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41. 发明授权

US07781606B2 Blocked mercaptosilane coupling agents, process for making and uses in rubber 有权
标题翻译：封闭的巯基硅烷偶联剂，橡胶制造和使用过程
公开(公告)号：US07781606B2
公开(公告)日：2010-08-24
申请号：US11647780
申请日：2006-12-28
申请人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Tiberiu L. Simandan , Prashant Joshi
发明人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Tiberiu L. Simandan , Prashant Joshi
IPC分类号： C07F7/04
CPC分类号： C08K5/548 , C07F7/1804 , Y02T10/862 , C08L21/00
摘要： The invention relates to sulfur silane coupling agents containing multiple blocked mercapto groups which are in a state of reduced activity until activated. The coupling agents are advantageously used in rubber formulations, for example, for fabricating tires with low rolling resistance.
摘要翻译：本发明涉及含有多个封闭的巯基的硫硅烷偶联剂，它们在活化之前处于活性降低的状态。偶联剂有利地用于橡胶制剂中，例如用于制造具有低滚动阻力的轮胎。

42. 发明授权

US07629430B2 Hybrid silicon-containing coupling agents for filled elastomer compositions 有权
标题翻译：用于填充弹性体组合物的混合含硅偶联剂
公开(公告)号：US07629430B2
公开(公告)日：2009-12-08
申请号：US11640736
申请日：2006-12-18
申请人： Richard W. Cruse
发明人： Richard W. Cruse
IPC分类号： C08G77/28
CPC分类号： C08K5/5415 , B60C1/00 , C07F7/045 , C07F7/1804 , C08K5/48 , C08K5/549 , C08L21/00
摘要： This invention describes novel chemical compounds whose structures are hybrids between sulfur-containing and non-sulfur-containing silanes wherein the two types of silanes are linked by siloxane bonds. The invention includes methods of preparation for the hybrid silanes as well as their use in filled rubbers as coupling agents. The hybrid silanes described are unique in that a certain amount of water in their preparation leads to superior performance in their intended application, and that they can thus be produced more efficiently and safely than coupling agents currently used in the art, from readily available hydrated raw materials.
摘要翻译：本发明描述了新型化合物，其结构是含硫和不含硫的硅烷之间的杂化物，其中两种类型的硅烷通过硅氧烷键连接。本发明包括制备混合硅烷的方法以及它们在填充橡胶中作为偶联剂的用途。所描述的混合硅烷是独特的，因为其制备中的一定量的水导致其预期应用中的优异性能，因此可以比现有技术中所用的偶联剂从易得的水合原料材料

43. 发明授权

US07550524B2 Elastomer composition containing mercaptofunctional silane and process for making same 有权
标题翻译：含有巯基官能团硅烷的弹性体组合物及其制备方法
公开(公告)号：US07550524B2
公开(公告)日：2009-06-23
申请号：US11544142
申请日：2006-10-06
申请人： Antonio Chaves , Eric Raymond Pohl , Richard W. Cruse , Daniel Gurovich
发明人： Antonio Chaves , Eric Raymond Pohl , Richard W. Cruse , Daniel Gurovich
IPC分类号： B60C1/00
CPC分类号： B60C1/0016 , C08K5/548 , C08K5/549 , C08L21/00
摘要： A filled elastomer composition comprises: a) at least one rubber component; b) at least one particulate filler; and, c) at least one mercaptofunctional silane of a particular structure.
摘要翻译：填充的弹性体组合物包含：a）至少一种橡胶组分; b）至少一种颗粒填料; 和c）至少一种具有特定结构的巯基官能的硅烷。

44. 发明申请

US20080161590A1 Blocked mercaptosilane coupling agents, process for making and uses in rubber 有权
标题翻译：封闭的巯基硅烷偶联剂，橡胶制造和使用过程
公开(公告)号：US20080161590A1
公开(公告)日：2008-07-03
申请号：US11647780
申请日：2006-12-28
申请人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Tiberiu L. Simandan , Prashant Joshi
发明人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Tiberiu L. Simandan , Prashant Joshi
IPC分类号： C07F7/08
CPC分类号： C08K5/548 , C07F7/1804 , Y02T10/862 , C08L21/00
摘要： The invention relates to sulfur silane coupling agents containing multiple blocked mercapto groups which are in a state of reduced activity until activated. The coupling agents are advantageously used in rubber formulations, for example, for fabricating tires with low rolling resistance.
摘要翻译：本发明涉及含有多个封闭的巯基的硫硅烷偶联剂，它们在活化之前处于活性降低的状态。偶联剂有利地用于橡胶制剂中，例如用于制造具有低滚动阻力的轮胎。

