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41. 发明授权

US08609894B2 Process for preparing aminopolycarboxylates 有权
标题翻译：制备氨基多羧酸盐的方法
公开(公告)号：US08609894B2
公开(公告)日：2013-12-17
申请号：US13437093
申请日：2012-04-02
申请人： Robert Baumann , Markus Christian Biel , Axel Franzke , Alfred Oftring , Friedhelm Teich , Paul Klingelhoefer , Marie Katrin Schroeter
发明人： Robert Baumann , Markus Christian Biel , Axel Franzke , Alfred Oftring , Friedhelm Teich , Paul Klingelhoefer , Marie Katrin Schroeter
IPC分类号： C07C51/21
CPC分类号： C07C227/02
摘要： A process for preparing aminopolycarboxylates proceeding from the corresponding polyalkanolamines by oxidative dehydrogenation in the presence of a catalyst comprising 1 to 90% by weight of copper, based on the total weight of the catalyst, using a base, which comprises first performing a partial conversion of the polyalkanolamine to a reaction mixture comprising the aminopolycarboxylate at a temperature in the range from 140 to 180° C. until at least 10 to 90 mol% of the polyalkanolamine has been depleted, and then continuing the conversion at elevated temperature.
摘要翻译：在催化剂存在下，通过氧化脱氢从相应的聚链烷醇胺制备氨基多羧酸盐的方法，所述催化剂包含1至90重量％的铜，基于催化剂的总重量，使用碱，其包括首先进行部分转化将聚烷醇胺加入到包含氨基多羧酸盐的反应混合物中，温度范围为140-180℃，直到聚链烷醇胺的至少10至90摩尔％已经耗尽，然后在升高的温度下继续转化。

42. 发明申请

US20110257431A1 PROCESS FOR PRODUCING SIDE PRODUCT-FREE AMINOCARBOXYLATES 审中-公开
标题翻译：生产无机氨基甲酸酯的方法
公开(公告)号：US20110257431A1
公开(公告)日：2011-10-20
申请号：US13050495
申请日：2011-03-17
申请人： Robert Baumann , Markus Christian Biel , Gordon Brasche , Axel Franzke , Thomas Heidenfelder , Paul Klingelhoefer , Alfred Oftring , Marie Katrin Schroter
发明人： Robert Baumann , Markus Christian Biel , Gordon Brasche , Axel Franzke , Thomas Heidenfelder , Paul Klingelhoefer , Alfred Oftring , Marie Katrin Schroter
IPC分类号： C07C227/02
CPC分类号： C07C227/02 , C07C229/16
摘要： The present invention relates to a process for preparing aminocarboxylates, proceeding from amines, by employing a reaction sequence composed of ethoxylation to amino alcohols and subsequent oxidative dehydrogenation to the corresponding aminocarboxylates, especially the alkali metal or alkaline earth metal salts of the complexing agents MGDA (methylglycinediacetic acid), EDTA (ethylenediaminetetra-acetic acid) and GLDA (glutamic acid diacetic acid) or the free acids thereof.
摘要翻译：本发明涉及一种通过使用由乙氧基化氨基醇组成的反应顺序并随后氧化脱氢至相应的氨基羧酸盐，特别是络合剂MGDA的碱金属或碱土金属盐来制备氨基羧酸盐的方法，甲基甘氨酸二乙酸），EDTA（乙二胺四乙酸）和GLDA（谷氨酸二乙酸）或其游离酸。

