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51. 发明授权

US07084294B2 Method for the recycling of a Lewis acid 失效
标题翻译：路易斯酸回收方法
公开(公告)号：US07084294B2
公开(公告)日：2006-08-01
申请号：US10520007
申请日：2003-07-04
申请人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
发明人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
IPC分类号： C07C253/10
CPC分类号： B01J31/24 , B01J27/32 , B01J31/1845 , B01J31/4015 , B01J31/403 , B01J2231/343 , C07C253/10 , Y02P20/584 , C07C255/07
摘要： A process for the recovery of a Lewis acid from a reaction mixture (I) which has been obtained in the hydrocyanation of an olefinically unsaturated compound to a nitrile which has a miscibility gap with water under certain pressure and temperature conditions, in the presence of a catalyst system comprising a Lewis acid and a complex compound. The method comprises a) removing the complex compound from mixture (I) to give a mixture (II), b) adding water to mixture (II) and placing mixture (II) under pressure and temperature conditions to provide a phase (III) and a phase (IV), c) adding a liquid diluent (V) which c1) does not form an azeotrope with water and whose boiling point under certain pressure conditions is higher than that of water, or c2) forms an azeotrope or heteroazeotrope with water under certain pressure conditions, to phase (III), d) subjecting the mixture of phase (III) and liquid diluent (V) to distillation under the pressure conditions mentioned in step c1) or c2), and e) subjecting mixture (VII) to hydrocyanation of an olefinically unsaturated compound to give the nitrile.
摘要翻译：从在不饱和化合物的氢氰化中获得的反应混合物（I）中回收路易斯酸的方法，该反应混合物在一定压力和温度条件下，在与催化剂体系包含路易斯酸和络合物。该方法包括：a）从混合物（I）中除去配合物，得到混合物（II），b）在混合物（II）中加入水并将混合物（II）置于压力和温度条件下以提供相（III）和相（Ⅳ），c）加入一种不与水形成共沸物的液体稀释剂（Ⅴ），其某些压力条件下的沸点高于水，或c2）与水形成共沸混合物（III），d）在步骤c1）或c2）所述的压力条件下使相（III）和液体稀释剂（V）的混合物进行蒸馏，和e）使混合物（VII）对烯属不饱和化合物进行氢化，得到腈。

52. 发明授权

US09258996B2 Composition comprising a pesticide and an alkoxylate of iso-nonylamine 有权
标题翻译：包含农药和异壬胺的烷氧基化物的组合物
公开(公告)号：US09258996B2
公开(公告)日：2016-02-16
申请号：US13048946
申请日：2011-03-16
申请人： Paul Klingelhoefer , Sophie Vogel , Kevin Huyghe , Gerd Haderlein , Gerhard Schnabel , Marc Nolte , Richard Roger Evans
发明人： Paul Klingelhoefer , Sophie Vogel , Kevin Huyghe , Gerd Haderlein , Gerhard Schnabel , Marc Nolte , Richard Roger Evans
IPC分类号： A01N25/30 , A01N25/22 , A01N57/20
CPC分类号： A01N25/30 , A01N25/22 , A01N57/20
摘要： The present invention relates to a composition comprising a pesticide and an alkoxylate. Moreover, the invention relates to the alkoxylate, to a process for its preparation and to its use as adjuvant in pesticide-comprising spray mixtures. The invention furthermore relates to a method of controlling phytopathogenic fungi and/or undesired vegetation and/or undesired insect or mite attack and/or for regulating the growth of plants, wherein the composition is allowed to act on the respective pests, their environment or the plants to be protected from the respective pest, on the soil and/or on undesirable plants and/or the crop plants and/or their environment. Furthermore, the invention relates to seed comprising the composition.
摘要翻译：本发明涉及包含农药和烷氧基化物的组合物。此外，本发明涉及烷氧基化物，其制备方法及其作为含农药喷雾混合物中的佐剂的用途。本发明还涉及一种控制植物病原真菌和/或不期望的植物和/或不期望的昆虫或螨攻击和/或调节植物生长的方法，其中允许组合物作用于相应的害虫，其环境或要保护的植物免受相应的害虫，土壤和/或不合需要的植物和/或作物植物和/或其环境的影响。此外，本发明涉及包含该组合物的种子。

