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51. 发明授权

US06890392B2 Nanocomposite magnet and method for producing same 有权
标题翻译：纳米复合磁体及其制造方法
公开(公告)号：US06890392B2
公开(公告)日：2005-05-10
申请号：US10222822
申请日：2002-08-19
申请人： Hirokazu Kanekiyo , Toshio Miyoshi , Satoshi Hirosawa
发明人： Hirokazu Kanekiyo , Toshio Miyoshi , Satoshi Hirosawa
IPC分类号： H01F1/057 , H01F1/058 , H01F1/053
CPC分类号： B82Y25/00 , B22F2009/041 , B22F2998/10 , H01F1/0571 , H01F1/0578 , H01F1/0579 , H01F1/058 , B22F9/008 , B22F9/04 , B22F9/007
摘要： A method of making a material alloy for an iron-based rare earth magnet includes the step of forming a melt of an alloy with a composition of (Fe1-mTm)100-x-y-z-n(B1-pCp)xRyTi2Mn. T is Co and/or Ni; R is at least one element selected from Y (yttrium) and the rare earth elements; and M is at least one element selected from Al, Si, V, Cr, Mn, Ni, Cu, Zn, Ga, Zr, Nb, Mo, Ag, Hf, Ta, W, Pt, Au and Pb, wherein the following inequalities are satisfied: 10
摘要翻译：一种制备铁基稀土磁体的材料合金的方法包括以下组合物形成合金熔体的步骤：（Fe 1-m M t））100-xyzn（B 1-p C p）x x X x X z Ti 2 N n N n。 T是Co和/或Ni; R是选自Y（钇）和稀土元素中的至少一种元素; 并且M是选自Al，Si，V，Cr，Mn，Ni，Cu，Zn，Ga，Zr，Nb，Mo，Ag，Hf，Ta，W，Pt，Au和Pb中的至少一种元素，其中以下满足不等式：10

52. 发明授权

US06878217B2 Rare earth metal-based permanent magnet having corrosion-resistant film and method for producing the same 有权
标题翻译：具有耐腐蚀膜的稀土金属永磁体及其制造方法
公开(公告)号：US06878217B2
公开(公告)日：2005-04-12
申请号：US10265725
申请日：2002-10-08
申请人： Atsushi Kikugawa , Fumiaki Kikui
发明人： Atsushi Kikugawa , Fumiaki Kikui
IPC分类号： H01F41/02 , H01F1/053
CPC分类号： H01F41/026 , Y10S428/90 , Y10T428/12465 , Y10T428/31678
摘要： The chemical conversion film containing, at least as the constituent components thereof, (a) at least one of the metals selected from molybdenum, zirconium, vanadium, and tungsten; (b) a rare earth metal constituting the magnet; and (c) oxygen, which is formed on the surface of a rare earth metal-based permanent magnet according to the present invention, contains a composite metal oxide provided on the surface of the R-rich phase having a lower oxidation-reduction potential through a preferential reaction of the metallic ions that are present in the form of complex ions or oxide ions, such as of molybdenum, contained in the treatment solution, with the rare earth metals that elute from the magnet. Thus formed composite metal oxide reduces the difference in corrosion potential as to realize a uniform surface potential, and effectively suppresses the corrosion based on potential difference. Furthermore, the chemical conversion film thus formed exhibits excellent corrosion resistance even if it is provided as a thin film. The production method thereof can be implemented at low cost and by a simple process comprising treating the surface of the magnet by using a treatment solution containing a molybdate and the like.
摘要翻译：所述化学转化膜至少包含其组成成分，（a）选自钼，锆，钒和钨中的至少一种金属; （b）构成磁体的稀土金属; 和（c）在根据本发明的稀土金属基永磁体的表面上形成的氧含有在富氧相的表面上提供的复合金属氧化物，其具有较低的氧化还原电位通过存在于处理溶液中所含的复合离子或氧化物离子（例如钼）形式的金属离子与从磁体洗脱的稀土金属的优先反应。如此形成的复合金属氧化物减少了腐蚀电位的差异，以实现均匀的表面电位，并且有效地抑制了基于电位差的腐蚀。此外，即使设置为薄膜，这样形成的化学转化膜也具有优异的耐腐蚀性。其制造方法可以低成本地实施，并且可以通过使用含有钼酸盐等的处理溶液处理磁体表面的简单方法来实现。

