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41. 发明授权

US6130198A Bleaching efficiency boosters for bleach and textile detergent compositions 失效
标题翻译：漂白剂和纺织洗涤剂组合物的漂白效率增强剂
公开(公告)号：US6130198A
公开(公告)日：2000-10-10
申请号：US155354
申请日：1998-09-28
申请人： Thomas Wehlage , Dieter Boeckh , Werner Bertleff , Alfred Oftring
发明人： Thomas Wehlage , Dieter Boeckh , Werner Bertleff , Alfred Oftring
IPC分类号： C11D3/30 , C11D3/39 , C11D3/395 , C11D3/28
CPC分类号： C11D3/30 , C11D3/3902 , C11D3/392
摘要： Use of amines as bleaching efficiency boosters for textile detergent compositions, where the pK.sub.a of the amines is greater than the pH minus 1, preferably greater than the pH, particularly preferably at least 0.5 greater than the pH of the 1% by weight wash liquor obtained from the textile detergent composition.
摘要翻译： PCT No.PCT / EP97 / 01513 Sec。 371日期：1998年9月28日 102（e）1998年9月28日PCT 1997年3月25日PCT公布。公开号WO97 / 35950 日期1997年10月2日使用胺作为纺织洗涤剂组合物的漂白效率增强剂，其中胺的pKa大于pH值减去1，优选大于pH，特别优选至少比pH 1％至少大0.5，由洗涤剂组合物得到的洗涤液。

42. 发明授权

US5254741A Rhodium hydroformylation catalysts containing bisphosphite ligands 失效
标题翻译：含有二亚磷酸酯配体的铑加氢甲酰化催化剂
公开(公告)号：US5254741A
公开(公告)日：1993-10-19
申请号：US967433
申请日：1992-10-28
申请人： Peter M. Lorz , Werner Bertleff , Michael Roeper , Dieter Koeffer
发明人： Peter M. Lorz , Werner Bertleff , Michael Roeper , Dieter Koeffer
IPC分类号： B01J31/22 , B01J31/18 , C07B61/00 , C07C45/50 , C07C47/02 , C07F9/6574 , C07F15/00
CPC分类号： C07F15/008 , B01J31/185 , C07C45/50 , C07F9/65746 , B01J2231/321 , B01J2531/0266 , B01J2531/822
摘要： Rhodium hydroformylation catalysts containing bisphosphite ligands of the formula I ##STR1## where -X- is a divalent bisarylene radical or R.sup.1,w is a divalent arylene, bisarylene or alkylene radical, andR.sup.1 and R.sup.2 are identical or different and are substituted or unsubstituted alkylene or ortho-arylene.
摘要翻译：铑加氢甲酰化催化剂含有式I的二亚磷酸酯配位体，其中-X-是二价双亚芳基或R 1，w是二价亚芳基，双亚芳基或亚烷基，R 1和R 2相同或不同，并且是取代或未取代的亚烷基或邻亚芳基。

43. 发明授权

US5107015A Process for the preparation of 2-formyl-2-methyl succinates 失效
标题翻译：制备2-甲基-2-甲基己酸酯的方法
公开(公告)号：US5107015A
公开(公告)日：1992-04-21
申请号：US602515
申请日：1990-10-24
申请人： Werner Bertleff , Gerhard Butz
发明人： Werner Bertleff , Gerhard Butz
IPC分类号： C07C67/347
CPC分类号： C07C67/347
摘要： The preparation of 2-formyl-2-methyl succinates by reacting itaconates with carbon monoxide and hydrogen in contact with a catalyst system comprising rhodium and a tertiary phosphorus compound, wherein the reaction is carried out under a pressure of from 90 to 325 bar.
摘要翻译：通过使衣康酸酯与一氧化碳和氢气与包含铑和叔磷化合物的催化剂体系接触来制备2-甲酰基-2-甲基琥珀酸酯，其中反应在90至325巴的压力下进行。

