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31. 发明授权

US4137346A Flame retarding process for proteinaceous material 失效
标题翻译：蛋白质材料的阻燃过程
公开(公告)号：US4137346A
公开(公告)日：1979-01-30
申请号：US833841
申请日：1977-09-16
申请人： George M. Wagner
发明人： George M. Wagner
IPC分类号： D06M13/282 , D06M13/46 , D06M15/667 , D06M15/673 , C09K3/28 , B05D3/04
CPC分类号： D06M13/282 , D06M13/46 , D06M15/667 , D06M15/673 , Y10S428/921
摘要： An improved apparatus and process for imparting durable flame retardancy to textile materials wherein said material is impregnated with a solution having a poly(hydroxymethyl) phosphonium cation content of from about 10 to about 60 percent by weight, dried to a moisture content of from about 0 to about 8 percent, aerated by passing air through the dried material, cured by polymerizing the monomer on and in the textile material with exposure in an enclosed chamber to an atmosphere containing gaseous ammonia and thereafter contacting with water, the improvement comprising, impregnating said material with said solution containing poly(hydroxymethyl) phosphonium cation having a pH of from about 2 to about 9, and after contacting said material with said water, further exposing said material to an atmosphere containing gaseous ammonia.
摘要翻译：一种用于赋予纺织材料持久阻燃性的改进的装置和方法，其中所述材料用聚（羟甲基）鏻阳离子含量为约10至约60重量％的溶液浸渍，干燥至水分含量为约0 通过使空气通过干燥的材料进行充气，通过在封闭的室中暴露于含有气态氨的气氛中并随后与水接触来使单体聚集在纺织材料中和在纺织材料中进行固化，该改进包括浸渍所述材料所述溶液含有pH为约2至约9的聚（羟甲基）鏻阳离子，并且在使所述材料与所述水接触之后，将所述材料进一步暴露于含有气态氨的气氛中。

32. 发明授权

US4123574A Process for flame retarding cellulosics 失效
标题翻译：阻燃纤维素工艺
公开(公告)号：US4123574A
公开(公告)日：1978-10-31
申请号：US720030
申请日：1976-09-02
申请人： George M. Wagner
发明人： George M. Wagner
IPC分类号： D06M13/282 , D06M13/46 , D06M15/667 , D06M15/673 , C09K3/28 , B05D3/04
CPC分类号： D06M15/667 , D06M13/282 , D06M13/46 , D06M15/673 , Y10S428/921 , Y10T442/2689
摘要： An improved process for imparting durable flame retardancy to textile materials wherein said material is impregnated with a solution having a poly(hydroxymethyl) phosphonium cation content of from about 10 to about 60 percent by weight, dried to a moisture content of from about 0 to about 8 percent, aerated by passing air through the dried material, cured by polymerizing the monomer on and in the cellulose material with exposure in an enclosed chamber to an atmosphere containing gaseous ammonia and thereafter contacting with water, the improvement comprising, impregnating said material with a poly(hydroxymethyl) phosphonium cation containing solution and a basic catalyst, said solution having a pH of from about 2 to about 9, and after contacting said material with said water, further exposing said material to an atmosphere containing gaseous ammonia.
摘要翻译：用于赋予纺织材料持久阻燃性的改进方法，其中所述材料用聚（羟甲基）鏻阳离子含量为约10至约60重量％的溶液浸渍，干燥至水分含量为约0至约 8％，通过使空气通过干燥的材料进行充气，通过在封闭的室中暴露于含有气态氨的气氛中将纤维素材料上和在纤维素材料中聚合而固化，然后与水接触，改进之处在于，将所述材料浸渍在聚（羟甲基）鏻阳离子溶液和碱性催化剂，所述溶液的pH为约2至约9，并且在使所述材料与所述水接触后，将所述材料进一步暴露于含有气态氨的气氛中。

