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1. 发明申请

US20110124919A1 3-AMINOMETHYL-1-CYCLOHEXYLAMINE, AND METHOD FOR THE PRODUCTION THEREOF 审中-公开
标题翻译： 3-氨基甲基-1-环己基氨基胺及其生产方法
公开(公告)号：US20110124919A1
公开(公告)日：2011-05-26
申请号：US13055595
申请日：2009-07-13
申请人： Martin Ernst , Kirsten Dahmen , Alfred Oftring
发明人： Martin Ernst , Kirsten Dahmen , Alfred Oftring
IPC分类号： C07C211/49
CPC分类号： C07C211/36 , C07B2200/09 , C07C2601/14
摘要： The present invention relates to 3-aminomethyl-1-cyclohexylamine and to a process for preparation thereof by a) reacting cyclohexenone with hydrogen cyanide in the presence of a basic catalyst, b) reacting the cyclohexanonenitrile obtained in stage a) with ammonia in the presence of an imine formation catalyst, and c) reacting the 3-cyanocyclohexylimine-containing reaction mixture obtained in stage b) with hydrogen and ammonia over hydrogenation catalysts.The present invention further relates to the use of 3-aminomethyl-1-cyclohexylamine as a hardener for epoxy resins, as an intermediate in the preparation of diisocyanates, as a starter in the preparation of polyetherols and/or as a monomer for polyamide preparation.
摘要翻译：本发明涉及3-氨基甲基-1-环己基胺及其制备方法，其通过以下步骤a）使环己烯酮与氰化氢在碱性催化剂存在下反应，b）在步骤a）中得到的环己腈与氨在存在下反应的亚胺形成催化剂，和c）使步骤b）中获得的含3-氰基环己基亚胺的反应混合物与氢气和氨在氢化催化剂上反应。本发明还涉及3-氨基甲基-1-环己胺作为环氧树脂的硬化剂的用途，作为制备二异氰酸酯的中间体，作为制备聚乙烯醇和/或作为聚酰胺制备的单体的起始物。

2. 发明申请

US20110218323A1 PROCESS FOR PREPARING CYCLIC DIAMINES 失效
标题翻译：制备循环泵的方法
公开(公告)号：US20110218323A1
公开(公告)日：2011-09-08
申请号：US13128508
申请日：2009-11-06
申请人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
发明人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
IPC分类号： C08G69/00 , C07C209/48 , C07C211/35 , C08G71/04
CPC分类号： C07C209/48 , C07C209/16 , C07C209/26 , C07C253/30 , C07C2601/14 , C07C211/36 , C07C255/46
摘要： The present invention relates to a process for preparing a cyclic diamine, comprising the reaction of at least one cyclic alkene with a gas mixture (G) comprising dinitrogen the subsequent conversion of monoxide to give at least one cyclic ketone and then converting the at least one cyclic ketone to a cyclic diamine. The invention also relates to the use of a cyclic diamine with primary and secondary amine functions thus obtained to prepare polyamides and polyurethanes.
摘要翻译：本发明涉及一种制备环状二胺的方法，其包括使至少一种环烯与包含二氮的气体混合物（G）的反应，随后将一氧化碳转化成至少一种环酮，然后将至少一种环酮到环状二胺。本发明还涉及具有如此获得的伯胺和仲胺官能团的环状二胺的用途，以制备聚酰胺和聚氨酯。

