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31. 发明授权

US5132014A Apparatus and method for supercritical fluid extraction 失效
标题翻译：超临界流体萃取装置及方法
公开(公告)号：US5132014A
公开(公告)日：1992-07-21
申请号：US786752
申请日：1991-11-01
申请人： Robert W. Allington , Dale L. Clay , Daniel G. Jameson , Robin R. Winter
发明人： Robert W. Allington , Dale L. Clay , Daniel G. Jameson , Robin R. Winter
IPC分类号： A61B17/32 , A61B18/14 , B01D11/02 , B01D11/04 , F04B9/04 , F04B15/08 , F04B49/06 , F16K15/18 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/02 , G01N30/28 , G01N30/60 , G01N35/04 , G21F5/015
CPC分类号： G21F5/015 , B01D11/0203 , B01D11/0407 , F04B15/08 , F04B49/065 , F04B9/042 , F16K15/183 , G01F1/34 , G01N1/34 , G01N1/40 , G01N30/28 , A61B17/32 , A61B2018/126 , F04B2205/03 , F04B2205/05 , F04B2205/09 , F05B2230/41 , F05C2201/0493 , F05C2253/12 , G01N2001/4033 , G01N2001/4061 , G01N2030/6013 , G01N2035/0441 , G01N30/02 , Y10T29/53443
摘要： An apparatus for supercritical fluid extraction incorporates a removable extraction cartridge which in operation has insignificant pressure difference between its inside and outside walls. Because of the low pressure difference, the extraction cartridge need not have the strength to withstand significant pressure and can be made out of molded plastic for disposable use as well as stainless steel and machined plastic for reusability. The extraction cartridge can be removed and opened for sample access without the use of tools. The outside of the cartridge can be purged after it is installed in a heated high pressure vessel to remove contamination from its exterior.
摘要翻译：用于超临界流体萃取的装置包括可移除的提取筒，其在操作中在其内壁和外壁之间具有不显着的压力差。由于低压差，提取盒不需要具有承受显着压力的强度，并且可以由用于一次性使用的模制塑料以及用于可重复使用的不锈钢和机加工塑料制成。提取盒可以拆卸和打开，无需使用工具进行样品通道。在将其安装在加热的高压容器中以清除其外部的污染物之后，可将其清除。

32. 发明授权

US5084150A Selective high performance electrokinetic separations employing the surface of moving charged colloidal particles 失效
标题翻译：选择性高性能电动分离采用移动带电胶体颗粒的表面
公开(公告)号：US5084150A
公开(公告)日：1992-01-28
申请号：US566846
申请日：1990-08-14
申请人： Barry L. Karger , Aharon Cohen
发明人： Barry L. Karger , Aharon Cohen
IPC分类号： B01D15/08 , B01D57/02 , G01N30/02 , G01N30/28 , G01N30/58
CPC分类号： B01D57/02 , B01D15/08 , B01D15/3885 , G01N30/58 , G01N2030/285 , G01N30/02
摘要： An electrokinetic method for separating molecular species employs the surface of moving charged colloidal particles in a buffered dispersing medium, in a process which combines electrophoresis and a variant of chromatography in which the "stationary phase" surface moves. The colloidal particles have on their surface a material having the ability to interact selectively with the molecular species to be separated. The surface of the particles as originally formed may have such an ability, or the surface is modified to produce it. In one embodiment the colloidal particles are negatively charged and the surface-modifying materials are metal ions. In another embodiment the surface of the colloidal particles is modified by the incorporation of affinity groups. The analytes distribute themselves between the dispersing medium and the surface of the colloidal particles, resulting in analyte migration rates which are functions of the individual distribution equilibrium constants and the rate of colloidal particle migration. A capillary column for conducting the method includes surface-modified charged colloidal particles in a buffered dispersing medium.
摘要翻译：用于分离分子种类的电动方法在组合电泳和“固定相”表面移动的色谱变体的过程中使用缓冲分散介质中移动带电胶体颗粒的表面。胶体颗粒在其表面上具有能够与要分离的分子物质选择性相互作用的材料。最初形成的颗粒的表面可以具有这样的能力，或者表面被修饰以产生它。在一个实施方案中，胶体颗粒带负电荷，表面改性材料是金属离子。在另一个实施方案中，通过引入亲和基团来修饰胶体颗粒的表面。分析物分散在分散介质和胶体颗粒的表面之间，导致分析物迁移速率，其是单个分布平衡常数和胶体颗粒迁移速率的函数。用于进行该方法的毛细管柱包括缓冲分散介质中的表面改性的带电胶体颗粒。