33. 发明授权

US4118590A Phosphorbetaines and process for making them 失效
标题翻译：磷酸甜菜碱及其制备方法
公开(公告)号：US4118590A
公开(公告)日：1978-10-03
申请号：US736092
申请日：1976-10-27
申请人： Hartfrid Vollmer , Klaus Hestermann
发明人： Hartfrid Vollmer , Klaus Hestermann
IPC分类号： C07F9/54 , D06M13/282 , D06M13/285 , D06M13/46
CPC分类号： D06M13/46 , C07F9/5407 , D06M13/282 , D06M13/285
摘要： Production of novel phosphobetaines of general formula I ##STR1## in which R.sup.1 and R.sup.2 each stand for organic groups having from 1 to 18 carbon atoms, and R.sup.1 or R.sup.2 may be identical with the substituent R, the substituent R being a radical of the general formula II ##STR2## in which R.sup.3 and R.sup.4 each stand for organic groups having from 1 to 18 carbon atoms, and/or hydrogen atoms, and R.sup.5 stands for a linear or branched alkyl group having from 1 to 4 carbon atoms, which may optionally have a halogen or hydroxylic group substituent attached thereto.
摘要翻译：制备通式I的新型磷酸甜菜碱，其中R 1和R 2各自代表具有1至18个碳原子的有机基团，并且R 1或R 2可以与取代基R相同，取代基R是通式II其中R 3和R 4各自代表具有1至18个碳原子的有机基团和/或氢原子，R 5代表具有1至4个碳原子的直链或支链烷基，其中可以任选地具有连接到其上的卤素或羟基取代基。

34. 发明授权

US3958061A Composition for making textiles flame-proof and its application 失效
标题翻译：制造纺织品防火组合物及其应用
公开(公告)号：US3958061A
公开(公告)日：1976-05-18
申请号：US360872
申请日：1973-05-16
申请人： Heinrich Singer , Sandor Csajagi
发明人： Heinrich Singer , Sandor Csajagi
IPC分类号： C09K21/12 , D06M13/02 , D06M13/244 , D06M13/282 , D06M13/292 , D06M13/295 , D06M13/322 , D06M13/402 , D06M13/432 , D06M15/423 , D06M15/667 , D06M101/12 , C09K3/28
CPC分类号： D06M15/667 , Y10S428/921 , Y10T442/2689
摘要： The present invention is concerned with the flame-proof finishing of textiles, and provide, a flame-proofing composition capable of giving stable emulsions in organic water-insoluble solvents. The composition comprises a salt of (a) guandine or salts thereof with weak acids, dicyandiamide or cyanamide and/or reaction products thereof with formaldehyde, and (b) acid mono and/or diphospheric acid esters of alcohols having 1 to 4 carbon atoms, the salt of (a) and (b) having in aqueous solution a pH value of more than 3.6, and (c) 3 to 15% by weight, based on the weight of the solid content of the composition, of compounds having the general formulae: ##EQU1## and/or ##EQU2## x being equal to 2 to 15, R.sup.1 representing a saturated alkyl group having 4 to 18 carbon atoms, and R.sup.2 representing hydrogen or a methyl group. An advantage of the composition is that it can be applied from organic water-insoluble solvents.
摘要翻译：本发明涉及纺织品的防火整理，并提供能够在有机水不溶性溶剂中提供稳定乳液的阻燃组合物。该组合物包含（a）胍或其盐与弱酸，双氰胺或氰胺和/或其与甲醛的反应产物的盐，和（b）具有1至4个碳原子的醇的酸单和/或二磷酸酯，（a）和（b）的盐在pH值大于3.6的水溶液中，和（c）基于组合物的固体含量的重量，3至15重量％的具有一般化合物的化合物式（I）1 R1（-O-C2H3R2）x-OO和/或R1（-O-C2H3R2）x-OOH P ANGLE（II）R1（-O-C2H3R2）x-OO x 等于2至15，R 1表示具有4至18个碳原子的饱和烷基，R 2表示氢或甲基。组合物的优点在于可以从有机水不溶性溶剂中应用。