53. 发明授权

US08618179B2 Composition comprising a pesticide and an alkoxylate of 2-propylheptylamine 有权
公开(公告)号：US08618179B2
公开(公告)日：2013-12-31
申请号：US13007187
申请日：2011-01-14
申请人： Paul Klingelhoefer , Arend Jouke Kingma , Sophie Vogel , Kevin Huyghe , Gerd Haderlein , Gerhard Schnabel , Marc Nolte , Richard Roger Evans
发明人： Paul Klingelhoefer , Arend Jouke Kingma , Sophie Vogel , Kevin Huyghe , Gerd Haderlein , Gerhard Schnabel , Marc Nolte , Richard Roger Evans
IPC分类号： A01N33/08 , A01N33/12 , A01N57/18 , A01N25/00 , A01N25/02 , A61K47/00 , C07C213/00 , C07C215/00 , C07C217/00 , C07C209/00
CPC分类号： A01N25/30 , A01N25/22 , A01N57/20 , C07C215/12 , A01N43/50
摘要： The present invention relates to a composition comprising a pesticide and an alkoxylate. Moreover, the invention relates to the alkoxylate, to a process for its preparation and to its use as adjuvant in pesticide-comprising spray mixtures. The invention furthermore relates to a method of controlling phytopathogenic fungi and/or undesired vegetation and/or undesired insect or mite attack and/or for regulating the growth of plants, wherein the composition is allowed to act on the respective pests, their environment or the plants to be protected from the respective pest, on the soil and/or on undesirable plants and/or the crop plants and/or their environment. Furthermore, the invention relates to seed comprising the composition.

54. 发明授权

US08450530B2 Process for preparing unsymmetric secondary tert-butylamines in the gas phase 失效
标题翻译：在气相中制备不对称二级叔丁胺的方法
公开(公告)号：US08450530B2
公开(公告)日：2013-05-28
申请号：US13080885
申请日：2011-04-06
申请人： Christoph Mueller , Christof Wilhelm Wigbers , Johann-Peter Melder , Gerd Haderlein , Norbert Gutfrucht
发明人： Christoph Mueller , Christof Wilhelm Wigbers , Johann-Peter Melder , Gerd Haderlein , Norbert Gutfrucht
IPC分类号： C07C209/16 , C07C209/26
CPC分类号： C07C209/26 , C07C211/08
摘要： The present invention relates to a process for preparing unsymmetric secondary tert-butylamines by continuous amination in the gas phase, wherein tert-butylamine is converted over hydrogenation catalysts in the presence of an alcohol or aldehyde and hydrogen.
摘要翻译：本发明涉及通过在气相中连续胺化来制备不对称仲叔丁胺的方法，其中叔丁胺在醇或醛和氢的存在下转化为氢化催化剂。

