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51. 发明授权

US5097055A Production of methylphenyltrisiloxane 失效
标题翻译：甲基苯基硅氧烷的生产
公开(公告)号：US5097055A
公开(公告)日：1992-03-17
申请号：US680696
申请日：1991-04-04
申请人： Katsuhiro Uehara , Toshinobu Ishihara , Jiyunitirow Maruta , Akira Hayashida
发明人： Katsuhiro Uehara , Toshinobu Ishihara , Jiyunitirow Maruta , Akira Hayashida
IPC分类号： C07F7/08
CPC分类号： C07F7/0874
摘要： A process of producing a methylphenyltrisiloxane having the following general formula: ##STR1## wherein R.sup.1 and R.sup.2 may be the same or different and are each a methyl or phenyl group, the process comprising the step of reacting:(A) methyldiphenylsilanol, with(B) a silazane compound having a diorganosilazane unit having the following formula: ##STR2## wherein R.sup.1 and R.sup.2 are as defined above. According to the process, colorless and odorless methylphenyltrisiloxanes can be obtained easily, safely and economically, without any special deodorizing or decoloring step.

52. 发明授权

US5081260A 3-(2-oxo-1-pyrrolidinyl)-propylsilanes and method for preparing the silane compounds 失效
标题翻译： 3-（2-氧代-1-吡咯烷基）丙烯酸酯及其制备硅烷化合物的方法
公开(公告)号：US5081260A
公开(公告)日：1992-01-14
申请号：US508570
申请日：1990-04-13
申请人： Tohru Kubota , Toshinobu Ishihara , Mikio Endo
发明人： Tohru Kubota , Toshinobu Ishihara , Mikio Endo
IPC分类号： C07F7/18 , C09K3/18
CPC分类号： C07F7/1824 , C09K3/18
摘要： 3-(2-oxo-1-pyrrolidinyl)-propylsilane compounds represented by the following general formula (I) are herein disclosed: ##STR1## wherein R.sup.1 and R.sup.2 may be the same or different and each represents a hydrocarbon group having 1 to 4 carbon atoms; and n is an integer ranging from 0 to 2. The propylsilane compounds may be prepared by, for instance, reacting 1-allyl-2-oxopyrrolidine with a hydrogen silane such as trimethoxysilane or trichlorosilane in the presence of a platinum catalyst or further optionally reacting the resulting 3-(2-oxo-1-pyrrolidinyl)-propyl halogenosilane (in the case where a halogenosilane is used) with an alcohol such as methanol. These propylsilane compounds are effective as anti-clouding agent for treating the surface of a variety of substrate.

53. 发明授权

US4727172A Method for the preparation of an organosiloxane oligomer and a novel organosiloxane oligomer thereby 失效
标题翻译：由此制备有机硅氧烷低聚物和新型有机硅氧烷低聚物的方法
公开(公告)号：US4727172A
公开(公告)日：1988-02-23
申请号：US905576
申请日：1986-09-09
申请人： Akira Yamamoto , Minoru Takamizawa , Toshinobu Ishihara , Tadao Kurosaki
发明人： Akira Yamamoto , Minoru Takamizawa , Toshinobu Ishihara , Tadao Kurosaki
IPC分类号： C07F7/08
CPC分类号： C07F7/0852 , C07F7/0874
摘要： An efficient method is proposed for the preparation of an organosiloxane oligomer represented by the general formula YSi(R.sup.1).sub.n (--O--SiR.sub.3).sub.3-n, in which each of the groups denoted by R and R.sup.1 is a halogen-substituted or unsubstituted monovalent hydrocarbon group having 1 to 8 carbon atoms, Y is a hydrogen atom or a monovalent group selected from methyl, phenyl, vinyl, chloromethyl and 3-(meth)acryloxypropyl groups and n is zero, 1 or 2, by the reaction of an organosilicon halomagnesium salt of the formula R.sub.3 Si--O--MgX, in which X is a halogen atom, and an organosilane compound of the general formula YSi(R.sup.1).sub.n (Z).sub.3-n, in which Z is a halogen atom or a lower alkoxy group. In particular, tetrasiloxane compounds represented by the general formula Y.sup.1 Si[--O--Si(CH.sub.3).sub.2 (CH.sub.2 CH.sub.2 CF.sub.3)].sub.3, in which Y.sup.1 is a hydrogen atom, chloromethyl group or 3-methacryloxypropyl group, are each a novel compound not known in the prior art.
摘要翻译：提出了制备由通式YSi（R1）n（-O-SiR 3）3-n表示的有机硅氧烷低聚物的有效方法，其中由R和R 1表示的每个基团是卤素取代或未取代的具有1至8个碳原子的一价烃基，Y是氢原子或选自甲基，苯基，乙烯基，氯甲基和3-（甲基）丙烯酰氧基丙基的一价基团，并且n为0,1或2，通过其中X为卤素原子的式R3Si-O-MgX的有机硅卤镁盐和通式YSi（R1）n（Z）3-n的有机硅烷化合物，其中Z为卤素原子或低级烷氧基。特别地，由通式Y1Si [-O-Si（CH3）2（CH2CH2CF3）] 3表示的四硅氧烷化合物，其中Y 1为氢原子，氯甲基或3-甲基丙烯酰氧基丙基，均为未知的新化合物现有技术

