELECTROPLATING METHOD 失效
标题翻译：电镀方法
公开(公告)号：US20090159452A1
公开(公告)日：2009-06-25
申请号：US12164429
申请日：2008-06-30
申请人： SHING-TZA LIOU , YAO-WEN BAI , RUI ZHANG , QIU-YUE ZHANG
发明人： SHING-TZA LIOU , YAO-WEN BAI , RUI ZHANG , QIU-YUE ZHANG
IPC分类号： C25D5/02
CPC分类号： C25D5/54 , C25D5/02 , C25D5/56
摘要： An electroplating method includes steps of: providing a substrate having a first portion and a second portion connected to the first portion; forming a metallic layer on a surface of the second portion; immersing the first portion of the substrate in an electrolyte solution, applying a current to the metallic layer to electroplate the first portion of the substrate with a metal layer; and moving the substrate in a direction away from the electrolyte solution during electroplating the first portion of the substrate. The method can improve a uniformity of the obtained plating layer.
摘要翻译：电镀方法包括以下步骤：提供具有连接到第一部分的第一部分和第二部分的基板; 在所述第二部分的表面上形成金属层; 将基板的第一部分浸入电解液中，向金属层施加电流以用金属层电镀基板的第一部分; 以及在电镀所述基板的第一部分期间沿着远离所述电解质溶液的方向移动所述基板。该方法可以提高所得镀层的均匀性。

54. 发明申请

US20090081500A1 FUEL CELL UTILIZING AMMONIA, ETHANOL OR COMBINATIONS THEREOF 审中-公开
标题翻译：燃料电池利用氨，乙醇或其组合
公开(公告)号：US20090081500A1
公开(公告)日：2009-03-26
申请号：US12114780
申请日：2008-05-04
申请人： Gerardine G. Botte
发明人： Gerardine G. Botte
IPC分类号： H01M8/18 , H01M8/04 , H01M8/10
CPC分类号： C25B1/00 , C25B1/02 , C25B9/06 , C25B11/041 , C25B11/0478 , C25B11/0484 , C25B11/0494 , C25D5/54 , H01M4/8615 , H01M4/8657 , H01M4/90 , H01M4/921 , H01M8/083 , H01M8/1013 , H01M8/222 , H01M2300/0014 , Y02E60/522
摘要： An fuel cell utilizing ammonia, ethanol, or combinations thereof, comprising: a housing; an anode disposed within the housing, the anode comprising at least one layered electrocatalyst, wherein the at least one layered electrocatalyst comprises at least one active metal layer and at least one second metal layer deposited on a carbon support; a basic electrolyte disposed adjacent the anode; a cathode disposed adjacent the basic electrolyte, wherein the cathode comprises a conductor; and an oxidant in communication with the cathode for connecting with a power conditioner, a load, or combinations thereof, wherein the power conditioner, the load, or combinations thereof is in communication with the anode, which oxidizes the ammonia, ethanol, or combinations thereof, causing the fuel cell to form an electric current.
摘要翻译：一种利用氨，乙醇或其组合的燃料电池，包括：壳体; 阳极，其设置在所述壳体内，所述阳极包括至少一层分层电催化剂，其中所述至少一层分层电催化剂包括至少一个活性金属层和沉积在碳载体上的至少一个第二金属层; 设置在阳极附近的基本电解质; 设置在所述碱性电解质附近的阴极，其中所述阴极包括导体; 以及与阴极连通以与功率调节器，负载或其组合连接的氧化剂，其中功率调节器，负载或其组合与阳极连通，氧化氨，乙醇或其组合，使燃料电池形成电流。

55. 发明申请

US20080314755A1 LAYERED ELECTROCATALYST FOR OXIDATION OF AMMONIA AND ETHANOL 有权
标题翻译：用于氧化氨和乙醇的层状电解质
公开(公告)号：US20080314755A1
公开(公告)日：2008-12-25
申请号：US12114782
申请日：2008-05-04
申请人： Gerardine G. Botte
发明人： Gerardine G. Botte
IPC分类号： B01J23/50 , B01J21/18 , B01J23/36 , B01J23/42 , C25D5/54 , B01J23/52 , B01J23/44 , B01J23/46
CPC分类号： C25B1/00 , C02F1/46109 , C02F1/4676 , C02F2001/46142 , C02F2101/16 , C25B1/02 , C25B9/06 , C25B11/041 , C25B11/0478 , C25B11/0484 , C25B11/0494 , C25D5/54 , H01M4/90 , H01M4/9083 , H01M4/921 , H01M4/926 , H01M4/98 , H01M8/083 , H01M8/222 , H01M2300/0014 , Y10T428/12028
摘要： A layered electrocatalyst for oxidizing ammonia, ethanol, or combinations thereof, comprising: a carbon support integrated with a conductive metal; at least one first metal plating layer at least partially deposited on the carbon support, wherein the at least one first metal plating layer is active to OH adsorption and inactive to a target species, and wherein the at least one first metal plating layer has a thickness ranging from 10 nanometers to 10 microns; and at least one second metal plating layer at least partially deposited on the at least one first metal plating layer, wherein the at least one second metal plating layer is active to the target species, and wherein the at least one second metal plating layer has a thickness ranging from 10 nanometers to 10 microns, forming a layered electrocatalyst.
摘要翻译：用于氧化氨，乙醇或其组合的层状电催化剂，包括：与导电金属一体化的碳载体; 至少部分沉积在所述碳载体上的至少一个第一金属镀层，其中所述至少一个第一金属镀层对OH吸附具有活性，对目标物质无活性，并且其中所述至少一个第一金属镀层具有厚度范围从10纳米到10微米; 以及至少部分地沉积在所述至少一个第一金属镀层上的至少一个第二金属镀层，其中所述至少一个第二金属镀层对所述目标物质是有活性的，并且其中所述至少一个第二金属镀层具有厚度范围为10纳米至10微米，形成层状电催化剂。

