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31. 发明申请

US20040127691A1 Process for surface functionalsation of polymeric substrates using diaryl carbenes as reactive intermediates 失效
标题翻译：使用二芳基卡宾作为反应性中间体的聚合物基材的表面官能化方法
公开(公告)号：US20040127691A1
公开(公告)日：2004-07-01
申请号：US10741288
申请日：2003-12-19
发明人： Mark Gerard Moloney , Warren Ebenezer , Karim Awenat
IPC分类号： C07C245/20
CPC分类号： C08J7/12 , C07C245/14 , C07C245/20 , D06P1/008 , D06P5/22
摘要： An alternative technique whereby highly reactive carbene or nitrene species are generated from inert precursors under less harsh photolytic, and sometimes thermolytic, conditions has also been investigated for application to dyeing and other surface modifying processes of various natural and synthetic polymers. The chemistry of cargenes and nitrenes is well documented, and these reactive entities are known to form covalent bonds with many types of functional group groups. The application of these species to the surface modification or organic solids using different approaches both for the generation of the required carbenes or nitrenes, and for their reaction with the solid surface has been reported. Interestingly, although nitrenes (often generated from an azide or sulfonylazide precursor under photolytic or thermolytic conditions) are more stable, and therefore less reactive, than their carbene analogues, they have used much more widely for the dyeing of polymeric substrates.
摘要翻译：一种替代技术，其中在较不苛刻的光解作用下，惰性前体产生高反应性的卡宾或者腈类物质，并且有时热解条件也被研究用于各种天然和合成聚合物的染色和其它表面改性方法。已证明了子基和亚硝基的化学性质，已知这些反应性实体与许多类型的官能团组形成共价键。已经报道了这些物质对于表面改性或有机固体的应用，使用不同的方法来产生所需的卡宾或腈，以及它们与固体表面的反应。有趣的是，虽然硝化物（通常在光解或热解条件下由叠氮化物或磺酰基叠氮化物前体产生）比它们的卡宾类似物更稳定，因此反应性更低，但它们对聚合物基材的染色使用更广泛。

32. 发明授权

US06703345B2 Diazonium salt and heat-sensitive recording material 失效
标题翻译：重氮盐和热敏记录材料
公开(公告)号：US06703345B2
公开(公告)日：2004-03-09
申请号：US10132292
申请日：2002-04-26
申请人： Kimiatsu Nomura , Tatsuo Kawabuchi , Hisato Nagase , Satoshi Higuchi , Kimi Ikeda , Yoshihiro Jinbo
发明人： Kimiatsu Nomura , Tatsuo Kawabuchi , Hisato Nagase , Satoshi Higuchi , Kimi Ikeda , Yoshihiro Jinbo
IPC分类号： B41M526
CPC分类号： G03C1/002 , B41M5/287 , C07C245/20 , G03C1/54
摘要： The present invention provides a diazonium salt represented by the following general formula (1) wherein R1 represents a branched alkyl group; R2 and R3 separately represent an alkyl group and may bond to each other to form a ring; R4, R5, and R6 separately represent a hydrogen atom, an alkyl group, or an aryl group and R4 and R5 may bond to each other to form a ring; and X− represents an anion and a heat-sensitive recording material comprising a heat-sensitive recording layer including the diazonium salt and a coupler. General formula (1)
摘要翻译：本发明提供由以下通式（1）表示的重氮盐，其中R 1表示支链烷基; R 2和R 3分别表示烷基并且可以彼此键合形成环; R 4，R 5和R 6分别表示氢原子，烷基或芳基，R 4和R 5可以彼此键合形成环; 和X'表示阴离子和热敏记录材料，其包含包含重氮盐和偶合剂的热敏记录层。通式（1）

