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    • 51. 发明授权
    • Method of preparing a urea-formaldehyde combination foam that is low in
formaldehyde
    • 制备低甲醛的脲 - 甲醛组合泡沫的方法
    • US4537913A
    • 1985-08-27
    • US586966
    • 1984-03-07
    • Heinz Baumann
    • Heinz Baumann
    • C08J9/00C08J9/30
    • C08J9/30C08J9/0014C08J9/0066C08J2361/24
    • A U.F. foam that is diamensionally stable, but low in formaldehyde, was made by adding to a conventional solution of a urea formaldehyde resin precondensate, before foaming, up to 50% urea, relative to the solid resin substance, and one or several connecting agents from the group of sulfurous alkyl compounds, saturated monobasic carbonic acids, saturated and unsaturated dicarbonic acids, purine compounds, inorganic acids of the group of halogens and chalcogens, and their salts, phosphoric acids and their salts, alkali metal salts and alkaline earth metal salts, in such quantity and in such a way that the pH of the resulting solution remains above 7; and subsequently foaming the solution with a hardener/foaming-agent solution in the conventional manner.
    • 联合国 通过在常规的脲甲醛树脂预缩合物溶液中,相对于固体树脂物质在发泡之前加入高达50%的尿素,以及一种或多种连接剂来制备通常在甲醛中稳定的泡沫, 亚硫烷基化合物,饱和一元碳酸,饱和和不饱和二羧酸,嘌呤化合物,卤素和硫属元素组的无机酸及其盐,磷酸及其盐,碱金属盐和碱土金属盐,在 这样的量并且使得所得溶液的pH保持在7以上; 然后用常规方法用固化剂/发泡剂溶液使溶液发泡。
    • 52. 发明授权
    • Process for manufacturing modified amino-resin products
    • 制备改性氨基树脂产品的方法
    • US4480055A
    • 1984-10-30
    • US352721
    • 1982-02-26
    • Heinz Baumann
    • Heinz Baumann
    • C04B26/12C08G14/06C08G16/02C08L61/34C08J9/30
    • C08G16/02C04B26/12C08G14/06C08L61/34
    • Amino-resin products, which include aminoplast foams, can be modified by reacting an aminoplast precondensate, which contains an excess of formaldehyde or to which supplemental formaldehyde or another lower monoaldehyde or dialdehyde has been added before processing, with a hardening agent or with a solution of hardening agent, surfactant, and foamer in the presence of an additive that consists of one or more mononuclear or binuclear phenols, phenolic ethers, or acenaphthene derivatives with the overall formulas ##STR1## in which X is H, OH, SO.sub.3 H, Cl, CH.sub.3, or C.sub.2 H.sub.5 andR is H or an alkyl radical, with 1 to 9 carbon atoms, at a pH between about 1 and 2, mixed if necessary with aromatic sulphonic acids, at a pH between about 1 and 2. The modified products can be employed wherever free formaldehyde is undesirable.
    • 包括氨基塑料泡沫的氨基树脂产物可以通过使含有过量甲醛的氨基塑料预缩合物或在加工前添加了另外的低级单醛或二醛的氨基塑料预缩合物与硬化剂或溶液 硬化剂,表面活性剂和起泡剂在由一种或多种单核或双核酚,酚醚或苊衍生物组成的添加剂的存在下,具有总体配方 ,其中X 是H,OH,SO 3 H,Cl,CH 3或C 2 H 5,R是H或具有1至9个碳原子的烷基,在约1和2之间的pH下,如果需要,与芳族磺酸混合, 约1和2.改性产物可用于不需要游离甲醛的地方。
    • 54. 发明授权
    • Plastic and foam plastic and method for making them
    • 塑料和泡沫塑料及其制造方法
    • US4370424A
    • 1983-01-25
    • US237028
    • 1981-02-23
    • Heinz Baumann
    • Heinz Baumann
    • C08G16/00C08J9/30
    • C08J9/30C08G16/00C08J2361/00
    • Plastics are produced by reacting at least one compound containing sulfonic acid groups with at least one aldehyde in the presence of a hydroxy compound in an acidic concentrated aqueous solution having a water content of about 20 to 30% by weight. If a tenside is present the reactants will form a foam. The preferred sulfonic acid-containing compound is the sodium salt of diisobutylnaphthalene sulfonic acid, the preferred hydroxy compound is a phenol, vix. resorcinol, and the preferred aldehyde is formaldehyde which may be formed in situ from hexamethylenetetramine, paraformaldehyde, trioxane, or the like.
    • 通过使含有磺酸基团的至少一种化合物与至少一种醛在羟基化合物的存在下,在含水量为约20至30重量%的酸性浓缩水溶液中反应制备塑料。 如果存在表面活性剂,反应物将形成泡沫。 优选的含磺酸化合物是二异丁基萘磺酸的钠盐,优选的羟基化合物是苯酚,Vix。 间苯二酚,优选的醛是可以由六亚甲基四胺,多聚甲醛,三恶烷等原位形成的甲醛。