3. 发明授权

US08592632B2 Process for preparing cyclic diamines 失效
标题翻译：制备环状二胺的方法
公开(公告)号：US08592632B2
公开(公告)日：2013-11-26
申请号：US13128508
申请日：2009-11-06
申请人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
发明人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
IPC分类号： C07C209/26
CPC分类号： C07C209/48 , C07C209/16 , C07C209/26 , C07C253/30 , C07C2601/14 , C07C211/36 , C07C255/46
摘要： The present invention relates to a process for preparing a cyclic diamine, comprising the reaction of at least one cyclic alkene with a gas mixture (G) comprising dinitrogen the subsequent conversion of monoxide to give at least one cyclic ketone and then converting the at least one cyclic ketone to a cyclic diamine. The invention also relates to the use of a cyclic diamine with primary and secondary amine functions thus obtained to prepare polyamides and polyurethanes.
摘要翻译：本发明涉及一种制备环状二胺的方法，其包括使至少一种环烯与包含二氮的气体混合物（G）的反应，随后将一氧化碳转化成至少一种环酮，然后将至少一种环酮到环状二胺。本发明还涉及具有如此获得的伯胺和仲胺官能团的环状二胺的用途，以制备聚酰胺和聚氨酯。

4. 发明授权

US08586794B2 5-isopropyl-3-aminomethyl-2-methyl-1-amino-cyclohexane (carvone diamine), and method for the production thereof 失效
标题翻译： 5-异丙基-3-氨基甲基-2-甲基-1-氨基 - 环己烷（葡萄糖酮二胺）及其制备方法
公开(公告)号：US08586794B2
公开(公告)日：2013-11-19
申请号：US13055604
申请日：2009-07-13
申请人： Martin Ernst , Alfred Oftring , Kathrin Wissel-Stoll , Oemer Uensal , Stephan Freyer , Ansgar Gereon Altenhoff , Wolfgang Staffel
发明人： Martin Ernst , Alfred Oftring , Kathrin Wissel-Stoll , Oemer Uensal , Stephan Freyer , Ansgar Gereon Altenhoff , Wolfgang Staffel
IPC分类号： C07C209/00 , C07C211/00 , C08G63/48 , C08G63/91 , C08L67/00 , C08L67/02
CPC分类号： C07C211/36
摘要： The present invention relates to 5-isopropyl-3-aminomethyl-2-methyl-1-aminocyclohexane (carvonediamine) and to a process for preparation thereof by a) reacting carvone with hydrogen cyanide, b) then reacting the carvonenitrile obtained in stage a) with ammonia in the presence of an imine formation catalyst and c) then reacting the carvonenitrile imine-containing reaction mixture obtained in stage b) with hydrogen and ammonia over hydrogenation catalysts.The present invention further relates to the use of carvonediamine as a hardener for epoxy resins, as an intermediate in the preparation of diisocyanates, as a starter in the preparation of polyetherols and/or as a monomer for polyamide preparation.
摘要翻译：本发明涉及5-异丙基-3-氨基甲基-2-甲基-1-氨基环己烷（carvonediamine）及其制备方法，其通过以下步骤：a）使香芹酮与氰化氢反应，b）然后使得a）与氨在亚胺形成催化剂存在下反应，c）然后使步骤b）中得到的含氰腈亚胺的反应混合物与氢气和氨在氢化催化剂上反应。本发明还涉及作为制备二异氰酸酯的中间体，作为制备聚醚类和/或作为聚酰胺制备用单体的起始剂的环氧树脂用硬化剂的用途。

