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1. 发明授权

US5338402A Process for preparing a bleached chemithermomechanical pulp 失效
标题翻译：制备漂白的机械浆的方法
公开(公告)号：US5338402A
公开(公告)日：1994-08-16
申请号：US957636
申请日：1992-10-06
申请人： Michel Devic , Robert Angelier
发明人： Michel Devic , Robert Angelier
IPC分类号： D21C3/22 , D21C3/14 , D21B1/16 , D21C9/16
CPC分类号： D21C3/222
摘要： A process for preparing chemithermomechanical pulp comprising subjecting a lignocellulosic substance from which said pulp is to be formed to the simultaneous action of a sulfite and a reducing agent that is more electronegative than the sulfite ion during a nondestructive cooking operation at a temperature of about 100.degree. C. or above under saturated steam pressure; said simultaneous action taking place at an initial pH of between 7 and 12.5.
摘要翻译：一种制备切割机械纸浆的方法，包括在约100℃的无损烹饪操作期间使形成所述纸浆的木质纤维素物质与亚硫酸盐和还原剂同时作用，所述亚硫酸盐和还原剂与非亚硝酸根离子相比更具电负性。 C.或以上饱和蒸气压; 所述同时作用发生在初始pH为7至12.5之间。

2. 发明授权

US4812206A Process for bleaching lignocellulosic matter 失效
标题翻译：漂白木质纤维素物质的方法
公开(公告)号：US4812206A
公开(公告)日：1989-03-14
申请号：US99762
申请日：1987-09-22
申请人： Michel Devic , Robert Angelier
发明人： Michel Devic , Robert Angelier
IPC分类号： D21C9/00 , D21B1/16 , D21C3/22 , D21C9/02 , D21C9/10 , D21C9/16 , D21C3/26 , D21C3/00
CPC分类号： D21C9/1057
摘要： A process for bleaching a lignocellulosic matter in the form of a mechanical, thermomechanical, chemicomechanical or chemicothermomechanical papermaking pulp, or of wood chips while being converted into one of these pulp types by processing in a machine consisting essentially of two interpenetrating spiral surfaces wound around parallel shafts driven in synchronous rotation in the same direction inside a barrel which encloses them, and determining between upstream and downstream in the direction of forward travel of the matter a series of zones for drawing and braking the matter, which comprises combining a bleaching treatment using a reducing agent and a bleaching treatment using an oxidizing agent, characterized in that, after pretreatment using at least one metal-complexing or sequestering agent, the lignocellulosic matter undergoes a washing operation with an efficiency greater than 96% before undergoing in succession a bleaching treatment using a reducing agent at a pH of between about 8 and 12, a washing operation to remove the reducing agent and a bleaching treatment using an oxidizing agent.
摘要翻译：一种在机械，机械机械，化学机械或化学机械造纸纸浆或木屑的形式中漂白木质纤维素物质的方法，同时通过在基本上由围绕平行缠绕的两个互穿螺旋表面的机器中加工而转化成这些纸浆类型之一在围绕它们的桶内以相同的方向同步旋转驱动的轴，以及在物体的向前行进方向上的上游和下游之间确定一系列用于拉制和制动该物质的区域，其包括将使用还原剂和使用氧化剂的漂白处理，其特征在于，在使用至少一种金属络合或螯合剂进行预处理之后，所述木质纤维素物质经历洗涤操作，其效率大于96％，然后连续进行漂白处理，使用在pH之间的还原剂约8和12，用于除去还原剂的洗涤操作和使用氧化剂的漂白处理。

3. 发明授权

US08946493B2 Method for producing pentafluoropropane 有权
标题翻译：五氟丙烷的制备方法
公开(公告)号：US08946493B2
公开(公告)日：2015-02-03
申请号：US13377189
申请日：2010-05-06
申请人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini
发明人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini
IPC分类号： C07C17/354 , C07C19/08
CPC分类号： C07C17/354 , Y02P20/582 , C07C19/08
摘要： The present invention relates to a method for producing 1,2,3,3,3-pentafluoropropane, involving reacting gaseous phase 1,2,3,3,3-pentafluoropropene with hydrogen in a superstoichimetric amount in the presence of a hydrogenation catalyst in a reactor, and recirculating a part of the gaseous effluent from the reactor.
摘要翻译：本发明涉及一种制备1,2,3,3,3-五氟丙烷的方法，包括使氢相中的氢化催化剂在超高速度条件下使氢相1,2,3,3,3-五氟丙烯与氢反应反应器，并且将来自反应器的一部分气态流出物再循环。