33. 发明申请

US20040002481A1 Novel 4-dedimethylaminotetracycline derivatives 失效
标题翻译：新型4-脱二甲基氨基四环素衍生物
公开(公告)号：US20040002481A1
公开(公告)日：2004-01-01
申请号：US10458076
申请日：2003-06-10
申请人： CollaGenex Pharmaceuticals, Inc.
发明人： Robert Ashley , Joseph J. Hlavka
IPC分类号： A61K031/65 , C07C237/26
CPC分类号： C07D295/13 , C07C235/82 , C07C237/26 , C07C245/20 , C07C247/18 , C07C329/20 , C07C2603/46 , Y10S514/825 , Y10S514/866 , Y10S514/903
摘要： The present invention provides new chemically modified 4-dedimethylaminotetracycline compounds that can be substituted with aryl, alkenyl, or alkynyl groups. The 7, 8, and/or 9 positions and methods for preparing such compounds. Other tetracycline compounds include the 4-dedimethylaminotetracycline derivatives with an oxime group, NH-Alkyl, or N-NH-Alkyl group substituted at the C4 position as well as C2 Mannich derivatives. The present invention also provides a method of treating a mammal suffering from conditions or diseases by administering to the mammal an effective amount of the new chemically modified tetracycline compounds.
摘要翻译：本发明提供可以被芳基，烯基或炔基取代的新的化学修饰的4-脱二甲基氨基四环素化合物。 7,8和/或9位及其制备方法。其他四环素化合物包括具有肟基的4-脱二氨基四环素衍生物，在C4位被取代的NH-烷基或N-NH-烷基以及C2曼尼希衍生物。本发明还提供了通过向哺乳动物施用有效量的新的化学修饰的四环素化合物来治疗患有病症或疾病的哺乳动物的方法。

34. 发明授权

US06239289B1 O-(perfluoroalkyl)dibenzofuranium salt derivatives, intermediates for the preparation of the same, process for the preparation of the intermediates, perfluoroalkylating agents, and process for perfluoroalkylation 失效
标题翻译： O-（全氟烷基）二苯并anium盐衍生物，其制备中间体，制备中间体的方法，全氟烷基化剂，以及全氟烷基化方法
公开(公告)号：US06239289B1
公开(公告)日：2001-05-29
申请号：US09463706
申请日：2000-02-15
申请人： Teruo Umemoto , Kenji Adachi , Sumi Ishihara
发明人： Teruo Umemoto , Kenji Adachi , Sumi Ishihara
IPC分类号： C07C21145
CPC分类号： C07D307/91 , C07C217/80 , C07C245/20
摘要： O-(perfluoroalkyl)dibenzofuranium salt derivatives represented by the following general formula (1), (wherein Rf in said general formula (1) is a C1-10 perfluoroalkyl group and X− is a conjugate base of a Brönsted acid). Intermediates for preparation of the derivatives, a preparation method thereof, perfluoroalkylating agents comprising the said derivatives and the said preparation intermediates, and a perfluoroalkylating method.
摘要翻译：由下列通式（1）表示的O-（全氟烷基）二苯并ur盐衍生物（其中，所述通式（1）中的Rf为C1-10全氟烷基，X为布朗斯台德酸的共轭碱）。用于制备衍生物的中间体，其制备方法，包含所述衍生物的全氟烷基化剂和所述制备中间体，以及全氟烷基化方法。

35. 发明授权

US06229055B1 Synthesis of fluorinated xanthene derivatives 有权
标题翻译：氟化呫吨衍生物的合成
公开(公告)号：US06229055B1
公开(公告)日：2001-05-08
申请号：US09632251
申请日：2000-08-03
申请人： Dieter H. Klaubert , Kyle R. Gee
发明人： Dieter H. Klaubert , Kyle R. Gee
IPC分类号： C07C3910
CPC分类号： C09B11/00 , C07C37/055 , C07C41/18 , C07C201/08 , C07C201/12 , C07C205/26 , C07C205/37 , C07C209/10 , C07C213/02 , C07C213/08 , C07C245/20 , C07D311/82 , C09B11/24 , G01N1/30 , Y10S430/116 , Y10S430/126 , C07C39/245 , C07C211/52 , C07C217/84 , C07C215/76 , C07C43/225
摘要： Facile syntheses for fluorinated resorcinol and aminophenol derivatives are provided that yield isomer-free products in good yield. These novel methods use generally available precursors and standard laboratory reagents and equipment to reproducibly produce these synthetically useful reagents in relatively large quantities. The resulting fluorinated resorcinols and aniinophenols possess utility in the preparation of fluorinated fluorescein and rhodol dyes.
摘要翻译：提供氟化间苯二酚和氨基苯酚衍生物的简便合成，其以良好的收率产生无异构体的产物。这些新颖的方法通常使用可用的前体和标准实验室试剂和设备以相当大的量重复地生产这些合成有用的试剂。得到的氟化间苯二酚和苯醌具有用于制备氟化荧光素和罗丹明染料。