53. 发明授权

US07344606B2 Permanent magnet manufacturing method and press apparatus 失效
标题翻译：永磁体制造方法和压制装置
公开(公告)号：US07344606B2
公开(公告)日：2008-03-18
申请号：US10489339
申请日：2002-10-18
申请人： Shuji Mino , Noboru Nakamoto
发明人： Shuji Mino , Noboru Nakamoto
IPC分类号： H01F1/04
CPC分类号： H01F41/0266 , H01F1/0573 , H01F41/0273
摘要： An anisotropic bonded magnet is produced at a low cost by avoiding various problems caused by remanence. Also, the unit weight and density of a compact is increased by filling even a cavity, having no easily feedable shape, with a magnet powder just as intended. An anisotropic bonded magnet is produced by feeding the cavity of a press machine with a magnetic powder (e.g., an HDDR powder) and compacting it. After the magnetic powder has been positioned outside of the cavity, an oscillating magnetic field (e.g., an alternating magnetic field) is created in a space including the cavity. The magnetic powder is transported into the cavity while being aligned parallel to the oscillating direction of the oscillating magnetic field. Thereafter, the magnetic powder is compressed within the cavity to make a compact for an anisotropic bonded magnet.
摘要翻译：通过避免由剩磁引起的各种问题，以低成本制造各向异性粘结磁体。此外，通过根据需要用磁铁粉末填充甚至没有容易进给的形状的空腔来增加压块的单位重量和密度。各向异性粘结磁体通过向压机的型腔供给磁性粉末（例如，HDDR粉末）并压实而制造。在磁粉被定位在空腔外部之后，在包括空腔的空间中产生振荡磁场（例如，交变磁场）。磁性粉末在平行于振荡磁场的振荡方向对准的同时被输送到空腔中。此后，磁性粉末在空腔内被压缩以使各向异性粘结磁体成形。

54. 发明申请

US20070269679A1 Method for Producing Rare Earth Metal-Based Permanent Magnet Having Copper Plating Film on the Surface Thereof 有权
标题翻译：用于生产表面具有镀铜膜的稀土金属基永久磁铁的方法
公开(公告)号：US20070269679A1
公开(公告)日：2007-11-22
申请号：US11659849
申请日：2005-08-09
申请人： Toshinobu Niinae
发明人： Toshinobu Niinae
IPC分类号： C25D3/58 , B32B15/00 , B32B15/20
CPC分类号： H01F41/026 , C25D3/38 , C25D7/001 , H01F1/0577 , Y10T428/12903
摘要： [Problems] To provide a method for producing a rare earth metal-based permanent magnet having on the surface thereof a copper plating film by using a novel plating solution for use in a copper electroplating treatment capable of forming a copper plating film having excellent adhesiveness on the surface of a rare earth metal-based permanent magnet. [Means for Resolution] The method for producing a rare earth metal-based permanent magnet having a copper plating film on the surface thereof according to the invention is characterized in that it comprises forming a copper plating film on the surface of a rare earth metal-based permanent magnet by means of a copper electroplating treatment by using a plating solution having its pH adjusted to a range from 9.0 to 11.5 and containing at least the following three components: (1) Cu2+ ions, (2) a chelating agent having a chelate stability constant of 10.0 or higher for Cu2+ ions, and (3) a chelating agent having a chelate stability constant of 16.0 or higher for Fe3+ ions (where, the aforementioned chelate stability constants are confined to conditions of pH 9.0 to 11.5).
摘要翻译： [问题]提供一种稀土类金属系永久磁铁的制造方法，该稀土类金属系永久磁铁的表面具有使用能够形成具有优异粘合性的镀铜膜的铜电镀处理用新型电镀液的铜镀膜稀土金属基永磁体的表面。 [解决方法]根据本发明的在其表面上具有镀铜膜的稀土金属基永磁体的制造方法的特征在于，其包括在稀土金属基永久磁铁的表面上形成镀铜膜，通过使用其pH调节至9.0〜11.5的范围的电镀液，并且至少包含以下三种成分，通过铜电镀处理进行铜基永久磁铁的处理：（1）Cu 2+离子，（2）螯合稳定常数为10.0以上的Cu 2+离子螯合剂，（3）Fe 3+螯合稳定性常数为16.0以上的螯合剂 +离子（其中上述螯合稳定常数限于pH 9.0〜11.5的条件）。