4. 发明授权

US08841493B2 Process for preparing fluoroolefin compounds 有权
标题翻译：氟烯烃化合物的制备方法
公开(公告)号：US08841493B2
公开(公告)日：2014-09-23
申请号：US13375582
申请日：2010-05-04
申请人： Dominique Guillet , Michel Devic
发明人： Dominique Guillet , Michel Devic
IPC分类号： C07C17/25 , C07C21/18
CPC分类号： C07C17/25 , Y02P20/582 , C07C21/18
摘要： The subject matter of the invention is a process for preparing fluoroolefin compounds. The invention relates more particularly to a process for producing a (hydro)fluoroolefin compound, which comprises (i) bringing at least one compound comprising from three to six carbon atoms, at least two fluorine atoms and at least one hydrogen atom, on the condition that at least one hydrogen atom and one fluorine atom are located on adjacent carbon atoms, into contact with a solid reactant comprising calcium hydroxide.
摘要翻译：本发明的主题是制备氟烯烃化合物的方法。本发明更具体地涉及（氢）氟代烯烃化合物的制备方法，该方法包括（i）在条件下使至少一种包含3至6个碳原子的化合物，至少2个氟原子和至少1个氢原子至少一个氢原子和一个氟原子位于相邻碳原子上，与包含氢氧化钙的固体反应物接触。

5. 发明申请

US20120101314A1 METHOD FOR PRODUCING HEXAFLUOROPROPANE 有权
标题翻译：生产十六烷基磺酸的方法
公开(公告)号：US20120101314A1
公开(公告)日：2012-04-26
申请号：US13377159
申请日：2010-05-05
申请人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini
发明人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini
IPC分类号： C07C17/354
CPC分类号： C07C17/354 , C07C19/08 , C07C21/18 , Y02P20/582
摘要： The present invention relates to a method for producing 1,1,1,2,3,3-hexaafluoropropane, involving reacting gaseous phase hexafluoropropene with hydrogen in a superstoichimetric amount in the presence of a hydrogenation catalyst in a reactor, and recirculating a part of the gaseous effluent from the reactor.
摘要翻译：本发明涉及一种生产1,1,1,2,3,3-六氟丙烷的方法，其包括在反应器中在加氢催化剂存在下使超过一定量的气相六氟丙烯与氢反应，并将一部分来自反应器的气态流出物。

6. 发明申请

US20120083632A1 PROCESS FOR PREPARING FLUOROOLEFIN COMPOUNDS 有权
标题翻译：制备荧光素化合物的方法
公开(公告)号：US20120083632A1
公开(公告)日：2012-04-05
申请号：US13375582
申请日：2010-05-04
申请人： Dominique Guillet , Michel Devic
发明人： Dominique Guillet , Michel Devic
IPC分类号： C07C17/23
CPC分类号： C07C17/25 , Y02P20/582 , C07C21/18
摘要： The subject matter of the invention is a process for preparing fluoroolefin compounds. The invention relates more particularly to a process for producing a (hydro)fluoroolefin compound, which comprises (i) bringing at least one compound comprising from three to six carbon atoms, at least two fluorine atoms and at least one hydrogen atom, on the condition that at least one hydrogen atom and one fluorine atom are located on adjacent carbon atoms, into contact with a solid reactant comprising calcium hydroxide.
摘要翻译：本发明的主题是制备氟烯烃化合物的方法。本发明更具体地涉及（氢）氟代烯烃化合物的制备方法，该方法包括（i）在条件下使至少一种包含3至6个碳原子的化合物，至少2个氟原子和至少1个氢原子至少一个氢原子和一个氟原子位于相邻碳原子上，与包含氢氧化钙的固体反应物接触。

7. 发明申请

US20110160498A1 PROCESS FOR THE PREPARATION OF TRIFLUORINATED AND TETRAFLUORINATED COMPOUNDS 有权
标题翻译：制备三氟化合物和四氢化合物的方法
公开(公告)号：US20110160498A1
公开(公告)日：2011-06-30
申请号：US13063079
申请日：2009-09-11
申请人： Anne Pigamo , Michel Devic , Laurent Wendlinger
发明人： Anne Pigamo , Michel Devic , Laurent Wendlinger
IPC分类号： C07C17/35 , C07C17/354
CPC分类号： C07C21/18 , C07C17/04 , C07C17/087 , C07C17/206 , C07C17/25 , C07C51/12 , C07C19/10
摘要： The subject of the invention is a process for the preparation of 2,3-dichloro-1,1,1-trifluoropropane by chlorination of 3,3,3-trifluoropropene at a pressure greater than 2 bar. Application in the synthesis of 1234yf.
摘要翻译：本发明的主题是通过在大于2巴的压力下氯化3,3,3-三氟丙烯来制备2,3-二氯-1,1,1-三氟丙烷的方法。应用于1234yf的合成。