36. 发明授权

US5204448A Chelating agents for attaching metal ions to proteins 失效
标题翻译：将金属离子连接到蛋白质的螯合剂
公开(公告)号：US5204448A
公开(公告)日：1993-04-20
申请号：US358917
申请日：1989-05-26
申请人： Ramaswamy Subramanian
发明人： Ramaswamy Subramanian
IPC分类号： G01N33/532 , A61K39/395 , A61K47/48 , A61K51/00 , A61K51/08 , A61K51/10 , C07B59/00 , C07C229/04 , C07C229/16 , C07C233/43 , C07C237/10 , C07C245/20 , C07C331/28 , C07D211/56 , C07F1/08 , C07F5/00 , C07F13/00 , C07K14/00 , C07K16/00 , C09K3/00 , G01N33/533 , G01N33/534 , G01N33/536
CPC分类号： C07B59/008 , A61K47/59 , A61K47/595 , A61K47/643 , A61K47/6885 , A61K47/6887 , A61K51/081 , A61K51/088 , A61K51/1093 , A61K2123/00 , C07B59/001 , C07B59/002 , C07C233/43 , C07C245/20 , C07D211/56 , C07F5/003 , C07F13/005 , G01N33/533 , G01N33/534
摘要： A new series of bifunctional chelating agents useful for attaching metal ions to proteins, polypeptides and other polymers and methods for their preparation are described. These reagents are unique in their ability to bind a variety of metal ions and to yield a high metal ion concentration per protein molecule. Using these methods polymeric analogs of these bifunctional chelating agents called Starburst ligands can also be obtained. Protein metal chelates thus obtained will have useful radiophysical, chemical, fluorescent, photochemical and magnetic properties suitable for biomedical applications.
摘要翻译：描述了一系列用于将金属离子附着到蛋白质，多肽和其它聚合物上的双功能螯合剂及其制备方法。这些试剂在结合各种金属离子的能力方面是独一无二的，并且每个蛋白质分子产生高的金属离子浓度。使用这些方法也可以获得称为Starburst配体的这些双功能螯合剂的聚合物类似物。如此获得的蛋白质金属螯合物将具有适用于生物医学应用的有用的放射性物理，化学，荧光，光化学和磁性。

37. 发明授权

US4246171A Continuous diazotization process, wherein the rate of addition of inorganic nitrite is automatically controlled by polarovoltric means 失效
标题翻译：连续重氮化方法，其中无机亚硝酸盐的添加速率通过极差方法自动控制
公开(公告)号：US4246171A
公开(公告)日：1981-01-20
申请号：US940414
申请日：1978-09-07
申请人： Alexander Hamilton , Colin Nelson
发明人： Alexander Hamilton , Colin Nelson
IPC分类号： C07C113/04
CPC分类号： C07C245/20
摘要： Automatically controlled continuous process for the diazotization or tetrazotization of aromatic amines in which the rate of addition of the inorganic nitrite is controlled by a polarovoltric method. The process comprises adding regularly and continuously to a reactor an aqueous slurry or solution of the amine containing sufficient acid for the diazotization process and simultaneously adding to the reactor a solution of an inorganic nitrite at a rate which is automatically regulated by a polarovoltric controller to ensure that a pre-selected concentration of unreacted nitrous acid is maintained in the reactor throughout the whole period of the reaction.
摘要翻译：用于芳族胺的重氮化或四唑化的自动控制连续方法，其中通过极性方法控制无机亚硝酸盐的加入速率。该方法包括向反应器中定期和连续地向反应器中加入含有足够酸的胺的含水浆液或溶液进行重氮化过程，同时向无机亚硝酸盐溶液中加入无定形亚硝酸盐溶液，该速率由极性控制器自动调节，以确保在反应器的整个整个周期内，在反应器中保持未反应的亚硝酸的预先选择的浓度。