56. 发明申请

US20080165912A1 CLAD TUBE FOR NUCLEAR FUEL 有权
标题翻译：核燃料用管
公开(公告)号：US20080165912A1
公开(公告)日：2008-07-10
申请号：US10730612
申请日：2003-12-08
申请人： William J. Carmack , Lewis C. Hartless , Jeffrey A. Halfinger
发明人： William J. Carmack , Lewis C. Hartless , Jeffrey A. Halfinger
IPC分类号： G21C3/07 , B32B1/08 , B32B15/02 , C25D1/02
CPC分类号： G21C3/07 , C25D1/02 , C25D1/20 , C25D5/10 , C25D5/54 , Y02E30/40 , Y10T428/12771 , Y10T428/12819
摘要： A rhenium lined niobium alloy tube for use as a clad tube for nuclear fuel in a nuclear reactor. The tube is produced by an electro deposit process. A graphite mandrel is placed in the electro deposit chamber as the cathode material. Refined rhenium stock is used as the anode material. The chamber is filled with the chloride electrolyte. The chamber is closed and the electrolyte bath is heated. Current and voltage applied across the anode and cathode cause the rhenium to be deposited on the mandrel. Refined niobium alloy is then used as the anode material and applied over the rhenium on the mandrel to a desired thickness. The part is removed from the chamber and ground to the desired outside diameter. The graphite mandrel is removed from the tube.
摘要翻译：一种用于核反应堆核燃料复合管的铼衬铌合金管。该管通过电沉积工艺生产。将石墨心轴放置在电沉积室中作为阴极材料。精炼的铼原料用作阳极材料。该室充满氯化物电解质。封闭室，电解液加热。施加在阳极和阴极两端的电流和电压使得铼沉积在心轴上。然后将精制的铌合金用作阳极材料，并将其施加在心轴上的铼上至所需厚度。将该部件从腔室中取出并研磨成所需的外径。从管中取出石墨心轴。

57. 发明申请

US20080105560A1 Method for Preparing Nano Metallic Particles 审中-公开
标题翻译：纳米金属颗粒的制备方法
公开(公告)号：US20080105560A1
公开(公告)日：2008-05-08
申请号：US11674507
申请日：2007-02-13
申请人： Yu Tsan Tseng , Cheng Hsuan Lin , Po Ling Shiao
发明人： Yu Tsan Tseng , Cheng Hsuan Lin , Po Ling Shiao
IPC分类号： C23C28/02 , C25D5/48 , C25D3/12 , C25D3/20 , C25D5/00
CPC分类号： C25D7/001 , B22F2998/00 , B82Y25/00 , B82Y30/00 , C25D5/02 , C25D5/18 , C25D5/34 , C25D5/54 , C25D7/006 , H01F1/0045 , B22F1/0018
摘要： A method for preparing nano metallic particles comprises the steps of dipping a conductive substrate in an electroplating solution containing metallic ions and performing an electroplating process to form the nano metallic particles on the conductive substrate by the reduction reaction of the metallic ions. The nano metallic particles can be used as a catalyst to perform a chemical vapor deposition process to form carbon nanotubes on the conductive substrate. Subsequently, fluorescent material can be positioned on the carbon nanotubes to form a light-emitting device. When a predetermined voltage is applied between the conductive substrate and the fluorescent material, the carbon nanotubes on the conductive substrate emit electrons due to the point discharge effect, and the electrons bombard the fluorescent material to emit light beams.
摘要翻译：制备纳米金属颗粒的方法包括以下步骤：将导电基材浸入含有金属离子的电镀溶液中，并进行电镀工艺，以通过金属离子的还原反应在导电基材上形成纳米金属颗粒。纳米金属颗粒可用作催化剂以进行化学气相沉积工艺以在导电基材上形成碳纳米管。随后，可以将荧光材料定位在碳纳米管上以形成发光装置。当在导电基板和荧光材料之间施加预定电压时，导电基板上的碳纳米管由于点放电效应而发射电子，并且电子轰击荧光材料发射光束。

