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41. 发明申请

US20080242886A1 Continuous Method for the Production of Linear Pentene Nitriles 有权
标题翻译：线性戊烯腈生产的连续方法
公开(公告)号：US20080242886A1
公开(公告)日：2008-10-02
申请号：US10587028
申请日：2005-01-27
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Jens Scheidel , Tim Jungkamp , Hermann Luyken
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Jens Scheidel , Tim Jungkamp , Hermann Luyken
IPC分类号： C07C253/10
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for continuously hydrocyanating 1,3-butadiene in the presence of at least one nickel(0) catalyst with chelate ligands, wherein 1,3-butadiene and hydrogen cyanide are used in a molar ratio of from 1.6:1 to 1.1:1.
摘要翻译：描述了在至少一种具有螯合配体的镍（O）催化剂的存在下连续氢氰化1,3-丁二烯的方法，其中使用1,3-丁二烯和氰化氢，摩尔比为1.6:1至1.1 ：1。

42. 发明申请

US20050207968A1 Process for removing water from a mixture containing water and zinc chloride 失效
标题翻译：从含水和氯化锌的混合物中除去水的方法
公开(公告)号：US20050207968A1
公开(公告)日：2005-09-22
申请号：US10519513
申请日：2003-07-04
申请人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
发明人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
IPC分类号： B01D3/36 , C01G9/04 , F26B5/00 , F26B7/00 , C01B9/00
CPC分类号： C01G9/04 , B01D3/36 , F26B5/005 , F26B7/00
摘要： A process for the removal of water from a mixture comprising water and zinc chloride, which comprises adding to said mixture comprising water and zinc chloride an aprotic, polar diluent whose boiling point in the case where an azeotrope is not formed between said diluent and water under the pressure conditions of the distillation mentioned below is higher than the boiling point of water and which is in liquid form at this boiling point of water or which forms an azeotrope or heteroazeotrope with water under the pressure and temperature conditions of the distillation mentioned below, and distilling the mixture comprising water, zinc chloride and the diluent with removal of water or said azeotrope or said heteroazeotrope from this mixture, giving an anhydrous mixture comprising zinc chloride and said diluent.
摘要翻译：一种用于从包含水和氯化锌的混合物中除去水的方法，其包括向包含水和氯化锌的所述混合物中加入非质子极性稀释剂，其中在所述稀释剂和水之间未形成共沸物的情况下为沸点下述蒸馏的压力条件高于水的沸点，并且在该沸点沸点下为液体形式，或者在下述蒸馏的压力和温度条件下与水形成共沸物或杂合物，并且从该混合物中除去包含水，氯化锌和稀释剂的混合物，除去水或所述共沸物或所述杂共聚物，得到包含氯化锌和所述稀释剂的无水混合物。

43. 发明授权

US08278474B2 Method for the separation of pentenenitrile isomers 有权
标题翻译：戊烯腈异构体分离方法
公开(公告)号：US08278474B2
公开(公告)日：2012-10-02
申请号：US13047212
申请日：2011-03-14
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/34
CPC分类号： C07C253/34 , C07C255/07
摘要： A process is described for separating mixtures of isomeric pentenenitriles, in which at least one isomer is removed from the mixture, wherein the separation of the substance mixtures of isomeric pentenenitriles is effected distillatively under reduced pressure.
摘要翻译：描述了用于分离异构戊烯腈混合物的方法，其中从混合物中除去至少一种异构体，其中异构戊烯腈的物质混合物的分离在减压下进行蒸馏。