43. 发明申请

US20110207634A1 PREPARING ETHER CARBOXYLATES 有权
标题翻译：制备醚类羧酸酯
公开(公告)号：US20110207634A1
公开(公告)日：2011-08-25
申请号：US13030816
申请日：2011-02-18
申请人： Robert Baumann , Markus Christian Biel , Andreas Deckers , Alfred Oftring , Frank Rittig , Wolfgang Staffel
发明人： Robert Baumann , Markus Christian Biel , Andreas Deckers , Alfred Oftring , Frank Rittig , Wolfgang Staffel
IPC分类号： C09K8/60 , C11D1/74 , C07C67/00 , C07C227/02 , C07C69/708 , C07C229/26 , C07C229/24 , C07C231/12 , C07C235/74
CPC分类号： C11D3/3711 , A61K8/86 , A61K2800/10 , A61K2800/80 , A61K2800/805 , A61Q19/00 , C07C51/41 , C07C213/06 , C11D1/74 , C07C59/125
摘要： The present invention relates to a process for preparing ether carboxylates.
摘要翻译：本发明涉及一种制备醚羧酸盐的方法。

44. 发明授权

US07977434B2 Polymeric hydrophobic aminonitrile quats used for bleach activation 有权
标题翻译：用于漂白活化的聚合疏水性氨基腈季铵盐
公开(公告)号：US07977434B2
公开(公告)日：2011-07-12
申请号：US11815410
申请日：2006-01-25
申请人： Frank Dietsche , Alfred Oftring
发明人： Frank Dietsche , Alfred Oftring
IPC分类号： C11D11/00 , C11D3/39 , C08G73/02
CPC分类号： C11D3/3925 , C08G73/0226 , C11D3/3769
摘要： The present invention relates to a polymer for use as a bleach activator, comprising the monomer units where n is an integer from 1 to 4 and R is a branched or unbranched, saturated hydrocarbyl radical having from 1 to 20 carbon atoms, to processes for the preparation and to the use thereof as laundry detergents, cleaning compositions and disinfectant compositions, and also in textile bleaching and paper bleaching.
摘要翻译：本发明涉及一种用作漂白活化剂的聚合物，其包含单体单元，其中n为1至4的整数，R为具有1至20个碳原子的支链或非支链的饱和烃基，用于制剂及其作为衣物洗涤剂，清洁组合物和消毒剂组合物以及织物漂白和纸张漂白的用途。

45. 发明申请

US20110124919A1 3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF 审中-公开
标题翻译： 3-氨基甲基-1-环己基氨基胺及其生产方法
公开(公告)号：US20110124919A1
公开(公告)日：2011-05-26
申请号：US13055595
申请日：2009-07-13
申请人： Martin Ernst , Kirsten Dahmen , Alfred Oftring
发明人： Martin Ernst , Kirsten Dahmen , Alfred Oftring
IPC分类号： C07C211/49
CPC分类号： C07C211/36 , C07B2200/09 , C07C2601/14
摘要： The present invention relates to 3-aminomethyl-1-cyclohexylamine and to a process for preparation thereof by a) reacting cyclohexenone with hydrogen cyanide in the presence of a basic catalyst, b) reacting the cyclohexanonenitrile obtained in stage a) with ammonia in the presence of an imine formation catalyst, and c) reacting the 3-cyanocyclohexylimine-containing reaction mixture obtained in stage b) with hydrogen and ammonia over hydrogenation catalysts.The present invention further relates to the use of 3-aminomethyl-1-cyclohexylamine as a hardener for epoxy resins, as an intermediate in the preparation of diisocyanates, as a starter in the preparation of polyetherols and/or as a monomer for polyamide preparation.
摘要翻译：本发明涉及3-氨基甲基-1-环己基胺及其制备方法，其通过以下步骤a）使环己烯酮与氰化氢在碱性催化剂存在下反应，b）在步骤a）中得到的环己腈与氨在存在下反应的亚胺形成催化剂，和c）使步骤b）中获得的含3-氰基环己基亚胺的反应混合物与氢气和氨在氢化催化剂上反应。本发明还涉及3-氨基甲基-1-环己胺作为环氧树脂的硬化剂的用途，作为制备二异氰酸酯的中间体，作为制备聚乙烯醇和/或作为聚酰胺制备的单体的起始物。