5. 发明申请

US20110124918A1 5-ISOPROPYL-3-AMINOMETHYL-2-METHYL-1-AMINO-CYCLOHEXANE (CARVONE DIAMINE), AND METHOD FOR THE PRODUCTION THEREOF 失效
标题翻译： 5-异丙基-3-氨基-2-乙基-2-甲基-1-氨基环己烷（卡波胺二胺）及其生产方法
公开(公告)号：US20110124918A1
公开(公告)日：2011-05-26
申请号：US13055604
申请日：2009-07-13
申请人： Martin Ernst , Alfred Oftring , Kathrin Wissel-Stoll , Oemer Uensal , Stephan Freyer , Ansgar Gereon Altenhoff , Wolfgang Staffel
发明人： Martin Ernst , Alfred Oftring , Kathrin Wissel-Stoll , Oemer Uensal , Stephan Freyer , Ansgar Gereon Altenhoff , Wolfgang Staffel
IPC分类号： C07C211/36 , C07C209/48
CPC分类号： C07C211/36
摘要： The present invention relates to 5-isopropyl-3-aminomethyl-2-methyl-1-aminocyclohexane (carvonediamine) and to a process for preparation thereof by a) reacting carvone with hydrogen cyanide, b) then reacting the carvonenitrile obtained in stage a) with ammonia in the presence of an imine formation catalyst and c) then reacting the carvonenitrile imine-containing reaction mixture obtained in stage b) with hydrogen and ammonia over hydrogenation catalysts.The present invention further relates to the use of carvonediamine as a hardener for epoxy resins, as an intermediate in the preparation of diisocyanates, as a starter in the preparation of polyetherols and/or as a monomer for polyamide preparation.
摘要翻译：本发明涉及5-异丙基-3-氨基甲基-2-甲基-1-氨基环己烷（carvonediamine）及其制备方法，其通过以下步骤：a）使香芹酮与氰化氢反应，b）然后使得a）与氨在亚胺形成催化剂存在下反应，c）然后使步骤b）中得到的含氰腈亚胺的反应混合物与氢气和氨在氢化催化剂上反应。本发明还涉及作为制备二异氰酸酯的中间体，作为制备聚醚类和/或作为聚酰胺制备用单体的起始剂的环氧树脂用硬化剂的用途。

6. 发明授权

US09234543B2 Guide arrangement and machine tool comprising such a guide arrangement 有权
标题翻译：引导装置和包括这种引导装置的机床
公开(公告)号：US09234543B2
公开(公告)日：2016-01-12
申请号：US13880104
申请日：2011-08-22
申请人： Kai Adler , Sabrina Gressler , Martin Ernst , Dietmar Kohler
发明人： Kai Adler , Sabrina Gressler , Martin Ernst , Dietmar Kohler
IPC分类号： F16C31/00 , F16C29/00 , B23Q1/01 , B23Q1/38 , B23Q1/40
CPC分类号： F16C29/008 , B23Q1/017 , B23Q1/38 , B23Q1/40 , F16C29/007 , F16C2322/39
摘要： Guide arrangement serving to guide a linear movement of a movable part (2) extending opposite a stationary part (1) along the movement axis and along a transverse direction oriented at a right angle to the movement axis, wherein the guide arrangement includes a support area belonging to the stationary part on which the movable part is slidingly supported and a roller guide arrangement (12) with a roller-guiding area belonging to the stationary part.
摘要翻译：引导装置，用于引导沿着运动轴线相对于静止部分（1）延伸并且沿着与移动轴线成直角定向的横向方向延伸的可移动部分（2）的线性运动，其中，引导装置包括支撑区域属于可移动部分滑动地支撑的固定部分，以及具有属于固定部分的滚轮引导区域的滚子引导装置（12）。

7. 发明授权

US08772547B2 Method for producing 1-adamantyl trimethylammonium hydroxide 有权
标题翻译： 1-金刚烷基三甲基氢氧化铵的制备方法
公开(公告)号：US08772547B2
公开(公告)日：2014-07-08
申请号：US13255805
申请日：2010-03-11
申请人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
发明人： Christof Wilhelm Wigbers , Martin Ernst , Laszlo Szarvas , Giovanni D'Andola , Ellen Dahlhoff , Gabriele Iffland , Peter Raatz , Falk Simon , Matthias Frauenkron
IPC分类号： C07C211/00
CPC分类号： C07C211/63 , C07C209/00 , C07C209/26 , C07C2603/74
摘要： The present invention relates to a process for preparing 1-adamantyltrimethylammonium hydroxide, by A) reacting 1-adamantyldimethylamine with dimethyl sulfate to give 1-adamantyltrimethylammonium sulfate; and B) subjecting the 1-adamantyltrimethylammonium sulfate obtained in A) to anion exchange with an ion exchanger loaded with OH ions.
摘要翻译：本发明涉及一种制备1-金刚烷基三甲基氢氧化铵的方法，通过A）使1-金刚烷基二甲胺与硫酸二甲酯反应得到1-金刚烷基三甲基硫酸铵; 和B）在A）中获得的1-金刚烷基三甲基硫酸铵与负载有OH离子的离子交换剂进行阴离子交换。