44. 发明授权

US07541486B2 Method for producing 3-pentenenitrile 有权
标题翻译： 3-戊烯腈的制备方法
公开(公告)号：US07541486B2
公开(公告)日：2009-06-02
申请号：US10586007
申请日：2005-01-27
申请人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
发明人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
IPC分类号： C07C255/00 , C07C253/00
CPC分类号： C07C253/10 , C07C253/34 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile, characterized by the following process steps: (a) reacting 1,3-butadiene with hydrogen cyanide over at least one catalyst to obtain a stream 1 which comprises 3-pentenenitrile, 2-methyl-3-butenenitrile, the at least one catalyst and 1,3-butadiene, (b) distilling stream 1 in a column to obtain a high-1,3-butadiene stream 2 as the top product and a low-1,3-butadiene stream 3 as the bottom product which comprises 3-pentenenitrile, the at least one catalyst and 2-methyl-3-butenenitrile, (c) distilling stream 3 in a column to obtain a stream 4 as the top product which comprises 1,3-butadiene, a stream 5 which comprises 3-pentenenitrile and 2-methyl-3-butenenitrile at a side draw of the column, and a stream 6 as the bottom product which comprises the at least one catalyst, (d) distilling stream 5 to obtain a stream 7 as the top product which comprises 2-methyl-3-butenenitrile, and a stream 8 as the bottom product which comprises 3-pentenenitrile.
摘要翻译：描述了一种制备3-戊烯腈的方法，其特征在于以下工艺步骤：（a）使1,3-丁二烯与氰化氢在至少一种催化剂上反应，得到流1，其包含3-戊烯腈，2-甲基-3 丁烯腈，至少一种催化剂和1,3-丁二烯，（b）在塔中蒸馏物流1，得到作为顶部产物的高-1,3-丁二烯流2和低-1,3-丁二烯流 3作为底部产物，其包含3-戊烯腈，至少一种催化剂和2-甲基-3-丁烯腈，（c）在塔中蒸馏流3以获得作为顶部产物的料流4，其包含1,3-丁二烯，在塔的侧馏分中包含3-戊烯腈和2-甲基-3-丁烯腈的料流5和作为底部产物的料流6，其包含至少一种催化剂，（d）蒸馏流5以获得流7作为顶部产物，其包含2-甲基-3-丁烯腈，以及作为底部产物的料流8，其包含3-戊烯腈

45. 发明授权

US07504529B2 Method for hydrocyanation 有权
标题翻译：加氢氰化法
公开(公告)号：US07504529B2
公开(公告)日：2009-03-17
申请号：US10587027
申请日：2005-01-26
申请人： Tim Jungkamp , Hans-Martin Polka , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Hans-Martin Polka , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/08
CPC分类号： C07C253/34 , C07C255/07 , C07C255/04
摘要： A process is described for removing hydrogen cyanide from mixtures comprising pentenenitrile, wherein the removal is effected by an azeotropic distillation of hydrogen cyanide with 1,3-butadiene.
摘要翻译：描述了从包含戊烯腈的混合物中除去氰化氢的方法，其中通过氰化氢与1,3-丁二烯的共沸蒸馏来进行除去。

46. 发明申请

US20080242883A1 Method for the Hydrocyanation of Butadiene 有权
标题翻译：丁二烯氢化方法
公开(公告)号：US20080242883A1
公开(公告)日：2008-10-02
申请号：US10587026
申请日：2005-01-27
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C255/01
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene in the presence of at least one catalyst, wherein the reaction is carried out in a loop reactor having external pumped circulation and jet nozzle for driving the internal circulation.
摘要翻译：描述了一种通过在至少一种催化剂存在下氢氰化1,3-丁二烯来制备3-戊烯腈的方法，其中反应在具有外部泵送循环的环流反应器和用于驱动内部循环的喷嘴中进行。

47. 发明申请

US20070112215A1 Method for the separation of pentenenitrile isomers 审中-公开
标题翻译：戊烯腈异构体分离方法
公开(公告)号：US20070112215A1
公开(公告)日：2007-05-17
申请号：US10586452
申请日：2005-01-26
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C255/04
CPC分类号： C07C253/34 , C07C255/07
摘要： A process is described for separating mixtures of isomeric pentenenitriles, in which at least one isomer is removed from the mixture, wherein the separation of the substance mixtures of isomeric pentenenitriles is effected distillatively under reduced pressure.
摘要翻译：描述了用于分离异构戊烯腈混合物的方法，其中从混合物中除去至少一种异构体，其中异构戊烯腈的物质混合物的分离在减压下进行蒸馏。

