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31. 发明授权

US07531610B2 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US07531610B2
公开(公告)日：2009-05-12
申请号：US12010586
申请日：2008-01-28
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C08F16/24 , C07C309/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1:
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是RF01为单键或C1-6二价全氟有机基团，RF02为C1-6二价全氟有机基团，n为0或1：

32. 发明申请

US20080146841A1 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US20080146841A1
公开(公告)日：2008-06-19
申请号：US12010586
申请日：2008-01-28
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C07C309/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1:
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是R < > F01 是单键或C 1-6 - 二价全氟有机基团，R F02是C 1-6烷基，二价全氟有机基团，n为0或1：

33. 发明授权

US07667083B2 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US07667083B2
公开(公告)日：2010-02-23
申请号：US12410524
申请日：2009-03-25
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C07C17/00 , C07C19/00 , C07C21/00 , C07C23/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1.
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是RF01为单键或C1-6二价全氟有机基团，RF02为C1-6二价全氟有机基团，n为0或1。

34. 发明授权

US08198394B2 Process for producing electrolyte material for polymer electrolyte fuel cells, and membrane-electrode assembly for polymer electrolyte fuel cells 失效
标题翻译：用于生产用于聚合物电解质燃料电池的电解质材料的方法和用于聚合物电解质燃料电池的膜 - 电极组件
公开(公告)号：US08198394B2
公开(公告)日：2012-06-12
申请号：US12430961
申请日：2009-04-28
申请人： Jun-ichi Tayanagi , Atsushi Watakabe , Susumu Saito , Katsuya Ueno
发明人： Jun-ichi Tayanagi , Atsushi Watakabe , Susumu Saito , Katsuya Ueno
IPC分类号： C08J5/20
CPC分类号： C08J5/225 , C08F8/12 , C08F2800/10 , C08F2800/20 , C08J2327/12 , H01M8/1004 , H01M8/1023 , H01M8/1039 , Y02P70/56 , C08F234/02 , C08F216/1408 , C08F214/26 , C08F224/00
摘要： A membrane-electrode assembly for polymer electrolyte fuel cells which is excellent in water repellency and gas diffusivity and which exhibits a high output power density, can be obtained by using, as an electrolyte material for polymer electrolyte fuel cells, a fluoropolymer obtained by contacting a fluoropolymer which is excellent in gas diffusivity and which has alicyclic structures in its main chain and further has sulfonic acid groups, with fluorine gas for fluorination to increase water repellency and stabilize the molecule ends. The above fluoropolymer is preferably made of a copolymer comprising repeating units based on the following monomer A and repeating units based on the following monomer B (wherein Y is a fluorine atom or a trifluoromethyl group, m is an integer of from 0 to 3, p is 0 or 1, and n is an integer of from 1 to 12): Monomer A: A perfluoromonomer which gives a polymer having repeating units containing cyclic structures in its main chain by radical polymerization Monomer B: CF2═CF—(OCF2CFY)m-0p-(CF2)n—SO3H.
摘要翻译：作为聚合物电解质型燃料电池的电解质材料，可以通过使用通过使聚合物电解质燃料电池接触而获得的含氟聚合物，获得具有优异的防水性和气体扩散性并且显示出高功率密度的聚合物电解质燃料电池用膜电极组件含氟聚合物，其气体扩散性优异，并且在其主链中具有脂环结构并且还具有磺酸基，氟气用于氟化以增加拒水性并稳定分子末端。上述含氟聚合物优选由包含以下单体A的重复单元和基于以下单体B的重复单元（其中Y为氟原子或三氟甲基，m为0〜3的整数，p 是0或1，n为1至12的整数）：单体A：通过自由基聚合在其主链中产生含有环状结构的重复单元的聚合物的全氟单体单体B：CF 2 = CF-（OCF 2 CF 3）m -Op-（CF2）n-SO3H。

35. 发明申请

US20110071272A1 FLUOROSULFONYL GROUP-CONTAINING MONOMER AND ITS POLYMER, AND SULFONIC ACID GROUP-CONTAINING POLYMER 有权
标题翻译：含氟基团的单体及其聚合物和含有磺酸基团的聚合物
公开(公告)号：US20110071272A1
公开(公告)日：2011-03-24
申请号：US12955443
申请日：2010-11-29
申请人： Atsushi WATAKABE , Hiromasa Yamamoto , Masao Iwaya , Susumu Saito
发明人： Atsushi WATAKABE , Hiromasa Yamamoto , Masao Iwaya , Susumu Saito
IPC分类号： C08G75/14
CPC分类号： C07D317/42 , C08G75/23
摘要： A fluorosulfonyl group-containing monomer having a high polymerization reactivity and plural fluorosulfonyl groups, a fluorosulfonyl group-containing polymer and a sulfonic acid group-containing polymer, obtained by using the monomer.
摘要翻译：具有高聚合反应性的氟磺酰基的单体和多个氟磺酰基，含氟磺酰基的聚合物和含磺酸基的聚合物通过使用该单体获得。