55. 发明授权

US07737310B2 Method for producing biphenols from monophenols 失效
标题翻译：从单酚生产双酚的方法
公开(公告)号：US07737310B2
公开(公告)日：2010-06-15
申请号：US11910665
申请日：2006-04-05
申请人： Michael Bartsch , Gerd Haderlein , Tobias Aechtner , Jens Scheidel , Christian Dienes , Alexander Tempel , Thorsten Hofrichter , Werner Weinle
发明人： Michael Bartsch , Gerd Haderlein , Tobias Aechtner , Jens Scheidel , Christian Dienes , Alexander Tempel , Thorsten Hofrichter , Werner Weinle
IPC分类号： C07C39/16
CPC分类号： C07C37/11 , C07C39/15
摘要： A process for preparing biphenols of the general formula I by reaction of monophenols of the general formula II where the radicals R1, R2 and R3 are each, independently of one another, hydrogen, alkyl, aryl or arylalkyl having from 1 to 10 carbon atoms, in the presence of an oxidant in a reactor, wherein a) the reactor comprises no stationary internals which act as baffles, b) a total of not more than 0.6 mol of oxidant is used per one mol of monophenol, and c) the oxidant is introduced either continuously or discontinuously in a plurality of portions over a period of from 10 minutes to 24 hours, with the amount of oxidant introduced per unit time not being constant over the total period of time but instead being varied.
摘要翻译：通式I的单酚的制备方法，其通式II的单酚，其中基团R 1，R 2和R 3各自独立地为具有1至10个碳原子的氢，烷基，芳基或芳基烷基，在反应器中存在氧化剂的情况下，其中a）反应器不包含用作挡板的固定内部物质，b）每1mol单酚使用总共不超过0.6mol的氧化剂，和c）氧化剂为在10分钟至24小时的时间内，以多个部分连续或不连续地引入，每单位时间内引入的氧化剂的量在总时间段内不是恒定的，而是变化。

56. 发明申请

US20090187039A1 Production of 3-pentenenitrile from 1,3-butadiene 有权
标题翻译：从1,3-丁二烯生产3-戊烯腈
公开(公告)号：US20090187039A1
公开(公告)日：2009-07-23
申请号：US10585590
申请日：2005-01-27
申请人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
发明人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
IPC分类号： C07C253/00
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene, wherein 1,3-butadiene is reacted with hydrogen cyanide in the presence of at least one catalyst and the stream resulting therefrom is purified distillatively, the bottom temperature during the distillation not exceeding 140° C.
摘要翻译：描述了一种通过氢化1,3-丁二烯制备3-戊烯腈的方法，其中在至少一种催化剂存在下，使1,3-丁二烯与氰化氢反应，由此产生的流体蒸馏纯化，在蒸馏不超过140℃

57. 发明申请

US20080275266A1 Method for the Production of Pentene Nitriles From N-Butane 失效
标题翻译：从丁烷生产戊烯腈的方法
公开(公告)号：US20080275266A1
公开(公告)日：2008-11-06
申请号：US10586451
申请日：2005-01-27
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Gotz-Peter Schindler , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Andreas Brodhagen
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Gotz-Peter Schindler , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Andreas Brodhagen
IPC分类号： C07C253/10
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for hydrocyanating 1,3-butadiene over at least one nickel(0) complex having phosphorus ligands as a catalyst, wherein the 1,3-butadiene is used in a mixture with n-butane and the mixture contains from 60 to 90% by volume of 1,3-butadiene and from 40 to 10% by volume of n-butane.
摘要翻译：描述了在至少一种具有磷配位体的镍（0）络合物作为催化剂中对1,3-丁二烯进行氢氰化的方法，其中1,3-丁二烯与正丁烷混合使用，混合物含有60〜 90体积％的1,3-丁二烯和40〜10体积％的正丁烷。

58. 发明授权

US07439381B2 Hydrocyanation method 失效
标题翻译：氢氰化法
公开(公告)号：US07439381B2
公开(公告)日：2008-10-21
申请号：US10586490
申请日：2005-01-26
申请人： Tim Jungkamp , Dagmar Pascale Kunsmann-Keitel , Michael Bartsch , Robert Baumann , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Dagmar Pascale Kunsmann-Keitel , Michael Bartsch , Robert Baumann , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/00
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene with hydrogen cyanide over at least one catalyst, wherein the 1,3-butadiene and/or hydrogen cyanide is contacted with at least one microporous solid before the reaction.
摘要翻译：描述了通过在至少一种催化剂上用氰化氢氢化1,3-丁二烯制备3-戊烯腈的方法，其中1,3-丁二烯和/或氰化氢在反应之前与至少一种微孔固体接触。