44. 发明授权

US4999443A Transition metal complexes 失效
标题翻译：过渡金属络合物
公开(公告)号：US4999443A
公开(公告)日：1991-03-12
申请号：US360863
申请日：1989-06-02
申请人： Werner Bertleff , Dieter Koeffer , Wolfgang Klaeui , Choong-Eui Song
发明人： Werner Bertleff , Dieter Koeffer , Wolfgang Klaeui , Choong-Eui Song
IPC分类号： B01J31/22 , B01J31/16 , B01J31/18 , C07B61/00 , C07C1/00 , C07C2/48 , C07C5/03 , C07C5/08 , C07C13/18 , C07C45/00 , C07C45/50 , C07C47/02 , C07C67/00 , C07C67/347 , C07C69/76 , C07F15/00 , C07F15/06
CPC分类号： C07F15/06 , B01J31/1845 , B01J31/185 , B01J31/2295 , C07C2/48 , C07C45/50 , C07C5/03 , C07C5/08 , C07F15/0006 , C07F15/0046 , C07F15/0073 , B01J2231/321 , B01J2231/328 , B01J2231/645 , B01J2531/821 , B01J2531/822 , B01J2531/827 , B01J2531/845 , C07C2531/22
摘要： Transition metal complexes of the general formula I[A].sup.x- [Q].sup.+.sub.x Iwhere Q is one equivalent of a cation, x is from 0 to 2 and A is a transition metal complex of the general formula ##STR1## where n is from 1 to 3, M is positively charged cobalt, rhodium, iridium or ruthenium, the ligands B are phosphonic, arsonic, phosphinic and/or arsinic acid ligands which are esterified with identical or different alcohols, one or more of these alcohol components carrying a functional group, L is ##STR2## the radicals R.sup.5 are identical or different radicals from the group consisting of C.sub.1 -C.sub.4 -alkyl and phenyl, p is an integer from 0 to 6, q is an integer from 0 to 5, and R.sup.1 is fluorine, chlorine, bromine, iodine, cyanide, isocyanide, cyanate, isocyanate, thiocyanate, isothiocyanate, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -trialkyl phosphite or triaryl phosphite, are used as catalysts, or prepared in situ, in processes for the cyclotrimerization of acetylene compounds, for the catalytic hydrogenation of unsaturated compounds and for the hydroformylation of alkenes.
摘要翻译：通式I [A] x- [Q] + xI的过渡金属配合物，其中Q是1当量阳离子，x为0-2，A为通式为A的过渡金属络合物，其中n M为正电荷的钴，铑，铱或钌，配位体B为与相同或不同的醇酯化的膦酸，芳香族，次膦酸和/或亚磺酸配体，一种或多种这些醇组分携带官能团，L是基团R 5是与C 1 -C 4烷基和苯基相同或不同的基团，p是0至6的整数，q是0至5的整数，并且R 1 使用氟，氯，溴，碘，氰化物，异氰酸酯，氰酸酯，异氰酸酯，硫氰酸酯，异硫氰酸酯，C1-C4烷基，C1-C4-三烷基亚磷酸酯或亚磷酸三芳基酯作为催化剂，或原位制备乙炔化合物的环三聚化，用于不饱和化合物的催化氢化并且用于烯烃的加氢甲酰化。

45. 发明授权

US4947005A Preparation of 1,1,2-trialkoxyethanes 失效
标题翻译： 1,1,2-三烷氧基乙醚的制备
公开(公告)号：US4947005A
公开(公告)日：1990-08-07
申请号：US398715
申请日：1989-08-25
申请人： Dieter Koeffer , Werner Bertleff
发明人： Dieter Koeffer , Werner Bertleff
IPC分类号： C07D325/00 , B01J31/20 , B01J31/26 , C07B61/00 , C07C41/48 , C07C43/315
CPC分类号： C07C41/48
摘要： 1,1,2-Trialkoxyethanes of the general formula I ##STR1## where R.sup.1 to R.sup.3 are each independently of the others C.sub.1 -C.sub.20 -alkyl or cycloalkyl, or R.sup.1 and R.sup.2 may be linked together to form a 5-, 6- or 7-membered ring, are prepared by reacting formaldehyde dialkyl acetals of the general formula II ##STR2## where R.sup.1 and R.sup.2 are each as defined above, or compounds which are capable of forming formaldehyde dialkyl acetals under the reaction conditions, with carbon monoxide, hydrogen and alkanols R.sup.3 OH under superatmospheric pressure at elevated temperature in the presence of a catalyst composed of a cobalt carbonyl compound and a promotor, wherein the promotor is an alkali metal, alkaline earth metal or ammonium salt of a protogenic compound having an acid constant K.sub.a of from 10.sup.-2 to 10.sup.-14, an alkali metal or alkaline earth metal hydroxide or an aminocarboxylic acid.
摘要翻译：其中R 1至R 3各自独立地为C 1 -C 20 - 烷基或环烷基的通式I（I）的1,1,2-三烷氧基乙基，或者R 1和R 2可以连接在一起形成5-， 6-或7-元环通过使通式II（II）的甲醛二烷基缩醛反应其中R1和R2各自如上所定义，或在反应条件下能够形成甲醛二烷基缩醛的化合物在由羰基钴化合物和促进剂组成的催化剂存在下，在高温下在超大气压下与一氧化碳，氢气和链烷醇R3OH反应，其中所述促进剂是原始化合物的碱金属，碱土金属或铵盐，其具有 10-2至10-14的酸常数K a，碱金属或碱土金属氢氧化物或氨基羧酸。