55. 发明申请

US20070199623A1 R-Fe-B Based Thin Film Magnet And Method For Preparation Thereof 有权
标题翻译： R-Fe-B型薄膜磁铁及其制备方法
公开(公告)号：US20070199623A1
公开(公告)日：2007-08-30
申请号：US10593624
申请日：2005-03-23
申请人： Shunji Suzuki , Kenichi Machida , Eiji Sakaguchi , Kazuya Nakamura
发明人： Shunji Suzuki , Kenichi Machida , Eiji Sakaguchi , Kazuya Nakamura
IPC分类号： B32B15/00 , H01F1/057
CPC分类号： H01F41/22 , H01F1/057 , H01F10/126 , H01F41/0253 , H01F41/0293 , Y10T428/32 , Y10T428/325
摘要： An R—Fe—B based thin film magnet including an R—Fe—B based alloy which contains 28 to 45 percent by mass of R element (where R represents at least one type of rare-earth lanthanide elements) and which is physically formed into a film, wherein the R—Fe—B based alloy has a composite texture composed of R2Fe14B crystals having a crystal grain diameter of 0.5 to 30 μm and R-element-rich grain boundary phases present at boundaries between the crystals. The magnetization characteristics of the thin film magnet are improved. The R—Fe—B based thin film magnet can be prepared by heating to 700° C. to 1,200° C. during physical film formation or/and the following heat treatment, so as to grow crystal grains and form R-element-rich grain boundary phases.
摘要翻译：包含R-Fe-B系合金的R-Fe-B类薄膜磁体，其含有28〜45质量％的R元素（其中R表示至少一种稀土镧系元素），并且其物理形成其中R-Fe-B基合金具有由晶体直径为0.5至30μm的R 2 Fe 14 N 12 B晶体组成的复合纹理，以及存在于晶体之间的边界处的富含R元素的晶界相。提高了薄膜磁铁的磁化特性。 R-Fe-B类薄膜磁体可以在物理成膜或/和随后的热处理中加热至700℃至1200℃，从而生长晶粒并形成富含R元素的薄膜晶界相。

56. 发明申请

US20070131309A1 Nano-composite magnet, quenched alloy for nano-composite magnet, and method for producing them and method for distinguishing them 审中-公开
标题翻译：纳米复合磁体，纳米复合磁体淬火合金及其制造方法和区别它们的方法
公开(公告)号：US20070131309A1
公开(公告)日：2007-06-14
申请号：US10596371
申请日：2004-12-06
申请人： Yasutaka Shigemoto , Satoshi Hirosawa , Toshio Miyoshi
发明人： Yasutaka Shigemoto , Satoshi Hirosawa , Toshio Miyoshi
IPC分类号： H01F1/057
CPC分类号： B82Y25/00 , B22D11/0611 , H01F1/0579 , H01F1/058 , H01F41/0253
摘要： A nanocomposite magnet according to the present invention has a composition represented by the general formula: RxQyMz(Fe1−mTm)bal, where R is at least one rare-earth element, Q is at least one element selected from the group consisting of B and C, M is at least one metal element that is selected from the group consisting of Al, Si, Ti, V, Cr, Mn, Cu, Zn, Ga, Zr, Nb, Mo, Ag, Hf, Ta, W, Pt, Au and Pb and that always includes Ti, and T is at least one element selected from the group consisting of Co and Ni. The mole fractions x, y, z and m satisfy the inequalities of 6 at % ≦x
摘要翻译：根据本发明的纳米复合材料磁体具有由以下通式表示的组成：R 1，X 3，M z（Fe 1）其中R是至少一种稀土元素，Q是选自B和B中的至少一种元素，其中R是至少一个稀土元素， C，M是选自Al，Si，Ti，V，Cr，Mn，Cu，Zn，Ga，Zr，Nb，Mo，Ag，Hf，Ta，W，Pt中的至少一种金属元素，Au和Pb，并且总是包括Ti，T是选自Co和Ni中的至少一种元素。摩尔分数x，y，z和m满足不等式6 at％<= x <10 at％，10 at％<= y <= 17 at％，0.5 at％<= z <= 6 at％和0 <= m <= 0.5。纳米复合磁体包括磁耦合在一起的硬磁相和软磁相。硬磁相由R 2 Fe 14 B型化合物制成，软磁相包括α-Fe相和具有居里温度的结晶相以610℃至700℃（ω相）为主要相。

