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    • 41. 发明授权
    • Amorphous precipitated siliceous pigments and improved process for
producing such pigments
    • 无定形沉淀硅质颜料和改进的制备这种颜料的方法
    • US3960586A
    • 1976-06-01
    • US402928
    • 1973-10-03
    • Satish K. Wason
    • Satish K. Wason
    • C01B33/187A61K8/00A61K8/25A61Q11/00C09C1/00C09C1/28C09C1/30
    • A61K8/25A61Q11/00C09C1/30C01P2002/02C01P2004/50C01P2004/51C01P2004/61C01P2004/62C01P2006/10C01P2006/12C01P2006/19C01P2006/82C01P2006/90
    • A process for producing precipitated silicic acid pigments having new and improved properties is disclosed. The pigments are produced by the simultaneous introduction of a solution of an alkali metal silicate and an acid, such as sulfuric acid, into an aqueous receiving medium which contains a salt or electrolyte. The pH of the aqueous receiving medium is adjusted prior to the introduction of the acid and silicate so that it is the same or equal to that pH at which the precipitation of the pigment is effected. The electrolyte is preferably a metal salt of the acid used for acidulation of the silicate. The acid and silicate are added to the receiving medium at a rate such that the precipitating pH is maintained constant. The products of the invention are characterized by their high abrasiveness and have a relative cleaning ability or scale (RCS) equivalent to high grade phosphates used as polishing agents in toothpastes and a superior fluoride compatibility to that of said phosphates. The silicates used in the process are preferably those which are partially polymerized and have an SiO.sub.2 /Na.sub.2 O ratio of at least 2.0.
    • 公开了一种具有新颖性和改进性能的沉淀硅酸颜料的制备方法。 颜料通过将碱金属硅酸盐和酸如硫酸的溶液同时引入含有盐或电解质的含水接收介质来制备。 在引入酸和硅酸盐之前调节含水接收介质的pH,使其与实现颜料沉淀的pH相同或相等。 电解质优选是用于酸化硅酸盐的酸的金属盐。 将酸和硅酸盐以使得沉淀pH保持恒定的速率加入到接收介质中。 本发明的产品的特征在于它们的高磨损性,并且具有与用于牙膏中抛光剂的高级磷酸盐相当的相对清洁能力或比例尺(RCS),并且与所述磷酸盐的氟化物相容性优异。 该方法中使用的硅酸盐优选是部分聚合并且具有至少2.0的SiO 2 / Na 2 O比的那些。