46. 发明授权

US4755625A Preparation of 1,1,2-trialkoxyethanes 失效
标题翻译： 1,1,2-三烷氧基乙醚的制备
公开(公告)号：US4755625A
公开(公告)日：1988-07-05
申请号：US73999
申请日：1987-07-16
申请人： Robert Maerkl , Werner Bertleff , Rudolf Kummer
发明人： Robert Maerkl , Werner Bertleff , Rudolf Kummer
IPC分类号： C07B61/00 , B01J31/00 , B01J31/20 , B01J31/24 , C07C41/00 , C07C41/48 , C07C43/315 , C07C67/00 , C07D317/22 , C07D319/06 , C07D321/06
CPC分类号： C07C41/48
摘要： 1,1,2-trialkoxyethanes I ##STR1## where R.sup.1, R.sup.2 and R.sup.3 are each C.sub.1 -C.sub.8 -alkyl and R.sup.1 and R.sup.2 may furthermore be bonded to one another to form a 5-membered to 7-membered ring, are prepared by reacting a formaldehyde dialkyl acetal II with carbon monoxide and hydrogen, from 0.5 to 1.5 moles of hydrogen being used per mole of carbon monoxide, and with not less than 1 mole of alcohol R.sup.3 OH per mole of formaldehyde dialkyl acetal under superatmospheric pressure and at elevated temperatures in the presence of a catalyst which is formed from a cobalt carbonyl compound and a trivalent organic compound of the formula III ##STR2## where A is phosphorus, arsenic, antimony or bismuth and R.sup.4, R.sup.5 and R.sup.6 are each an organic radical.
摘要翻译：其中R 1，R 2和R 3各自是C 1 -C 8 - 烷基，R 1和R 2可以彼此键合形成5元至7元环，通过使甲醛二烷基缩醛II与一氧化碳和氢反应，每摩尔一氧化碳使用0.5至1.5摩尔氢，并且在超大气压下每摩尔甲醛二烷基缩醛不少于1摩尔醇R3OH，在由羰基钴化合物和式III的三价有机化合物形成的催化剂存在下，在升高的温度下，其中A是磷，砷，锑或铋，并且R 4，R 5和R 6各自是有机的激进。

47. 发明授权

US4600726A Preparation of ethylene glycol 失效
标题翻译：乙二醇的制备
公开(公告)号：US4600726A
公开(公告)日：1986-07-15
申请号：US758293
申请日：1985-07-24
申请人： Werner Bertleff , Franz-Josef Muller , Rudolf Kummer , Wolfgang Harder
发明人： Werner Bertleff , Franz-Josef Muller , Rudolf Kummer , Wolfgang Harder
IPC分类号： C07C27/06 , B01J23/00 , B01J23/89 , C07B61/00 , C07C27/00 , C07C29/15 , C07C29/158 , C07C31/20 , C07C67/00
CPC分类号： C07C29/158 , Y02P20/52
摘要： Ethylene glycol is prepared from carbon monoxide and hydrogen under superatmospheric pressure and at an elevated temperature in the presence of a rhodium-containing catalyst together with a cobalt catalyst, the molar ratio of rhodium to cobalt being from about 20:1 to 60:1.
摘要翻译：乙二醇由一氧化碳和氢气在超大气压和高温下在含铑催化剂和钴催化剂存在下制备，铑与钴的摩尔比为约20:1至60:1。

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