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    • 54. 发明授权
    • Process for bleaching lignocellulosic matter
    • 漂白木质纤维素物质的方法
    • US4812206A
    • 1989-03-14
    • US99762
    • 1987-09-22
    • Michel DevicRobert Angelier
    • Michel DevicRobert Angelier
    • D21C9/00D21B1/16D21C3/22D21C9/02D21C9/10D21C9/16D21C3/26D21C3/00
    • D21C9/1057
    • A process for bleaching a lignocellulosic matter in the form of a mechanical, thermomechanical, chemicomechanical or chemicothermomechanical papermaking pulp, or of wood chips while being converted into one of these pulp types by processing in a machine consisting essentially of two interpenetrating spiral surfaces wound around parallel shafts driven in synchronous rotation in the same direction inside a barrel which encloses them, and determining between upstream and downstream in the direction of forward travel of the matter a series of zones for drawing and braking the matter, which comprises combining a bleaching treatment using a reducing agent and a bleaching treatment using an oxidizing agent, characterized in that, after pretreatment using at least one metal-complexing or sequestering agent, the lignocellulosic matter undergoes a washing operation with an efficiency greater than 96% before undergoing in succession a bleaching treatment using a reducing agent at a pH of between about 8 and 12, a washing operation to remove the reducing agent and a bleaching treatment using an oxidizing agent.
    • 一种在机械,机械机械,化学机械或化学机械造纸纸浆或木屑的形式中漂白木质纤维素物质的方法,同时通过在基本上由围绕平行缠绕的两个互穿螺旋表面的机器中加工而转化成这些纸浆类型之一 在围绕它们的桶内以相同的方向同步旋转驱动的轴,以及在物体的向前行进方向上的上游和下游之间确定一系列用于拉制和制动该物质的区域,其包括将使用 还原剂和使用氧化剂的漂白处理,其特征在于,在使用至少一种金属络合或螯合剂进行预处理之后,所述木质纤维素物质经历洗涤操作,其效率大于96%,然后连续进行漂白处理,使用 在pH之间的还原剂 约8和12,用于除去还原剂的洗涤操作和使用氧化剂的漂白处理。
    • 55. 发明授权
    • Process for the preparation of anthraquinone dispersions and their use
in alkaline wood digestion processes
    • 制备蒽醌分散体的方法及其在碱性木材消化过程中的应用
    • US4717451A
    • 1988-01-05
    • US810405
    • 1985-12-18
    • Michel DevicJean-Pierre Schirmann
    • Michel DevicJean-Pierre Schirmann
    • C07C50/18C07C45/00C07C46/00C07C67/00D21C3/00D21C3/20
    • C07C46/00
    • The process of making a wet or dry dispersion containing anthraquinone suitable for use in the alkaline digestion of wood comprising cyclizing ortho-benzoylbenzoic acid at a temperature of about 150.degree. to 180.degree. C. and at an absolute pressure between about 5 and 40 millibars in the presence of between about 0.05 to 2 parts by weight of sulfuric acid, having a concentration of at least about 95%, per part by weight of ortho-benzoylbenzoic acid to form a reaction mixture containing anthraquinone, bringing the reaction mixture to a pH of at least about 7 by addition thereto at a temperature between about ambient temperature and 100.degree. C. of an aqueous solution of sodium hydroxide or potassium hydroxide containing between about 10% to 40% hydroxide by weight, and then forming a dispersion thereof and using such dispersion in the alkaline digestion of wood.
    • 制备适合用于木材碱性消化的含有蒽醌的湿或干分散体的方法,包括在约150-180℃的温度和绝对压力为约5至40毫巴之间环化邻苯甲酰基苯甲酸, 存在约0.05至2重量份的浓度为至少约95重量%的邻苯甲酰基苯甲酸的至少约95重量%的硫酸,以形成含有蒽醌的反应混合物,使反应混合物的pH为 在大约环境温度和100℃之间的温度下加入至少约7的氢氧化钠或氢氧化钾水溶液,其含有约10重量%至40重量%的氢氧化物,然后形成其分散体,并使用它们 分散在木材的碱性消化中。