59. 发明申请

US20080227998A1 Method For Producing 3-Pentenenitrile 有权
标题翻译：生产3-戊烯腈的方法
公开(公告)号：US20080227998A1
公开(公告)日：2008-09-18
申请号：US10586007
申请日：2005-01-27
申请人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
发明人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
IPC分类号： C07C255/01
CPC分类号： C07C253/10 , C07C253/34 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) reacting 1,3-butadiene with hydrogen cyanide over at least one catalyst to obtain a stream 1 which comprises 3-pentenenitrile, 2-methyl-3-butenenitrile, the at least one catalyst and 1,3-butadiene, (b) distilling stream 1 in a column to obtain a high-1,3-butadiene stream 2 as the top product and a low-1,3-butadiene stream 3 as the bottom product which comprises 3-pentenenitrile, the at least one catalyst and 2-methyl-3-butenenitrile, (c) distilling stream 3 in a column to obtain a stream 4 as the top product which comprises 1,3-butadiene, a stream 5 which comprises 3-pentenenitrile and 2-methyl-3-butenenitrile at a side draw of the column, and a stream 6 as the bottom product which comprises the at least one catalyst, (d) distilling stream 5 to obtain a stream 7 as the top product which comprises 2-methyl-3-butenenitrile, and a stream 8 as the bottom product which comprises 3-pentenenitrile.
摘要翻译：描述了一种制备3-戊烯腈的方法，其特征在于以下工艺步骤：（a）使1,3-丁二烯与氰化氢在至少一种催化剂上反应，得到流1，其包含3-戊烯腈，2-甲基-3 丁烯腈，至少一种催化剂和1,3-丁二烯，（b）在塔中蒸馏物流1，得到作为顶部产物的高-1,3-丁二烯流2和低-1,3-丁二烯流 3作为底部产物，其包含3-戊烯腈，至少一种催化剂和2-甲基-3-丁烯腈，（c）在塔中蒸馏流3以获得作为顶部产物的料流4，其包含1,3-丁二烯，在塔的侧馏分中包含3-戊烯腈和2-甲基-3-丁烯腈的料流5和作为底部产物的料流6，其包含至少一种催化剂，（d）蒸馏流5以获得流7作为顶部产物，其包含2-甲基-3-丁烯腈，以及作为底部产物的料流8，其包含3-戊烯腈

60. 发明授权

US07407643B2 Process for removing water from a mixture containing water and zinc chloride 失效
标题翻译：从含水和氯化锌的混合物中除去水的方法
公开(公告)号：US07407643B2
公开(公告)日：2008-08-05
申请号：US10519513
申请日：2003-07-04
申请人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
发明人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
IPC分类号： C01B9/02
CPC分类号： C01G9/04 , B01D3/36 , F26B5/005 , F26B7/00
摘要： A process for the removal of water from a mixture comprising water and zinc chloride, which comprises adding to said mixture comprising water and zinc chloride an aprotic, polar diluent whose boiling point in the case where an azeotrope is not formed between said diluent and water under the pressure conditions of the distillation mentioned below is higher than the boiling point of water and which is in liquid form at this boiling point of water or which forms an azeotrope or heteroazeotrope with water under the pressure and temperature conditions of the distillation mentioned below, and distilling the mixture comprising water, zinc chloride and the diluent with removal of water or said azeotrope or said heteroazeotrope from this mixture, giving an anhydrous mixture comprising zinc chloride and said diluent.
摘要翻译：一种用于从包含水和氯化锌的混合物中除去水的方法，其包括向包含水和氯化锌的所述混合物中加入非质子极性稀释剂，其中在所述稀释剂和水之间未形成共沸物的情况下为沸点下述蒸馏的压力条件高于水的沸点，并且在该沸点沸点下为液体形式，或者在下述蒸馏的压力和温度条件下与水形成共沸物或杂合物，并且从该混合物中除去包含水，氯化锌和稀释剂的混合物，除去水或所述共沸物或所述杂共聚物，得到包含氯化锌和所述稀释剂的无水混合物。

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