35. 发明授权

US3956243A Process for flameproofing organic fibre material 失效
标题翻译：隔爆有机纤维材料的工艺
公开(公告)号：US3956243A
公开(公告)日：1976-05-11
申请号：US422819
申请日：1973-12-07
申请人： Rudolf Loss , Rene Berini , Armin Hiestand , Peter Hofmann , Hermann Nachbur
发明人： Rudolf Loss , Rene Berini , Armin Hiestand , Peter Hofmann , Hermann Nachbur
IPC分类号： C09K21/12 , C07C67/00 , C07C231/00 , C07C233/36 , D06M13/02 , D06M13/244 , D06M13/282 , D06M13/322 , D06M13/325 , D06M13/35 , D06M13/355 , D06M13/358 , D06M13/402 , D06M13/405 , D06M13/432 , D06M13/46 , D06M13/467 , D06M13/47 , D06M13/473 , D06M15/431 , D06M101/00 , D06M101/16 , D06M101/30 , D06M101/32 , D06M13/44 , C09K3/28
CPC分类号： D06M15/431 , Y10S260/24 , Y10S428/921 , Y10T428/31786 , Y10T428/31953
摘要： Composition for flameproofing organic fibre material which contains at least1. a tetrakis-(hydroxymethyl)-phosphonium compound, its self-condensation product or its condensation product with a reactive nitrogen compound2. an aliphatic amide or an imidazole or an imidazoline as agent for imparting a soft handle3. a methylolated amino groups containing 1,3,5-triazine and, optionally,4. an optionally methylolated and esterified derivative of a urea and, optionally,5. a low molecular amine.These compositions yield flameproof finishes paired with a soft handle especially on polyester-cotton blends.
摘要翻译：含有至少1种有机纤维材料的组合物。一种四（羟甲基） - 磷酸酯化合物，其自溶产物或其具有反应性硝酸化合物的冷凝产物2.一种酰胺或咪唑或咪唑啉作为代谢物一种软手柄3.一种含有1,3,5-三嗪的甲基化氨基酸组合物，有选择地，4.一种选择性甲基化和衍生的尿素衍生物，并且可选地，5.低分子量胺。

36. 发明授权

US3939228A Process for producing phosphazene compound 失效
标题翻译：磷腈化合物的制备方法
公开(公告)号：US3939228A
公开(公告)日：1976-02-17
申请号：US347833
申请日：1973-04-04
申请人： James T. F. Kao
发明人： James T. F. Kao
IPC分类号： C07F9/6581 , D06M13/282 , C07F9/15
CPC分类号： C07F9/65812 , D06M13/282
摘要： A process for manufacture of phosphazene compounds in a liquid aliphatic hydrocarbon reaction medium providing process advantages by reacting therein an alkali metal alkoxide, phenoxide or thiol derivative with a phosphonitrilic halide.
摘要翻译：在液体脂族烃反应介质中制造磷腈化合物的方法，其中通过使碱金属醇盐，酚盐或硫醇衍生物与磷酸三氢卤化物反应来提供工艺优点。