58. 发明申请

US20070272560A1 Method and compositions for direct copper plating and filing to form interconnects in the fabrication of semiconductor devices 有权
标题翻译：用于在半导体器件的制造中直接镀铜和填充以形成互连的方法和组合物
公开(公告)号：US20070272560A1
公开(公告)日：2007-11-29
申请号：US11708293
申请日：2007-02-20
申请人： Jose Gonzalez , Herve Monchoix
发明人： Jose Gonzalez , Herve Monchoix
IPC分类号： C25D3/38 , H01L21/44
CPC分类号： C25D3/38 , C25D5/18 , C25D5/54 , H01L21/2885 , H01L21/76877
摘要： The object of the present invention is a method and compositions for direct copper plating and filling to form interconnects in the fabrication of semiconductor devices. According to the invention, this method comprises providing an electrolytic copper bath containing, in solution in a solvent, a source of copper ions with a concentration of between 45 and 200 mM, preferably of between 45 and 100 mM and at least one copper complexing agent which is an aliphatic polyamine having 2 to 4 amine functions with a concentration of between 30 and 200 mM, preferably of between 60 and 200 mM; the copper/complexing agent(s) molar ratio being of between 0.2 and 2, preferably between 0.3 and 1.5; bringing said copper diffusion barrier layer of said substrate into contact with said electrolytic copper bath, applying an electrical bias to the substrate for a duration adjusted according to the thickness of copper to be electroplated, removing the substrate from said electrolytic copper bath.
摘要翻译：本发明的目的是在半导体器件的制造中直接镀铜和填充以形成互连的方法和组合物。根据本发明，该方法包括提供一种电解铜浴，其在溶剂中含有浓度为45-200mM，优选45-100mM的铜离子源和至少一种铜络合剂其是具有2至4个胺官能团的脂族多胺，其浓度为30至200mM，优选为60至200mM; 铜/络合剂的摩尔比为0.2至2，优选0.3至1.5; 使所述衬底的所述铜扩散阻挡层与所述电解铜浴接触，向所述衬底施加电偏压持续时间，以根据要电镀的铜的厚度调节，从所述电解铜浴移除衬底。

59. 发明申请

US20070256937A1 Apparatus and method for electrochemical processing of thin films on resistive substrates 审中-公开
标题翻译：电阻衬底薄膜电化学处理的装置和方法
公开(公告)号：US20070256937A1
公开(公告)日：2007-11-08
申请号：US11417146
申请日：2006-05-04
申请人： Veeraraghavan Basker , John Cotte , Hariklia Deligianni , Matteo Flotta
发明人： Veeraraghavan Basker , John Cotte , Hariklia Deligianni , Matteo Flotta
IPC分类号： C25D7/12
CPC分类号： C25D5/54 , C25D5/006 , C25D5/02 , C25D7/123 , C25D11/005 , C25D11/024 , C25D17/001 , C25F3/14 , H01L21/28079 , H01L21/2885
摘要： An electrochemical process comprising: providing a 125 mm or larger semiconductor wafer in electrical contact with a conducting surface, wherein at least a portion of the semiconductor wafer is in contact with an electrolytic solution, said semiconductor wafer functioning as a first electrode; providing a second electrode in the electrolytic solution, the first and second electrode connected to opposite ends of an electric power source; and irradiating a surface of the semiconductor wafer with a light source as an electric current is applied across the first and the second electrodes. The invention is also directed to an apparatus including a light source and electrochemical components to conduct the electrochemical process.
摘要翻译：一种电化学方法，包括：提供与导电表面电接触的125mm或更大的半导体晶片，其中所述半导体晶片的至少一部分与电解液接触，所述半导体晶片用作第一电极; 在所述电解液中提供第二电极，所述第一和第二电极连接到电源的相对端; 并且在第一和第二电极之间施加用作为电流的光源照射半导体晶片的表面。本发明还涉及一种包括光源和用于进行电化学过程的电化学组分的设备。

60. 发明授权

US07291385B2 Conductive film and method for preparing the same 失效
标题翻译：导电膜及其制备方法
公开(公告)号：US07291385B2
公开(公告)日：2007-11-06
申请号：US10911577
申请日：2004-08-05
申请人： Ken Kawata , Akihiko Koshika
发明人： Ken Kawata , Akihiko Koshika
IPC分类号： B32B5/16
CPC分类号： C25D5/54 , C23C18/08 , C23C18/165 , C23C18/42 , H05K3/105 , H05K3/181 , H05K3/38 , H05K2201/0347 , H05K2203/1105 , H05K2203/121 , Y10T428/25
摘要： A conductive film comprising: a support; a particle-containing layer; and a metal thin film layer, in this order, wherein the particle-containing layer contains particles having a mean particle size of from 1 to 10 μm and a heat decomposed material of a metal acetylide and has irregularities derived from a shape of the particles formed on a surface thereof, and the metal thin film layer contains a metal element.
摘要翻译：一种导电膜，包括：支撑体; 含颗粒的层; 和金属薄膜层，其中含有粒子的层含有平均粒径为1-10μm的颗粒和金属乙炔化物的热分解材料，并且具有衍生自形成的颗粒形状的不规则性在其表面上，金属薄膜层含有金属元素。

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