48. 发明申请

US20080083607A1 Extraction of Nickel (0) Complexes from Nitrile Mixtures with Reduced Rag Formation 有权
标题翻译：从腈混合物中提取镍（0）配合物，减少碎屑形成
公开(公告)号：US20080083607A1
公开(公告)日：2008-04-10
申请号：US11577231
申请日：2005-10-12
申请人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
发明人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
IPC分类号： B01D11/04
CPC分类号： B01J31/4053 , B01D11/0434 , B01J31/1845 , B01J31/185 , B01J31/24 , B01J31/403 , B01J2231/323 , B01J2531/847 , C07C253/10 , C07C253/32 , Y02P20/584 , C07C255/04
摘要： A process for extractively removing homogeneously dissolved catalysts from a reaction effluent of a hydrocyanation of unsaturated mononitriles to dinitriles, by extraction by means of a hydrocarbon H, which comprises a) adding a nonpolar aprotic liquid L to the reaction effluent to obtain a stream I, and b) extracting the stream I at a temperature T with the hydrocarbon H to obtain a stream II comprising the hydrocarbon H enriched with the catalyst and a stream III having a low catalyst content.
摘要翻译：一种通过烃H提取从不饱和单腈的氢化氰化反应流出物向二腈提取均匀溶解的催化剂的方法，该方法包括：a）向反应流出物中加入非极性非质子液体L以获得流I，和b）用烃H提取温度T下的物流I以获得包含富含催化剂的烃H的流II和具有低催化剂含量的流III。

49. 发明授权

US07935229B2 Extraction of nickel (0) complexes from nitrile mixtures with reduced rag formation 有权
标题翻译：从腈混合物中提取镍（0）配合物，并减少破布形成
公开(公告)号：US07935229B2
公开(公告)日：2011-05-03
申请号：US11577231
申请日：2005-10-12
申请人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
发明人： Petra Deckert , Peter Bassler , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel , Peter Pfab , Tobias Aechtner , Wolfgang Siegel
IPC分类号： B01D3/34 , B01D11/04 , B01J31/40 , B01J38/56 , C07C253/32
CPC分类号： B01J31/4053 , B01D11/0434 , B01J31/1845 , B01J31/185 , B01J31/24 , B01J31/403 , B01J2231/323 , B01J2531/847 , C07C253/10 , C07C253/32 , Y02P20/584 , C07C255/04
摘要： A process for extractively removing homogeneously dissolved catalysts from a reaction effluent of a hydrocyanation of unsaturated mononitriles to dinitriles with a hydrocarbon H, including performing the steps of a) concentrating the reaction effluent before step b) by distillation at pressures of from 0.1 to 5000 mbar and temperatures of from 10 to 150° C., b) adding a hydrocarbon H to the concentrated reaction effluent to obtain a stream I, and c) feeding stream I, without prior separation of the liquid phases, into an extraction apparatus and extracting it at a temperature T with the hydrocarbon H to obtain a stream II comprising the hydrocarbon H enriched with the catalyst and a stream III having a low catalyst content.
摘要翻译：一种从均匀溶解的催化剂中将不饱和单腈的氢化氰化为碳氢化合物的反应流出物的方法，包括以下步骤：a）在步骤b）之前将反应流出物浓缩至0.1至5000毫巴和10至150℃的温度，b）向浓缩的反应流出物中加入烃H以获得流I，和c）将料流I未经预先分离的液相进入萃取装置并萃取在与烃H的温度T下，获得包含富含催化剂的烃H的流II和具有低催化剂含量的流III。

50. 发明申请

US20080076944A1 Purification of Phosphorus Chelate Ligands 审中-公开
标题翻译：磷螯合配体的纯化
公开(公告)号：US20080076944A1
公开(公告)日：2008-03-27
申请号：US11576575
申请日：2005-09-30
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Tobias Aechtner , Jens Scheidel , Hermann Luyken , Peter Pfab , Wolfgang Siegel , Verena Weiskopf
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Tobias Aechtner , Jens Scheidel , Hermann Luyken , Peter Pfab , Wolfgang Siegel , Verena Weiskopf
IPC分类号： C07F9/09
CPC分类号： B01D11/0492 , C07F9/025 , C07F9/145
摘要： A process for purifying phosphorus chelate ligands by extraction, by using polar extractants.
摘要翻译：通过萃取，通过极性萃取剂纯化磷螯合配体的方法。

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