57. 发明授权

US07217328B2 Compound for rare-earth bonded magnet and bonded magnet using the compound 有权
标题翻译：使用该化合物的稀土粘结磁体和粘结磁体的化合物
公开(公告)号：US07217328B2
公开(公告)日：2007-05-15
申请号：US10642324
申请日：2003-08-18
申请人： Takeshi Nishiuchi , Hirokazu Kanekiyo , Satoshi Hirosawa , Toshio Miyoshi
发明人： Takeshi Nishiuchi , Hirokazu Kanekiyo , Satoshi Hirosawa , Toshio Miyoshi
IPC分类号： H01F1/053 , H01F1/057
CPC分类号： B82Y25/00 , B22F2998/10 , C22C1/0441 , H01F1/0578 , H01F1/0579 , B22F9/008 , B22F9/04 , B22F9/007
摘要： A compound for a rare-earth bonded magnet includes a rare-earth alloy powder and a binder. The rare-earth alloy powder includes at least about 2 mass % of Ti-containing nanocomposite magnet powder particles with a composition represented by (Fe1-mTm)100-x-y-zQxRyMz, where T is Co and/or Ni; Q is B with or without C; R is at least one rare-earth element substantially excluding La and Ce; M is at least one metal element selected from Ti, Zr and Hf and always includes Ti; and 10
摘要翻译：稀土类粘结磁铁用复合体包括稀土类合金粉末和粘合剂。所述稀土类合金粉末至少含有2质量％以下的含Ti的纳米复合磁体粉末颗粒，其组成由（Fe 1-m M m） > 100-xyz其中T是Co和/或Ni;其中T是Co和/或Ni; Q是带有或不带C的B; R是至少一种基本上不含La和Ce的稀土元素; M是选自Ti，Zr和Hf中的至少一种金属元素，并且总是包括Ti; 和10

58. 发明授权

US07214343B2 Method for producing granulated powder of R—FE—B type alloy and method for producing R—FE—B type alloy sintered compact 有权
标题翻译：制造R-FE-B型合金粉粒的方法及R-FE-B型合金烧结体的制造方法
公开(公告)号：US07214343B2
公开(公告)日：2007-05-08
申请号：US10473335
申请日：2002-03-27
申请人： Futoshi Kuniyoshi , Yuji Kaneko , Akihito Tsujimoto , Kazunari Shimauchi , Kazuo Tanaka , Shizuo Mori , Kiyofumi Suzuki
发明人： Futoshi Kuniyoshi , Yuji Kaneko , Akihito Tsujimoto , Kazunari Shimauchi , Kazuo Tanaka , Shizuo Mori , Kiyofumi Suzuki
IPC分类号： B22F9/04
CPC分类号： B22F1/0059 , B22F1/0096 , B22F2998/10 , B22F2999/00 , C22C1/0441 , H01F1/0571 , H01F1/0577 , H01F1/0578 , B22F3/02 , B22F3/1021 , B22F2202/05
摘要： The method for producing a granulated powder of the present invention includes the steps of: preparing an R—Fe—B alloy powder; and granulating the alloy powder using at least one kind of granulating agent selected from normal paraffins, isoparaffins and depolymerized oligomers, to prepare a granulated powder. The produced R—Fe—B alloy granulated powder is excellent in flowability and compactibility as well as in binder removability.
摘要翻译：本发明的造粒粉末的制造方法包括以下步骤：制备R-Fe-B合金粉末; 并使用选自正链烷烃，异链烷烃和解聚低聚物中的至少一种造粒剂造粒合金粉末，制备造粒粉末。生产的R-Fe-B合金造粒粉末的流动性和紧实性以及粘合剂的去除性都优异。