33. 发明授权

US4971915A Simulated distillation of petroleum residues by capillary SFC 失效
标题翻译：通过毛细管SFC模拟石油残渣蒸馏
公开(公告)号：US4971915A
公开(公告)日：1990-11-20
申请号：US50755
申请日：1987-05-15
申请人： Herbert E. Schwartz , Robert G. Brownlee
发明人： Herbert E. Schwartz , Robert G. Brownlee
IPC分类号： G01N25/08 , G01N30/02 , G01N30/10 , G01N30/28 , G01N30/30 , G01N30/32 , G01N30/62 , G01N30/68 , G01N33/28
CPC分类号： G01N30/28 , G01N25/08 , G01N33/2823 , G01N2030/3007 , G01N2030/626 , G01N30/02 , G01N30/10 , G01N30/32 , G01N30/68 , Y10T436/21
摘要： A method is provided which can be used to accurately determine the boiling points of middle to heavy petroleum residues (AEBP of 250-1400 degrees F.) using temperatures well below their decomposition temperatures. The method involves the use of a capillary supercritical fluid chromatography apparatus, and consists of a calibration run followed by a measurement run. First, a temperature T1 (between 100 degrees C. and 180 degrees C.) is established in a gas chromatographic (GC) oven of the SFC apparatus, and that temperature is maintained throughout the method. Then a calibration run is performed on a calibration standard using a pressure program, and a calibration function is calculated using the known boiling points of the calibration standard. Then the test sample is run using the same pressure program and the calibration function is used to calculate the boiling point distribution of the test sample.
摘要翻译：提供了一种方法，可以使用远低于其分解温度的温度来精确测定中等重质石油残渣（AE-二氧化碳：250-1400°F）的沸点。该方法包括使用毛细管超临界流体色谱仪，并由校准运行和随后的测量运行组成。首先，在SFC装置的气相色谱（GC）烘箱中建立温度T1（在100摄氏度和180摄氏度之间），并且在整个方法中保持温度。然后使用压力程序对校准标准进行校准运行，并使用校准标准的已知沸点计算校准功能。然后使用相同的压力程序运行测试样品，并使用校准功能计算测试样品的沸点分布。

34. 发明授权

US4891120A Chromatographic separation device 失效
标题翻译：色谱分离装置
公开(公告)号：US4891120A
公开(公告)日：1990-01-02
申请号：US175389
申请日：1988-04-12
申请人： Rajinder S. Sethi , Jack Brettle , Christopher Lowe
发明人： Rajinder S. Sethi , Jack Brettle , Christopher Lowe
IPC分类号： G01N30/28 , G01N30/38 , G01N30/46 , G01N30/60
CPC分类号： G01N30/6086 , G01N2030/285 , G01N30/38 , G01N30/466 , G01N30/6082 , G01N30/6095
摘要： A chromatographic separation device comprises a body 2 of a semiconductor material which body has a longitudinal channel 1 formed in a surface thereof, the channel 1 being capable of containing a predetermined volume of a liquid or solid material for a chromatography test or separation procedure, the channel carrying at least one electrode 6 positioned intermediate the channel ends. The semiconductor body may additionally support an electronic or optical sensor 8 arranged in line with said channel 1 to provide an integrated detection system.
摘要翻译： PCT No.PCT / GB87 / 00393 Sec。 371日期：1988年4月12日 102（e）日期1988年4月12日PCT Filed 1987年6月8日PCT公布。公开号WO87 / 07953 日期为1987年12月30日.A色谱分离装置包括半导体材料的主体2，其主体在其表面形成有纵向通道1，通道1能够容纳预定体积的液体或固体材料，用于色谱测试或分离程序，承载位于通道末端的至少一个电极6的通道。半导体本体还可以支持与所述通道1成一直线排列的电子或光学传感器8，以提供集成的检测系统。