8. 发明授权

US08536377B2 Method for producing N,N-substituted-3-aminopropan-1-ols 有权
标题翻译：制备N，N-取代-3-氨基丙-1-醇的方法
公开(公告)号：US08536377B2
公开(公告)日：2013-09-17
申请号：US13127828
申请日：2009-11-02
申请人： Christof Wilhelm Wigbers , Johann-Peter Melder , Martin Ernst
发明人： Christof Wilhelm Wigbers , Johann-Peter Melder , Martin Ernst
IPC分类号： C07C213/00
CPC分类号： C07C213/02 , C07C227/08 , Y02P20/582 , C07C215/08 , C07C229/12
摘要： The present invention relates to a process for preparing N,N-substituted 3-aminopropan-1-ols by a) reacting secondary amine with acrolein at a temperature of (−50) to 100° C. and a pressure of 0.01 to 300 bar, and b) reacting the reaction mixture obtained in stage a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a pressure of 1 to 400 bar, wherein the molar ratio of secondary amine to acrolein in stage a) is 1:1 or more and the temperature in stage b) is in the range from (−50) to 70° C. In a preferred embodiment, acrolein which has been obtained from glycerol based on renewable raw materials is used. The invention further relates to the use of an N,N-dimethyl-3-aminopropan-1-ol (DMAPOL) based on renewable raw materials as a catalyst for polyurethane preparation, as a scrubbing fluid in gas scrubbing, in the electronics chemicals and electroplating sectors, as a feedstock in organic synthesis, and as an intermediate in the production of pharmaceuticals and crop protection compositions.
摘要翻译：本发明涉及一种通过以下步骤制备N，N-取代的3-氨基丙-1-醇的方法：a）在（-50）至100℃的温度和0.01至300巴的压力下使仲胺与丙烯醛反应，和b）在加氢催化剂存在下，在1至400巴的压力下，将a）中获得的反应混合物与氢气和氨反应，其中a）步中仲胺与丙烯醛的摩尔比为1:1 或更高，步骤b）中的温度在（-50）至70℃的范围内。在优选的实施方案中，使用了基于可再生原料从甘油获得的丙烯醛。本发明还涉及使用基于可再生原料的N，N-二甲基-3-氨基丙-1-醇（DMAPOL）作为聚氨酯制备的催化剂，在电气化学品中用作气体洗涤中的洗涤液，电镀部门，作为有机合成中的原料，以及作为药物和作物保护组合物生产中的中间体。