37. 发明授权

US3936585A Fire retarding textile materials 失效
标题翻译：阻燃纺织材料
公开(公告)号：US3936585A
公开(公告)日：1976-02-03
申请号：US422058
申请日：1973-12-05
申请人： Robert Bruce Leblanc , Destin A. Leblanc
发明人： Robert Bruce Leblanc , Destin A. Leblanc
IPC分类号： D06M13/44 , C07F9/50 , D06M13/02 , D06M13/244 , D06M13/282 , D06M13/285 , D06M13/292 , D06M13/298 , D06M13/322 , D06M13/402 , D06M13/432 , D06M15/667
CPC分类号： D06M13/285 , C07F9/50 , D06M15/667 , Y10S428/921 , Y10T428/31739
摘要： A water soluble product suitable for rendering textile materials fire retardant is produced by condensing a poly (.alpha.-hydroxyalkyl)phosphorus compound of the formula(RCHOH).sub.n (RCHR').sub.4.sub.-n P-Yor(RCHOH).sub.m (RCHR').sub.3.sub.-m Pand a nitrogen compound of the formula RNH.sub.2, HO--R"NH.sub.2 or ##EQU1## wherein R is hydrogen or alkyl of 1 to 3 carbon atoms,R' is OR or ##EQU2## R" is alkylene of 1 to 3 carbon atoms, Y is at least one anion selected from the group consisting of chloride, sulfate, phosphate, acetate and formate,n is an integer from 2 to 4, andm is an integer from 2 to 3,The phosphorus compound being present in about 0.5 to 6 times the molar amount of the nitrogen compound.Advantageously the phosphorus compound is a tetrakis(hydroxy-methyl)phosphonium salt or a tris(hydroxymethyl) phosphine and is present in about 1 to 3 times the nitrogen compound which is preferably ammonia. The condensation product, dissolved in water, is padded onto a fabric, preferably a polyester-cotton blend, which is thereafter dried and cured thermally and/or chemically. The fabrics are fire retardant even after multiple launderings.
摘要翻译：通过将式（RCHOH）n（RCHR'）4-n PY或（RCHOH）m（RCHR'）3-PY的聚（α-羟基烷基）磷化合物缩合成适于提供纺织材料阻燃剂的水溶性产品， mP和式RNH2，HO-R''NH2或R ANGLEN-R''NH2，R的氮化合物，其中R是氢或1至3个碳原子的烷基，R'是OR或RN ANGLE，R R “是1至3个碳原子的亚烷基，Y是至少一个选自氯化物，硫酸盐，磷酸盐，乙酸盐和甲酸盐的阴离子，N是从2到4的整数，M是从2到 3，磷化合物在0.5至6时间内出现了氮化合物的摩尔量。

38. 发明授权

US3930079A Method for fire-proofing treatment of fabrics composed of polyester and cellulosic filaments or fibers 失效
标题翻译：由聚酯纤维素纤维或纤维构成的织物的防火处理方法
公开(公告)号：US3930079A
公开(公告)日：1975-12-30
申请号：US53223974
申请日：1974-12-12
申请人： TEIJIN LTD
发明人： HASHIZUME ASTUO , TSUZUKI RYUICHIRO , MIZUSHIMA HARUO
IPC分类号： D06M13/02 , D06M13/244 , D06M13/282 , D06M13/292 , D06M13/298 , D06M13/322 , D06M13/35 , D06M13/355 , D06M13/402 , D06M15/431 , D06M101/00 , D06M101/02 , D06M101/06 , D06M101/08 , D06M101/16 , D06M101/30 , D06M101/32 , D06M13/28 , C09K3/28
CPC分类号： D06M15/431 , Y10T442/2689
摘要： A method for fire-proofing treatment of a fabric composed of polyester and cellulosic filaments of fibers, which comprises impregnating said fabric with the following treating agents: (1) a tetrakis-hydroxymethyl phosphonium compound, (2) methylolmelamine, (3) a specific thiocarbamic acid derivative, (4) a specific organic halogenated phosphorus compound and (5) a specific long-chain alkylethyleneurea, the amounts of the treating agents (1), (2), (3), (4) and (5), when designated a, b, c, d and e respectively, being as follows based on the total weight of a to e, A 40 TO 80 PERCENT, B 10 TO 50 PERCENT, C 5 TO 25 PERCENT, D 3 TO 10 PERCENT, E 1 TO 5 PERCENT AND SATISFYING THE FOLLOWING EQUATION

AND HEAT-SETTING THE IMPREGNATED FABRIC.
摘要翻译：一种由纤维聚酯纤维素纤维构成的织物的防火处理方法，其特征在于，包括以下处理剂浸渍所述织物：（1）四羟甲基鏻化合物，（2）羟甲基三聚氰胺，（3）特定的硫代氨基甲酸衍生物，（4）特定的有机卤化磷化合物和（5）特定的长链烷基亚乙基脲，处理剂（1），（2），（3），（4）和（5）当分别指定为a，b，c，d和e时，基于a至e的总重量，A = 40至80％，B = 10至50％，C = 5至25％，D = 3 至10％，E = 1至5％，并满足以下公式100（D％+ E％）4 15 A％+ B％+ C％和加热印花织物。