45. 发明申请

US20080161461A1 Free-flowing filler composition and rubber composition containing same 有权
标题翻译：自由流动的填料组合物和含有它的橡胶组合物
公开(公告)号：US20080161461A1
公开(公告)日：2008-07-03
申请号：US11648460
申请日：2006-12-28
申请人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Prashant Joshi
发明人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Prashant Joshi
IPC分类号： B60C1/00
CPC分类号： C08K5/548 , C08G75/14 , C08K3/04 , C08K3/36 , C08K5/372 , C08K5/5419 , C08L21/00 , C08L81/04 , Y02T10/862
摘要： This invention relates to novel free-flowing filler compositions containing sulfur-containing silane coupling agents, and to a rubber containing the filler composition.
摘要翻译：本发明涉及含有含硫硅烷偶联剂的新型自由流动填料组合物和含有填料组合物的橡胶。

46. 发明申请

US20080083350A1 Mercaptofunctional silane and process for its preparation 有权
公开(公告)号：US20080083350A1
公开(公告)日：2008-04-10
申请号：US11544132
申请日：2006-10-06
申请人： Antonio Chaves , Eric Raymond Pohl , Richard W. Cruse
发明人： Antonio Chaves , Eric Raymond Pohl , Richard W. Cruse
IPC分类号： C07F7/08 , C09C1/28
CPC分类号： C08K5/549 , C07F7/1804 , C08K5/548 , C08L21/00
摘要： A mercaptofunctional silane is provided of general Formula (1): [HSG1SiZθZβ]m[HSG2SiZβ3]n[HSG3SiZβ2X]o[[HSG4SiZβX2]p (1) wherein: each occurrence of G1, G2, G3, and G4 is independently a hydrocarbylene group containing from 1 to 30 carbon derived by substitution of a hydrogen on alkyl, alkenyl, aryl, or aralkyl or a divalent heterocarbon group containing 2 to 30 carbon atoms and one or more etheric oxygen (—O—) and/or sulfur (—S—) atoms; each occurrence of X is independently selected from the group consisting of —Cl, —Br, RO—, RC(—O)O—, R2C═NO—, R2NO—, —R, (HO)d-1G5O—, wherein each R is independently selected from the group consisting of hydrogen, straight, cyclic or branched alkyl that can or can not contain unsaturation, alkenyl groups, aryl groups, and aralkyl groups, wherein each R, other than hydrogen, contains from 1 to 18 carbon atoms, G5 is independently a substituted hydrocarbon group from 2 to 15 carbon atoms or a substituted heterocarbon group from about 4 to 15 carbon atoms and contains one or more etheric oxygen atoms; each occurrence of Zβ, which forms a bridging structure between two silicon atoms, is [—OG5(OH)d-2O—]0.5, wherein each occurrence of G5 is independently selected form the group consisting of a hydrocarbylene group of from 2 to 15 carbon atoms or a divalent heterocarbon group of from 4 to 15 carbon atoms containing one or more etheric oxygen atoms; each occurrence of Zθ, which forms a cyclic structure with a silicon atom, is independently given by —OG5(OH)d-2O—, wherein G5 is independently selected form the group consisting of a hydrocarbylene group of from 2 to 15 carbon atoms or a divalent heterocarbon group of from 4 to 15 carbon atoms containing one or more etheric oxygen atoms; and, each occurrence of subscripts d, m, n, o and p independently is an integer wherein d is from 2 to 6 in a first embodiment, 2 or 3 in a second embodiment and 2 in a third embodiment; m is 0 to 20; n is 0 to 18; o is 0 to 20; and, p is 0 to 20; with the proviso that m+n+o+p is equal to or greater than 2.

47. 发明授权

US06683135B2 Blocked mercaptosilane coupling agents for filled rubbers 有权
标题翻译：用于填充橡胶的封闭的巯基硅烷偶联剂
公开(公告)号：US06683135B2
公开(公告)日：2004-01-27
申请号：US09986511
申请日：2001-11-09
申请人： Richard W. Cruse , Robert J. Pickwell , Keith J. Weller , Eric R Pohl
发明人： Richard W. Cruse , Robert J. Pickwell , Keith J. Weller , Eric R Pohl
IPC分类号： C08C1920
CPC分类号： C07F9/4075 , C07F7/1804 , C07F9/1651 , C08J3/203 , C08J2321/00 , C08K3/013 , C08K3/36 , C08K5/0025 , C08K5/5406 , C08K5/548 , C08L9/00 , C08L9/06 , C08L21/00 , C08L2666/08
摘要： Disclosed herein is a rubber composition comprising: a) a blocked mercaptosilane of a defined structure, wherein the blocking group contains an unsaturated heteroatom or carbon chemically bound directly to sulfur via a single bond and, optionally, may be substituted with one or more carboxylate ester or carboxylic acid functional groups; b) an organic polymer; c) a filler; and d) a deblocking agent.
摘要翻译：本文公开了一种橡胶组合物，其包含：a）具有限定结构的封端巯基硅烷，其中所述封闭基团含有不饱和杂原子或通过单键与硫直接化学键合的碳，并且任选地可被一个或多个羧酸酯或羧酸官能团; b）有机聚合物; c）填料; andd）一种去块剂。