35. 发明授权

US4880543A Supercritical fluid chromatography packing material containing alumina 失效
标题翻译：含氧化铝的超临界流体色谱填充材料
公开(公告)号：US4880543A
公开(公告)日：1989-11-14
申请号：US214309
申请日：1988-07-01
申请人： Robinson P. Khosah , John W. Novak , Douglas G. Weaver , Karen R. Fraser-Milla , Richard R. Burr
发明人： Robinson P. Khosah , John W. Novak , Douglas G. Weaver , Karen R. Fraser-Milla , Richard R. Burr
IPC分类号： G01N30/28
CPC分类号： G01N30/482 , G01N30/28 , B01J2220/54
摘要： Disclosed is a method of separating organic or organometallic materials under supercritical fluid conditions, the method comprising the steps of providing a bed of packing material selected from a metal oxide/hydroxide support material having phsophorous-containing organic molecules bonded to reactive sites on said support material, alumina and alumina-containing mixtures. The materials are introduced to the bed and a fluid is added to the bed under supercritical fluid conditions. The fluid removes one of the materials from the bed.
摘要翻译：公开了一种在超临界流体条件下分离有机或有机金属材料的方法，所述方法包括以下步骤：提供选自金属氧化物/氢氧化物载体材料的填充床，所述金属氧化物/氢氧化物载体材料具有结合到所述载体材料上的反应性位点的含声孔的有机分子，氧化铝和含氧化铝的混合物。将材料引入床中，并在超临界流体条件下将流体加入到床中。流体从床中去除一种材料。

36. 发明授权

US4599115B1 失效
公开(公告)号：US4599115B1
公开(公告)日：1988-06-28
申请号：US63400684
申请日：1984-07-24
IPC分类号： B01D15/00 , B01D15/08 , B01D15/18 , B01D53/04 , C13K3/00 , C13K13/00 , G01N30/28 , G01N30/46
CPC分类号： B01D53/08 , B01D15/1828 , B01D53/04 , B01D53/0446 , B01D53/0454 , B01D2215/023 , B01D2215/024 , B01D2256/24 , B01D2259/404 , B01D2259/41 , C13K3/00 , C13K13/007

37. 发明授权

US4599115A Method for controlling simulated moving bed system 失效
标题翻译：控制模拟移动床系统的方法
公开(公告)号：US4599115A
公开(公告)日：1986-07-08
申请号：US634006
申请日：1984-07-24
申请人： Masao Ando , Masatake Tanimura
发明人： Masao Ando , Masatake Tanimura
IPC分类号： B01D15/00 , B01D15/08 , B01D15/18 , B01D53/04 , C13K3/00 , C13K13/00 , G01N30/28 , G01N30/46 , C13J1/06 , C13J1/08
CPC分类号： B01D53/08 , B01D15/1828 , B01D53/04 , B01D53/0454 , C13K13/007 , C13K3/00 , B01D2215/023 , B01D2215/024 , B01D2256/24 , B01D2259/404 , B01D2259/41 , B01D53/0446
摘要： A method is disclosed for controlling a simulated moving bed system of a type including at least four series-arranged beds each packed with a solid adsorbent, with the downstream end of each bed and the upstream end of the next succeeding bed being connected by conduits to form an endless loop, and in which a fluid is caused to circulate through the beds in one direction, a feed stock and a desorbent are introduced into the system while a raffinate and a sorbate are withdrawn from the system, and the positions of introduction and withdrawal of the four kinds of fluid are periodically shifted in the direction of the circulating fluid flow. In accordance with the invention, two or more circulating pumps, provided with variable speed controllers and pressure detectors for detecting the suction pressure of each of the circulating pumps, are disposed between two beds. The flow rates of three of the four fluids introduced into or withdrawn from the system are adjusted to predetermined values, and the flow rate of the other fluid is controlled in such a manner that the suction pressure of one of the circulating pumps or the average of the suction pressures of two or more of the circulating pumps is held constant, and a rotational speed of each of the circulating pumps is controlled independently so as to control the flow rate of the circulating fluid and to maintain the suction pressure of each circulating pump at a low level.
摘要翻译：公开了一种用于控制一种类型的模拟移动床系统的方法，其包括每个填充有固体吸附剂的至少四个串联布置的床，每个床的下游端和下一个后续床的上游端通过导管连接到形成无限循环，并且使流体在一个方向上循环通过床，将原料和解吸剂引入系统中，同时从系统中抽出萃余液和吸附物，并且引入和四种流体的排出周期性地沿循环流体的流动方向移动。根据本发明，设置有两个或更多个循环泵，其设置有用于检测每个循环泵的吸入压力的变速控制器和压力检测器，两个床之间。将引入或取出的四种流体中的三种流体的流量调节到预定值，并且以这样一种方式控制其它流体的流量，使得一种循环泵的吸入压力或平均值循环泵的两个或更多个的吸入压力保持恒定，并且独立地控制每个循环泵的转速，以便控制循环流体的流量并将每个循环泵的吸入压力保持在低水平