9. 发明授权

US08461391B2 Method for producing N,N-substituted-1,3-propandiamines 有权
标题翻译：制备N，N-取代-1,3-丙二胺的方法
公开(公告)号：US08461391B2
公开(公告)日：2013-06-11
申请号：US12991767
申请日：2009-05-11
申请人： Martin Ernst , Johann-Peter Melder , Christof Wilhelm Wigbers
发明人： Martin Ernst , Johann-Peter Melder , Christof Wilhelm Wigbers
IPC分类号： C07C209/60
CPC分类号： C07C211/11 , C07C209/60 , Y02P20/582
摘要： The present invention relates to a process for preparing N,N-substituted 1,3-propanediamine by a) reacting secondary amine with acrolein at a temperature of from (−50) to 100° C. and a pressure of from 0.01 to 300 bar, and b) reacting the reaction mixture obtained in stage a) with hydrogen and ammonia in the presence of a hydrogenation catalyst at a temperature of from 40 to 400° C. and a pressure of from 1 to 400 bar, wherein the molar ratio of secondary amine to acrolein in stage a) is 2:1 or more and the hydrogenation catalyst used in stage b) comprises cobalt. In a preferred embodiment, acrolein which has been obtained from glycerol based on renewable raw materials is used. The invention further relates to the use of N,N-dimethyl-1,3-propanediamine (DMAPA) based on renewable raw materials as a feedstock for lubricant soaps and other detergents, coagulants, polymers and comb polymers. In a further preferred embodiment, stage b) is performed in the presence of water.
摘要翻译：本发明涉及一种通过以下步骤制备N，N-取代的1,3-丙二胺的方法：a）在（-50）至100℃的温度和0.01至300巴的压力下使仲胺与丙烯醛反应和b）在加氢催化剂存在下，在40〜400℃，压力为1〜400巴下，使a）中获得的反应混合物与氢气和氨反应，其中摩尔比阶段a）中的仲胺与丙烯醛的比例为2:1或更高，而阶段b）中使用的氢化催化剂包括钴。在优选的实施方式中，使用从基于可再生原料的甘油获得的丙烯醛。本发明还涉及基于可再生原料的N，N-二甲基-1,3-丙二胺（DMAPA）作为润滑剂皂和其它洗涤剂，凝结剂，聚合物和梳状聚合物的原料的用途。在另一优选实施方案中，步骤b）在水的存在下进行。

10. 发明申请

US20120071692A1 PROCESS FOR THE PREPARATION OF AROMATIC AMINES 审中-公开
标题翻译：制备芳香胺的方法
公开(公告)号：US20120071692A1
公开(公告)日：2012-03-22
申请号：US13234328
申请日：2011-09-16
申请人： SEBASTIAN AHRENS , Christoph Mueller , Axel Paul , Martin Ernst , Nadja Pollmer , Johann-Peter Melder , Thomas Heidemann , Joachim-Thierry Anders , Bram Willem Hoffer
发明人： SEBASTIAN AHRENS , Christoph Mueller , Axel Paul , Martin Ernst , Nadja Pollmer , Johann-Peter Melder , Thomas Heidemann , Joachim-Thierry Anders , Bram Willem Hoffer
IPC分类号： C07C209/18 , B01J21/06
CPC分类号： C07C209/18 , B01J21/066 , B01J23/44 , B01J35/002 , B01J35/026 , B01J35/08 , B01J35/1014 , B01J35/1038 , B01J37/0063 , B01J37/0072 , B01J37/0201 , Y02P20/582 , C07C211/45
摘要： A process for preparing an aromatic amine by reacting a corresponding aromatic alcohol with an aminating agent selected from the group consisting of ammonia, primary amines and secondary amines, in the presence of hydrogen and a catalyst molding, at a temperature of from 60-300°. The catalyst molding comprises Zr, Pd and Pt and has an annular tablet form with an external diameter in the range from 2-6 mm, a height in the range from 1-4 mm and an internal diameter of from 1-5 mm or a topologically equivalent form with the same volume. Catalyst moldings comprising Zr, Pd and Pt are also provided. The catalyst molding has an annular tablet form with an external diameter in the range from 3-6 mm, a height in the range from 1-4 mm and an internal diameter of from 2-5 mm or a topologically equivalent form.
摘要翻译：通过使相应的芳族醇与选自氨，伯胺和仲胺的胺化剂在氢和催化剂模塑的存在下，在60-300℃的温度下反应制备芳族胺的方法。催化剂成型包括Zr，Pd和Pt，并且具有环形片形式，其外径为2-6mm，高度为1-4mm，内径为1-5mm，或具有相同体积的拓扑等效形式。还提供了包含Zr，Pd和Pt的催化剂模制品。催化剂成型具有环形片形式，其外径为3-6mm，高度为1-4mm，内径为2-5mm或拓扑等效形式。

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