48. 发明授权

US09932437B2 Moisture curable silylated polymer compositions containing reactive modifiers 有权
公开(公告)号：US09932437B2
公开(公告)日：2018-04-03
申请号：US13608142
申请日：2012-09-10
申请人： Misty Huang , Richard W. Cruse , Benjamin Falk , Eric Pohl , Shiu-Chin Su , Jeries Nesheiwat , Philbert Ramdatt , Thomas Fay-Oy Lim , Vikram Kumar
发明人： Misty Huang , Richard W. Cruse , Benjamin Falk , Eric Pohl , Shiu-Chin Su , Jeries Nesheiwat , Philbert Ramdatt , Thomas Fay-Oy Lim , Vikram Kumar
IPC分类号： C08G18/83 , C09J175/04 , C08G18/10 , C08G18/28 , C09J201/10 , C09D201/10 , C08K5/541 , C08K5/544 , C08K5/548
CPC分类号： C08G18/837 , C08G18/10 , C08G18/289 , C08G2170/20 , C08K5/541 , C08K5/544 , C08K5/548 , C09D201/10 , C09J175/04 , C09J201/10 , C08G18/718 , C08L101/10
摘要： Moisture-curable resin compositions comprising (a) a moisture-curable polymer having at least one hydrolysable silyl group; (b) a reactive modifier; (c) a catalyst for catalyzing the reaction between the moisture-curable polymer (a) and reactive modifier (b) under curing conditions; and cured compositions produced by contacting such resin compositions with water are disclosed. The moisture-curable resin composition is useful in the production of adhesives, including hot melt adhesives, primers, sealants, and coatings.

49. 发明授权

US08829257B2 Trivinylcyclohexane stereoisomeric compositions and methods for preparing same 有权
标题翻译：三乙烯基环己烷立体异构体组合物及其制备方法
公开(公告)号：US08829257B2
公开(公告)日：2014-09-09
申请号：US13547703
申请日：2012-07-12
申请人： Richard W. Cruse , Vivek Khare , Jozef Kowalski , Wlodzimierz Stanczyk
发明人： Richard W. Cruse , Vivek Khare , Jozef Kowalski , Wlodzimierz Stanczyk
IPC分类号： C07C5/29 , C07C13/19 , C07C5/22
CPC分类号： C07C5/22 , C07B2200/07 , C07C5/29 , C07C2601/14 , C07C13/19
摘要： Disclosed herein is a process for making 1,2,4-trivinylcyclohexane that is enriched in a particular geometric isomer. The process involves the thermal isomerization of 1,5,9-cyclododecatriene at temperature between 400° C. and 600° C. followed by an equilibration of the resultant intermediate in either the gas phase or liquid phase at temperature between 180° C. and 375° C. and at pressures ranging from 0.101 kPa to 1,013 kPa. Also disclosed are 1,2,4-trivinylcyclohexane compositions that are enriched in a particular geometric isomer.
摘要翻译：本文公开了一种制备富含特定几何异构体的1,2,4-三乙烯基环己烷的方法。该方法涉及在400℃和600℃之间的温度下1,5,9-环十二碳三烯的热异构化，然后在180℃和180℃之间的温度下在气相或液相中平衡所得中间体 375℃，压力范围为0.101kPa至1,013kPa。还公开了富含特定几何异构体的1,2,4-三乙烯基环己烷组合物。

50. 发明授权

US08501849B2 Silated core polysulfides, their preparation and use in filled elastomer compositions 有权
标题翻译：硅酸盐核心多硫化物，其制备和用于填充弹性体组合物
公开(公告)号：US08501849B2
公开(公告)日：2013-08-06
申请号：US13458100
申请日：2012-04-27
申请人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Prashant Joshi
发明人： Richard W. Cruse , W. Michael York , Eric R. Pohl , Antonio Chaves , Prashant Joshi
IPC分类号： B60C1/00 , C08K5/24 , C08K3/34 , C08K3/04
CPC分类号： C08K5/548 , C07F7/1804 , C08L21/00
摘要： This invention relates to novel sulfur-containing silane coupling agents, and organic polymers containing carbon-carbon double bonds. These novel silanes can be carried on organic and inorganic fillers. The invention also relates to articles of manufacture, particularly tires, made from the elastomer compositions described herein.
摘要翻译：本发明涉及新型含硫硅烷偶联剂和含有碳 - 碳双键的有机聚合物。这些新型硅烷可以带有机和无机填料。本发明还涉及由本文所述的弹性体组合物制成的制品，特别是轮胎。

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