54. 发明授权

US4339397A Method for the preparation of a sodium salt of 1-alkyne compound 失效
标题翻译： 1-炔炔化合物钠盐的制备方法
公开(公告)号：US4339397A
公开(公告)日：1982-07-13
申请号：US209266
申请日：1980-11-21
申请人： Toshinobu Ishihara , Kenichi Taguchi , Akira Yamamoto
发明人： Toshinobu Ishihara , Kenichi Taguchi , Akira Yamamoto
IPC分类号： C07F1/04
CPC分类号： C07F1/04
摘要： The invention provides a novel and improved method for the preparation of a sodium salt of a 1-alkyne of the general formula ##STR1## in which R.sup.1 and R.sup.2 are each a hydrogen atom or a monovalent hydrocarbon group free from aliphatic unsaturation, by the reaction of a corresponding 1,2-alkadiene with metallic sodium in an inert organic solvent. According to the invention, the metallic sodium is dispersed in the inert solvent as finely as possible to have a particle diameter not exceeding 1000 .mu.m so as that the reaction velocity is very much increased even under atmospheric pressure to give an improved yield of the product.
摘要翻译：本发明提供了一种制备通式“IMAGE”的1-炔的钠盐的新型改进方法，其中R 1和R 2各自为氢原子或不含脂肪族不饱和键的单价烃基，通过反应的相应的1,2-链二烯与金属钠在惰性有机溶剂中反应。根据本发明，金属钠尽可能细地分散在惰性溶剂中以具有不超过1000μm的粒径，使得即使在大气压下反应速度也非常大，以提高产物的产率。

55. 发明授权

US4324931A 1-Halo-4-decene compounds 失效
标题翻译： 1-卤代-4-癸烯化合物
公开(公告)号：US4324931A
公开(公告)日：1982-04-13
申请号：US206991
申请日：1980-11-14
申请人： Toshinobu Ishihara , Kenichi Taguchi , Akira Yamamoto , Nobuo Takasaka , Hisashi Shimizu , Mitsuyoshi Oshima
发明人： Toshinobu Ishihara , Kenichi Taguchi , Akira Yamamoto , Nobuo Takasaka , Hisashi Shimizu , Mitsuyoshi Oshima
IPC分类号： A01N29/02 , C07C17/00 , C07C17/16 , C07C17/263 , C07C21/02 , C07C21/04 , C07C21/14 , C07C21/17 , C07C29/17 , C07C29/36 , C07C67/00
CPC分类号： C07C17/16 , C07C21/04 , C07C21/14 , C07C29/17 , C07C29/36
摘要： The invention provides a novel class of organic compounds 1-halo-4-decene as a useful intermediate for the synthesis of cis-6-heneicosen-11-one which is a promising exterminating chemical of the noxious insect Douglas-fir tussock moth in North American forests acting as a sexual pheromone. The synthetic procedures for the synthetic preparation of the above 1-halo-4-decene are also described.
摘要翻译：本发明提供了一种新型的有机化合物1-卤代-4-癸烯作为合成顺式-6-己烯-7-酮的有用中间体，其是北方有害昆虫道格拉斯冷杉蛾飞蛾的有前途的灭绝化学物质美国森林作为一种性信息素。还描述了合成制备上述1-卤代-4-癸烯的合成方法。

56. 发明授权

US09410951B2 Method for producing substrate for making microarray 有权
标题翻译：制备微阵列的基质的制备方法
公开(公告)号：US09410951B2
公开(公告)日：2016-08-09
申请号：US12458637
申请日：2009-07-17
申请人： Wataru Kusaki , Takeshi Kinsho , Toshinobu Ishihara
发明人： Wataru Kusaki , Takeshi Kinsho , Toshinobu Ishihara
IPC分类号： G01N33/543 , C40B40/04 , C40B50/18
CPC分类号： G01N33/54353 , B01J2219/00527 , B01J2219/00596 , B01J2219/00612 , B01J2219/00626 , B01J2219/00637 , B01J2219/00659 , C40B40/04 , C40B50/18
摘要： There is disclosed a method for producing a substrate for making a microarray, the method comprising: at least, a step of forming a monomolecular film having orientated oxysilanyl groups toward an outmost surface on the substrate; and a step of forming a monomolecular film having orientated amino groups toward an outmost surface on the substrate by applying a solution containing a diamine compound to the oxysilanyl groups. There can be provided a method for producing a substrate for making a microarray in which density and orientation of amino groups orientated toward an outmost surface are controllable, and in addition, there is no delamination of a monomolecular film formed on the substrate.
摘要翻译：公开了一种制造微阵列的基板的制造方法，该方法至少包括：向基板的最外表面形成具有取向的氧联苯乙烯基的单分子膜的工序; 以及通过将含有二胺化合物的溶液施加到氧联苯乙酰基上而形成具有取向氨基的单分子膜朝向基板上的最外表面的步骤。可以提供一种制造用于制造微阵列的基板的方法，其中朝向最外表面取向的氨基的密度和取向是可控的，此外，在基板上形成的单分子膜不会发生分层。