8. 发明授权

US06554958B1 Process for the delignification and bleaching of chemical paper pulps with hydrogen peroxide and at least one polymer 失效
标题翻译：用过氧化氢和至少一种聚合物进行化学纸浆的脱木质素漂白的方法
公开(公告)号：US06554958B1
公开(公告)日：2003-04-29
申请号：US08840305
申请日：1997-04-11
申请人： Michel Devic
发明人： Michel Devic
IPC分类号： D21C916
CPC分类号： D21C9/163 , D21C9/1036
摘要： A process for the delignification and bleaching of chemical paper pulps comprising one or more stage(s) of treatment with hydrogen peroxide, at a temperature greater than 100° C. and under high pressure, in the presence of a polymer and of a compound A chosen from potassium hydroxide, sodium hydroxide and alkali metal or alkaline-earth metal carbonates.
摘要翻译：化学纸浆的脱木质素和脱色方法，包括在高于100℃和高压下，在聚合物和化合物A存在下，用过氧化氢处理的一个或多个阶段选自氢氧化钾，氢氧化钠和碱金属或碱土金属碳酸盐。

9. 发明授权

US4966984A Process for the cyclization of orthobenzoylbenzoic acid 失效
标题翻译：邻苯甲酰苯甲酸环化方法
公开(公告)号：US4966984A
公开(公告)日：1990-10-30
申请号：US433365
申请日：1989-11-08
申请人： Michel Devic
发明人： Michel Devic
IPC分类号： C07C50/18 , C07C46/00 , C07C51/42 , C07C51/487
CPC分类号： C07C51/42 , C07C51/487
摘要： The process for the cyclization of orthobenzoylbenzoic acid into anthraquinone comprising heating orthobenzoylbenzoic acid in the solid phase at a temperature between about 300.degree. C. to 400.degree. C. in the presence of a superactive bleaching earth. The invention also comprises a process for the separation of phthalic acid and any phthalic anhydride impurities from orthobenzoylbenzoic acid prior to its cyclization into anthraquinone through the use of said earth at a temperature from 200.degree. C. to 250.degree. C.
摘要翻译：将邻苯甲酰苯甲酸环化成蒽醌的方法，包括在超活性漂白土存在下，在约300℃至400℃的温度下，在固相中加热邻苯甲酰苯甲酸。本发明还包括一种将邻苯二甲酸和任何邻苯二甲酸酐杂质从邻苯甲酰基苯甲酸分离出的方法，在通过使用所述土壤在200-250℃的温度环化成蒽醌之前。

10. 发明申请

US20120136183A1 METHOD FOR PREPARING FLUORINE COMPOUNDS 有权
标题翻译：氟化合物的制备方法
公开(公告)号：US20120136183A1
公开(公告)日：2012-05-31
申请号：US13382574
申请日：2010-05-21
申请人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini , Pierre-Marie Sedat , Karine Avril
发明人： Michel Devic , Nicolas Doucet , Laurent Wendlinger , Geraldine Cavallini , Pierre-Marie Sedat , Karine Avril
IPC分类号： C07C17/25 , C07C17/383
CPC分类号： C07C17/25 , C07C17/354 , C07C21/18 , C07C19/08
摘要： The invention relates to a method for preparing fluoropropenes of formula (I) CF3CF═CHR, where R is a hydrogen or a fluorine atom from at least one compound of formula (Ia) CF3CF═CFR, where R has the same meaning as in formula (I), said method including the following steps: (i) hydrogenating at least one compound of formula (Ia) in an adiabatic reactor in the presence of a catalyst with a superstoichiometric amount of hydrogen so as to produce a hydrofluoropropane; (ii) partially condensing the flow from the adiabatic reactor of step (i) so as to produce a gaseous phase fraction, including unreacted hydrogen and a portion of the formed hydrofluoropropane, which is recirculated to step (i), and a liquid phase fraction including the residue of the hydrofluoropropane; (iii) dehydrofluorinating hydrofluoropropane from the liquid fraction of step (ii) using potassium hydroxide in an aqueous reaction medium contained in an agitated reactor so as to produce the fluoropropene of formula (I); and (iv) purifying the fluoropropene obtained in step (iii).
摘要翻译：本发明涉及一种制备式（I）CF 3 CF = CHR的氟丙烯的方法，其中R是至少一种式（Ia）CF 3 CF = CFR的化合物的氢或氟原子，其中R的定义与式（I），所述方法包括以下步骤：（i）在具有超化学计量的氢的催化剂存在下，在绝热反应器中氢化至少一种式（Ia）化合物以产生氢氟丙烷; （ii）部分冷凝来自步骤（i）的绝热反应器的流，以便产生气相馏分，包括未反应的氢气和一部分所形成的氢氟丙烷，其循环至步骤（i），以及液相馏分包括氢氟丙烷的残留物; （iii）使用氢氧化钾在搅拌反应器中的含水反应介质中，从步骤（ii）的液体馏分中脱氢氟化氢氟丙烷，以制备式（I）的氟丙烯; 和（iv）纯化步骤（iii）中获得的氟丙烯。

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