38. 发明授权

US4005151A Process for producing polyhalogenated phenols 失效
标题翻译：生产多卤代酚的方法
公开(公告)号：US4005151A
公开(公告)日：1977-01-25
申请号：US555627
申请日：1975-03-05
申请人： Masataka Wataya , Nobuo Onodera , Shosuke Imamura
发明人： Masataka Wataya , Nobuo Onodera , Shosuke Imamura
IPC分类号： C07C27/00 , C07C37/045 , C07C37/05 , C07C39/27 , C07C67/00 , C07C39/30 , C07C39/32
CPC分类号： C07C37/045 , C07C245/20
摘要： A process for producing polyhalogenated phenol by mixing a polyhalogenated aniline with an aqueous sulfuric acid solution to obtain a suspension of fine particles of polyhalogenated aniline sulfate having the particle size of 50 .mu. or less, diazotizing the polyhalogenated aniline sulfate to obtain polyhalogenate benzenediazonium sulfate, hydrolyzing the resulting benzenediazonium sulfate by heating it as such, recycling to the diazotization step the aqueous sulfuric acid solution from which the desired polyhalogenated phenol has been separated.
摘要翻译：通过将多卤代苯胺与硫酸水溶液混合，得到粒径为50μm以下的多卤代苯胺硫酸盐微粒的悬浮液，重氮化多卤代苯胺硫酸盐，得到多卤代苯二氮硫酸盐，水解通过将其加热得到的重氮化硫酸盐，将所需的多卤代酚分离出来的硫酸水溶液再循环至重氮化步骤。

39. 发明授权

US3914325A Method for preparing phenol compounds using mixed acid system 失效
标题翻译：使用混合酸体系制备酚类化合物的方法
公开(公告)号：US3914325A
公开(公告)日：1975-10-21
申请号：US37224473
申请日：1973-06-21
申请人： OLIN CORP
发明人： GAVIN DAVID F , TOBIN JOHN H
IPC分类号： C07C27/00 , C07C37/045 , C07C37/05 , C07C67/00 , C07C201/00 , C07C205/22 , C07C39/24
CPC分类号： C07C37/045 , C07C245/20 , C07C39/27 , C07C39/24
摘要： This invention relates to a novel integrated route to selected phenols by diazotization of selected aminobenzene compounds in a mixed phosphoric-sulfuric acid system and subsequent decomposition of the diazonium salt.
摘要翻译：本发明涉及一种通过在混合的磷酸 - 硫酸体系中重氮化选择的氨基苯化合物并随后分解重氮盐来选择的酚类的新途径。

40. 发明授权

US3107057A Process and apparatus for the production of parts from synthetic materials of any kind reinforced with fibres 失效
标题翻译：用纤维增强的任何一种合成材料生产零件的工艺和设备
公开(公告)号：US3107057A
公开(公告)日：1963-10-15
申请号：US61045756
申请日：1956-09-18
申请人： CIMEX TRUST
发明人： HUGO HANUSCH
IPC分类号： A61C3/14 , B05B7/14 , B29C41/36 , B29C70/30 , C09B43/44 , C09B67/00
CPC分类号： A61C3/14 , B05B7/1495 , B29C41/365 , B29C70/305 , C07C245/20 , C09B43/44 , C09B67/00 , Y10S239/08

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