57. 发明授权

US07608805B2 Control system for battery powered heating device 有权
标题翻译：电池供电装置控制系统
公开(公告)号：US07608805B2
公开(公告)日：2009-10-27
申请号：US11036417
申请日：2005-01-14
申请人： Mitsuhiko Miyazaki , Toshinobu Ishihara , Hitoshi Takeuchi
发明人： Mitsuhiko Miyazaki , Toshinobu Ishihara , Hitoshi Takeuchi
IPC分类号： H05B1/02
CPC分类号： B23K3/0323 , B23K3/033 , G05D23/1917 , G05D23/2401
摘要： A control system and method of controlling a battery powered heating device such as a soldering or desoldering tool that includes a control circuit to control the delivery of power to a cartridge heating tip and to cycle the power to the cartridge heating tip during times of no use so as to minimize the amount of power expended to maintain the device in a ready or usable state.
摘要翻译：一种控制系统和控制电池供电加热装置的方法，例如焊接或脱焊工具，其包括控制电路，以控制向盒加热尖端传递电力，并且在不使用的时间期间将电力循环到盒加热尖端以便最小化维持设备处于就绪或可用状态的功率消耗。

58. 外观设计

USD530349S1 Controller for soldering iron 有权
公开(公告)号：USD530349S1
公开(公告)日：2006-10-17
申请号：US29224058
申请日：2005-02-23
申请人： Toshinobu Ishihara , Toshikazu Mochizuki
设计人： Toshinobu Ishihara , Toshikazu Mochizuki

59. 发明申请

US20060157466A1 Control system for battery powered heating device 有权
公开(公告)号：US20060157466A1
公开(公告)日：2006-07-20
申请号：US11036417
申请日：2005-01-14
申请人： Mitsuhiko Miyazaki , Toshinobu Ishihara , Hitoshi Takeuchi
发明人： Mitsuhiko Miyazaki , Toshinobu Ishihara , Hitoshi Takeuchi
IPC分类号： H05B3/02 , H05B1/00 , H05B11/00
CPC分类号： B23K3/0323 , B23K3/033 , G05D23/1917 , G05D23/2401
摘要： A control system and method of controlling a battery powered heating device such as a soldering or desoldering tool that includes a control circuit to control the delivery of power to a cartridge heating tip and to cycle the power to the cartridge heating tip during times of no use so as to minimize the amount of power expended to maintain the device in a ready or usable state.

60. 发明授权

US5783717A Method for purifying organometal compound 失效
标题翻译：有机金属化合物的纯化方法
公开(公告)号：US5783717A
公开(公告)日：1998-07-21
申请号：US517093
申请日：1995-08-21
申请人： Hiromi Ohsaki , Toshinobu Ishihara , Kazuyuki Asakura , Isao Kaneko , Kouhei Satou
发明人： Hiromi Ohsaki , Toshinobu Ishihara , Kazuyuki Asakura , Isao Kaneko , Kouhei Satou
IPC分类号： C07F3/06 , C07F5/00 , C07F5/06 , C07F3/00
CPC分类号： C07F5/063 , C07F3/06 , C07F5/00
摘要： A method for purifying an organometal compound by removing oxygen atom-containing compounds included in the organometal compound as impurities is herein disclosed. The method comprises the steps of mixing an organometal compound represented by the following formula: ##STR1## with a crude product including an oxygen atom-containing compound represented by the following formula: R.sub.3-n M.sup.1 (OR).sub.n or R.sub.2-m M.sup.2 (OR).sub.m and an alkylaluminum chloride represented by the formula: X.sub.6-q Al.sub.2 R and then distilling the resulting mixture. In the foregoing formulas, R's may be the same or different and each represents an alkyl group having 1 to 3 carbon atoms; M.sup.1 represents a trivalent metal element; M.sup.2 represents a divalent metal element; n is an integer of 1, 2 or 3; m is an integer of 1 or 2; q is an integer ranging from 1 to 5; and X represents a chlorine atom.
摘要翻译：本文公开了通过除去作为杂质的有机金属化合物中包含的含氧原子的化合物来纯化有机金属化合物的方法。该方法包括以下步骤：将由下式表示的有机金属化合物：＆lt; IMAGE＆gt;与由下式表示的含氧原子的化合物的粗产物：R3-n M1（OR）n或R2-m M2（ OR）m和由式X6-qAl2R表示的烷基氯化铝，然后蒸馏所得混合物。在上述式中，R可以相同或不同，表示碳原子数1〜3的烷基。 M1表示三价金属元素; M2表示二价金属元素; n为1,2或3的整数; m为1或2的整数; q为1〜5的整数; X表示氯原子。

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