39. 发明授权

US3929940A Halogen-containing phosphoric acid esters 失效
标题翻译：含卤素的磷酸酯
公开(公告)号：US3929940A
公开(公告)日：1975-12-30
申请号：US44792174
申请日：1974-03-04
申请人： SANDOZ AG
发明人： MAYERHOEFER HORST , MUELLER WOLFGANG , SOLLBERGER URS , WOLF RAINER
IPC分类号： C08K5/00 , C07F9/12 , C08K5/52 , C08K5/523 , C08L7/00 , C08L21/00 , C08L23/00 , C08L33/00 , C08L33/02 , C08L51/00 , C08L51/02 , C08L67/00 , C08L77/00 , C08L101/00 , D06M13/02 , D06M13/244 , D06M13/282 , D06M13/292 , D06M13/298 , C07F9/09 , C08K5/53
CPC分类号： C07F9/12 , C08K5/523
摘要： The present invention concerns novel phosphoric acid esters of the formula:

WHEREIN EACH R, is independently, a radical of formula -CH2-C(CH2Hal)3, or

EACH Hal is independently, chlorine or bromine, N IS O or an integer 1, 2, 3 or 4 M IS AN INTEGER 1, 2, 3, 4 OR 5 AND THE MOLECULE CONTAINS AT LEAST EIGHT BROMINE ATOMS. The compounds are useful flame retardants for, e.g., flammable plastics materials.
摘要翻译：本发明涉及下式的新型磷酸酯：

40. 发明授权

US3877974A Flame retardants for blends of natural and synthetic fibers 失效
标题翻译：天然和合成纤维混合物的阻燃剂
公开(公告)号：US3877974A
公开(公告)日：1975-04-15
申请号：US33073172
申请日：1972-10-25
申请人： WHITE CHEMICAL CORP
发明人： MISCHUTIN VLADIMIR
IPC分类号： C08J7/04 , C08K13/02 , D06M11/20 , D06M11/45 , D06M11/46 , D06M11/47 , D06M11/79 , D06M13/02 , D06M13/08 , D06M13/152 , D06M13/21 , D06M13/244 , D06M13/248 , D06M13/256 , D06M13/282 , D06M13/292 , D06M13/298 , D06M13/325 , D06M13/335 , D06M13/338 , D06M15/263 , D06M15/693 , C09K3/28 , C09D5/18
CPC分类号： D06M13/338 , C08K13/02 , D06M11/20 , D06M11/45 , D06M11/46 , D06M11/47 , D06M11/79 , D06M13/02 , D06M13/08 , D06M13/152 , D06M13/21 , D06M13/292 , D06M15/263 , D06M15/693 , D06M2101/06 , D06M2101/32 , D06M2200/30 , Y10S428/921 , Y10T442/2713
摘要： A process for rendering synthetic materials, of synthetic fibers or mixtures of the same flame resistant which entails employing water insoluble flame retardant agents which are treated as colorless pigments, reduced to extremely finely divided condition, suspended in latex medium and applied as such or as part of a dispersed dye paste to the fabric, dried and set in place. The active flame retardant agents are brominated organic chemical compounds, and reduced to a fine state of subdivision, preferably under two microns, average particle diameter, which compound is supported in an aqueous suspension with a colloidal protective agent, and thus, is in a form for blending in a binder, plastic resin latex, so that when the composition is dried and cured in place on the fabric, a very useful retardant effect is obtained which is durable to laundering and dry cleaning, and the hand of the fabric is preserved.
摘要翻译：制造合成纤维或合成纤维或具有相同阻燃性的混合物的方法，其需要使用被视为无色颜料的水不溶性阻燃剂，被还原成极细的状态，悬浮在胶乳介质中并作为部分施用将分散的染料糊剂涂布到织物上，干燥并固化。

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