46. 发明授权

US07915454B2 Method for producing ethylenediamine 有权
标题翻译：乙二胺的制备方法
公开(公告)号：US07915454B2
公开(公告)日：2011-03-29
申请号：US12529107
申请日：2008-02-28
申请人： Alfred Oftring , Kirsten Dahmen , Randolf Hugo , Thilo Hahn , Katrin Baumann , Johann-Peter Melder
发明人： Alfred Oftring , Kirsten Dahmen , Randolf Hugo , Thilo Hahn , Katrin Baumann , Johann-Peter Melder
IPC分类号： C07C209/48
CPC分类号： C07C209/48 , C07C211/10
摘要： The invention relates to a process for preparing ethylenediamine by hydrogenation of aminoacetonitrile over a catalyst, wherein the hydrogenation is carried out in a solution comprising aminoacetonitrile, water in a proportion of from 0 to 60% by weight and a solvent and the aminoacetonitrile comprised in the solution is fed into the reaction vessel at a rate which is not greater than the rate at which the aminoacetonitrile reacts with hydrogen in the hydrogenation.
摘要翻译：本发明涉及一种通过氨基乙腈在催化剂上氢化制备乙二胺的方法，其中氢化是在包含氨基乙腈的溶液中，以0至60重量％的比例的水和溶剂和包含在其中的氨基乙腈溶液以不大于氨基乙腈在氢化中与氢反应的速率进料到反应容器中。

47. 发明申请

US20100099872A1 PRODUCTION METHOD FOR ETHYLENEAMINE MIXTURES 有权
标题翻译：乙烯胺混合物的生产方法
公开(公告)号：US20100099872A1
公开(公告)日：2010-04-22
申请号：US12529087
申请日：2008-02-27
申请人： Kirsten Dahmen , Alfred Oftring , Katrin Baumann , Randolf Hugo , Thilo Hahn , Johann-Peter Melder
发明人： Kirsten Dahmen , Alfred Oftring , Katrin Baumann , Randolf Hugo , Thilo Hahn , Johann-Peter Melder
IPC分类号： C07D241/04 , C07C209/00
CPC分类号： C07C209/48 , C07C211/10 , C07C211/13 , C07C211/14 , C07C253/30 , C07C255/25
摘要： The invention relates to a process for preparing an ethylene amine mixture, which comprises hydrogenating an amino nitrile mixture comprising at least two α-amino nitriles in an amount of at least 5% by weight in each case in the presence of a catalyst and, if appropriate, a solvent.
摘要翻译：本发明涉及一种制备乙烯胺混合物的方法，该方法包括在催化剂存在下，将包含至少两种α-氨基腈的氨基腈混合物氢化为至少5重量％，如果适当的溶剂。

48. 发明授权

US07671234B2 Method for producing methylglycine-N,N-diethanoic acid-trialkali metal salts with a low by-product content 有权
标题翻译：具有低副产物含量的甲基甘氨酸-N，N-二乙酸 - 三烷基金属盐的制备方法
公开(公告)号：US07671234B2
公开(公告)日：2010-03-02
申请号：US11913597
申请日：2006-05-02
申请人： Alfred Oftring , Gerold Braun , Friedrich Wirsing , Armin Stamm , Kai-Uwe Baldenius
发明人： Alfred Oftring , Gerold Braun , Friedrich Wirsing , Armin Stamm , Kai-Uwe Baldenius
IPC分类号： C07C227/26 , C07C229/16
CPC分类号： C07C227/26 , C07C229/16
摘要： The invention relates to a process for preparing low-by-product, light-color methylglycine-N,N-diacetic acid tri(alkali metal) salt by alkaline hydrolysis of methylglycinediacetonitrile (MGDN), comprising the steps in the sequence (a) to (f): (a) mixing of MGDN with aqueous alkali at a temperature of ≦30° C.; (b) allowing the aqueous alkaline MGDN suspension to react at a temperature in the range from 10 to 30° C. over a period of from 0.1 to 10 h to form a solution; (c) allowing the solution from step (b) to react at a temperature in the range from 30 to 40° C. over a period of from 0.1 to 10 h; (d) optionally allowing the solution from step (c) to react at a temperature in the range from 50 to 80° C. over a period of from 0.5 to 2 h; (e) optionally allowing the solution from step (c) or (d) to react at a temperature in the range from 110 to 200° C. over a period of from 5 to 60 min; (f) hydrolysis and removal of ammonia of the solution obtained in step (c), (d) or (e) by stripping at a temperature of from 90 to 105° C.
摘要翻译：本发明涉及通过甲基甘氨二乙腈（MGDN）的碱水解制备低副产物，浅色甲基甘氨酸-N，N-二乙酸三（碱金属）盐的方法，包括步骤（a）至（f）：（a）在温度为30℃的温度下，将MGDN与碱水溶液混合; （b）使含水碱性MGDN悬浮液在10至30℃的温度下反应0.1至10小时以形成溶液; （c）允许来自步骤（b）的溶液在0.1至10小时的时间内在30至40℃的温度下反应; （d）任选地允许步骤（c）的溶液在0.5至2小时的时间内在50至80℃的温度下反应; （e）任选地允许来自步骤（c）或（d）的溶液在110至200℃的温度下在5至60分钟的时间内反应; （f）通过在90至105℃的温度下汽提来水解和除去在步骤（c），（d）或（e）中获得的溶液中的氨。