38. 发明授权

US2875144A Apparatus for electrochromatographic separation 失效
标题翻译：电色谱分离装置
公开(公告)号：US2875144A
公开(公告)日：1959-02-24
申请号：US55505255
申请日：1955-12-23
申请人： ARTHUR KARLER
发明人： ARTHUR KARLER
IPC分类号： G01N30/02 , G01N30/28 , G01N30/38
CPC分类号： G01N30/38 , G01N2030/285 , G01N30/02 , G01N27/44743 , G01N2030/0035

39. 发明授权

US11034721B2 Method for the reduction of viral titer in pharmaceuticals 有权
公开(公告)号：US11034721B2
公开(公告)日：2021-06-15
申请号：US15836683
申请日：2017-12-08
申请人： LONZA LTD
发明人： Paul Pease , Wilburn Miller , Jesse Cobb , Anthony Castagnaro , Andrew Harris
IPC分类号： B01D61/12 , G01N30/28 , C07K1/34 , C07K16/06 , B01D61/00 , B01D63/02 , C07K16/08 , B01D61/14 , B01D61/22 , C07K1/36
摘要： Disclosed are methods and devices for the optimization of virus removal from solutions. A method of filtering a process fluid comprising a product includes allowing some of the process fluid to flow from a first reservoir to a viral filter; adding a chase fluid to the process fluid in the first reservoir to form a composite fluid; and allowing the composite fluid to flow from the first reservoir to the viral filter to produce eluent. In some embodiments, flow of fluid across the viral filter is sufficient to avoid significant impairment to viral removal until a preselected event, occurs. In some embodiments, flow of fluid from the first reservoir across the viral filter is maintained in the absence of an interruption or slowing of flow of duration or magnitude sufficient to impair viral removal to a level below a log-reduction value of the viral filter.

40. 发明申请

US20210116429A1 SAMPLE ANALYSIS APPARATUS 有权
公开(公告)号：US20210116429A1
公开(公告)日：2021-04-22
申请号：US16606517
申请日：2017-04-25
申请人： SHIMADZU CORPORATION
发明人： Yukihiko KUDO
IPC分类号： G01N30/72 , G01N30/28
摘要： A response factor that is a signal strength ratio with respect to a reference compound for various compounds is previously stored in a response factor storage (22). When an operator instructs to estimate an analysis limit value, a measurement unit (1) performs GC-MS analysis on a sample containing the reference compound a plurality of times under control of an analysis controller (3). A signal strength calculator (23) obtains a signal strength value of the reference compound based on an analysis result of the measurement unit (1), a relative strength calculator (24) calculates a relative standard deviation from the plurality of measured signal strength values, and calculates the relative standard deviation of a target compound from the response factor of the target compound read from the response factor storage (22). An analysis limit value estimator (25) estimates a limit of detection (LOD) and the like from the relative standard deviation of the target compound by a known method, and displays the LOD on a display (6). Consequently, the analysis limit value can simply be obtained without actually measuring the target compound.

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