59. 发明授权

US07201810B2 Rare earth alloy sintered compact and method of making the same 有权
标题翻译：稀土合金烧结体及其制造方法
公开(公告)号：US07201810B2
公开(公告)日：2007-04-10
申请号：US10381008
申请日：2002-03-29
申请人： Hitoshi Morimoto , Yuji Kaneko
发明人： Hitoshi Morimoto , Yuji Kaneko
IPC分类号： H01F1/057
CPC分类号： H01F1/058 , B22F1/0003 , B22F2998/10 , C22C1/0441 , H01F1/0571 , H01F1/0577 , H01F41/0293 , B22F3/1017 , B22F3/10
摘要： A rare earth alloy sintered compact includes a main phase represented by (LR1-xHRx)2T14A, where T is Fe with or without non-Fe transition metal element(s); A is boron with or without carbon; LR is a light rare earth element; HR is a heavy rare earth element; and 0
摘要翻译：稀土合金烧结体包括由（LR×1-x×××××××××××××××××××××××××× A，其中T是具有或不具有非Fe过渡金属元素的Fe; A是具有或不具有碳的硼; LR是轻稀土元素; HR是重稀土元素; 0 T>>>>>>，，，，，，，，，，，，，，，。。。。。。。。。。。。。。。合金材料包括由（LR 1-u u）））））/ / / / / / / / / / / include include include include include include include include include include include include include SUB> A（其中0 <= mu＆amp; X）和（LR 1-v H 2 H 2）2＆lt; 14＆lt; SUB> A（其中x

60. 发明授权

US07169319B2 Anisotropic, sintered ferrite magnet and method for producing the same 有权
标题翻译：各向异性烧结铁氧体磁体及其制造方法
公开(公告)号：US07169319B2
公开(公告)日：2007-01-30
申请号：US10963832
申请日：2004-10-14
申请人： Takashi Takami , Yutaka Kubota , Yasunobu Ogata
发明人： Takashi Takami , Yutaka Kubota , Yasunobu Ogata
IPC分类号： H01F1/00 , C04B35/40 , C04B35/64
CPC分类号： C04B35/2641 , C01G49/0018 , C01P2006/42 , C04B35/2633 , C04B35/62685 , C04B35/63 , C04B35/6303 , C04B35/632 , C04B2235/3208 , C04B2235/3213 , C04B2235/3215 , C04B2235/3217 , C04B2235/3224 , C04B2235/3225 , C04B2235/3227 , C04B2235/3229 , C04B2235/3232 , C04B2235/3239 , C04B2235/3241 , C04B2235/3262 , C04B2235/3272 , C04B2235/3274 , C04B2235/3275 , C04B2235/3277 , C04B2235/3279 , C04B2235/3281 , C04B2235/3284 , C04B2235/3418 , C04B2235/5436 , C04B2235/605 , C04B2235/656 , C04B2235/767 , C04B2235/85 , C04B2235/9615 , H01F1/086 , H01F1/11 , H01F41/0273
摘要： A ferrite magnet having a basic composition represented by the following general formula: (A1−xRx)O.n[(Fe1−yMy)2O3] by atomic ratio, wherein A is Sr and/or Ba, R is at least one of rare earth elements including Y, M is at least one element selected from the group consisting of Co, Mn, Ni and Zn, and x, y and n are numbers meeting the conditions of 0.01≦x≦0.4, [x/(2.6n)]≦y≦[x/(1.6n)], and 5≦n≦6, and substantially having a magnetoplumbite-type crystal structure, is obtained by uniformly mixing a compound of Sr and/or Ba with an iron compound; calcining the resultant uniform mixture; adding a compound of the R element and/or the M element to the resultant calcined powder at a pulverization step thereof; and sintering the resultant mixture. The compound of the R element and/or the M element may be added at a percentage of more than 0 atomic % and 80 atomic % or less, on an element basis, at a mixing step before calcination.
摘要翻译：具有由以下通式表示的碱性组成的铁氧体磁体：（A 1-x R x X）在[（Fe 1-y）其中A是Sr和/或Ba，R是稀土元素中的至少一种，其中A是Sr和/或Ba，R是至少一种稀土元素包括Y，M是选自Co，Mn，Ni和Zn中的至少一种元素，x，y和n是满足条件为0.01 <= x <= 0.4，[x /（2.6n）通过将Sr和/或Ba的化合物与铁均匀混合，得到基本上具有磁铅矿型晶体结构的5 <= n <= 6，并且5 <= n < 复合; 煅烧所得的均匀混合物; 在其粉碎步骤中向所得煅烧粉末中加入R元素和/或M元素的化合物; 并烧结所得混合物。 R元素和/或M元素的化合物可以在煅烧之前的混合步骤中以元素为基准以大于0原子％和80原子％或更少的百分比加入。

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