49. 发明申请

US20100029976A1 METHOD FOR PRODUCING TETRAETHYLENEPENTAMINE 有权
标题翻译：生产四氯乙烯胺的方法
公开(公告)号：US20100029976A1
公开(公告)日：2010-02-04
申请号：US12529047
申请日：2008-02-27
申请人： Kirsten Dahmen , Alfred Oftring , Randolf Hugo , Thilo Hahn , Katrin Baumann , Johann-Peter Melder
发明人： Kirsten Dahmen , Alfred Oftring , Randolf Hugo , Thilo Hahn , Katrin Baumann , Johann-Peter Melder
IPC分类号： C07C209/44 , C07C255/25 , C07C253/00
CPC分类号： C07C209/48 , C07C255/25 , C07C211/14
摘要： The invention relates to a process for preparing tetraethylenepentamine (TEPA) by hydrogenation of diethylenetriaminediacetonitrile (DETDN) over a catalyst. If appropriate, DETDN can also be present as a constituent of an amino nitrile mixture which additionally comprises diethylenetriaminemonoacetonitrile (DETMN).
摘要翻译：本发明涉及通过在催化剂上氢化二亚乙基三胺二乙酸（DETDN）制备四亚乙基五胺（TEPA）的方法。如果合适，DETDN也可以作为另外包含二亚乙基三氨基乙腈（DETMN）的氨基腈混合物的组分存在。

50. 发明申请

US20080197082A1 Aminocarboxylic Acid Esters Having Eo/Po/Buo-Blockpolymers and Use Thereof as Demulsifiers 审中-公开
标题翻译：具有Eo / Po / Buo-Blockpolymers的氨基羧酸酯及其用作破乳剂
公开(公告)号：US20080197082A1
公开(公告)日：2008-08-21
申请号：US11917829
申请日：2006-06-14
申请人： Marcus Guzmann , Peter Neumann , Karl-Heinz Buchner , Alfred Oftring
发明人： Marcus Guzmann , Peter Neumann , Karl-Heinz Buchner , Alfred Oftring
IPC分类号： B01D17/04 , C08G65/00
CPC分类号： B01D17/047 , C08L53/00 , C08L2666/04 , C08L2666/14 , C08L2666/02 , C08L2666/24
摘要： The present invention relates to aminocarboxylic esters with EO/PO/BuO block polymers, processes for preparing such compounds and the use of these compounds as emulsion breakers, in particular for crude oil emulsions.
摘要翻译：本发明涉及具有EO / PO / BuO嵌段聚合物的氨基羧酸酯，制备这些化合物的方法以及这些化合物作为乳液破乳剂的用途，特别是用于原油乳液。

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