36. 发明授权

US07790817B2 Process for producing fluoropolymer 失效
标题翻译：生产含氟聚合物的方法
公开(公告)号：US07790817B2
公开(公告)日：2010-09-07
申请号：US11618088
申请日：2006-12-29
申请人： Atsushi Watakabe , Susumu Saito , Adam Luke Safir
发明人： Atsushi Watakabe , Susumu Saito , Adam Luke Safir
IPC分类号： C08F2/00
CPC分类号： C08F214/182 , C08F214/26 , C08F214/262
摘要： Provided is a process for producing a fluoropolymer containing repeating units based on a fluoromonomer represented by the following formula (m) in an amount of from 5 to 50 mol % based on the entire repeating units in the polymer by polymerization reaction of tetrafluoroethylene and the fluoromonomer, wherein the polymerization reaction is carried out by continuously charging the reactor with tetrafluoroethylene and the fluoromonomer: wherein ml is an integer of from 1 to 6. Also provided is an electrolyte material for an electrolyte fuel cell which can be operated at a high temperature to obtain a high output, wherein the electrolyte material contains the fluoropolymer produced by the process.
摘要翻译：本发明提供一种含氟聚合物的制造方法，所述含氟聚合物含有基于由下式（m）表示的含氟单体的重复单元，所述重复单元的量为5-40摩尔％，相对于聚合物中的全部重复单元，四氟乙烯与含氟单体的聚合反应其中聚合反应是通过用四氟乙烯和含氟单体连续地加入反应器来进行的：其中，ml是1至6的整数。还提供了一种用于电解质燃料电池的电解质材料，其可以在高温至获得高产量，其中电解质材料含有通过该方法生产的含氟聚合物。

37. 发明授权

US07557178B2 Process for producing electrolyte material for polymer electrolyte fuel cells, and membrane-electrode assembly for polymer electrolyte fuel cells 有权
标题翻译：用于生产用于聚合物电解质燃料电池的电解质材料的方法和用于聚合物电解质燃料电池的膜 - 电极组件
公开(公告)号：US07557178B2
公开(公告)日：2009-07-07
申请号：US11183748
申请日：2005-07-19
申请人： Jun-ichi Tayanagi , Atsushi Watakabe , Susumu Saito , Katsuya Ueno
发明人： Jun-ichi Tayanagi , Atsushi Watakabe , Susumu Saito , Katsuya Ueno
IPC分类号： C08J5/20
CPC分类号： C08J5/225 , C08F8/12 , C08F2800/10 , C08F2800/20 , C08J2327/12 , H01M8/1004 , H01M8/1023 , H01M8/1039 , Y02P70/56 , C08F234/02 , C08F216/1408 , C08F214/26 , C08F224/00
摘要： A membrane-electrode assembly for polymer electrolyte fuel cells which is excellent in water repellency and gas diffusivity and which exhibits a high output power density, can be obtained by using, as an electrolyte material for polymer electrolyte fuel cells, a fluoropolymer obtained by contacting a fluoropolymer which is excellent in gas diffusivity and which has alicyclic structures in its main chain and further has sulfonic acid groups, with fluorine gas for fluorination to increase water repellency and stabilize the molecule ends. The above fluoropolymer is preferably made of a copolymer comprising repeating units based on the following monomer A and repeating units based on the following monomer B (wherein Y is a fluorine atom or a trifluoromethyl group, m is an integer of from 0 to 3, p is 0 or 1, and n is an integer of from 1 to 12): Monomer A: A perfluoromonomer which gives a polymer having repeating units containing cyclic structures in its main chain by radical polymerization Monomer B: CF2═CF—(OCF2CFY)m—Op—(CF2)n—SO3H.
摘要翻译：作为聚合物电解质型燃料电池的电解质材料，可以通过使用通过使聚合物电解质燃料电池接触而获得的含氟聚合物，获得具有优异的防水性和气体扩散性并且显示出高功率密度的聚合物电解质燃料电池用膜电极组件含氟聚合物，其气体扩散性优异，并且在其主链中具有脂环结构并且还具有磺酸基，氟气用于氟化以增加拒水性并稳定分子末端。上述含氟聚合物优选由包含以下单体A的重复单元和基于以下单体B的重复单元（其中Y为氟原子或三氟甲基，m为0〜3的整数，p 是0或1，n是1至12的整数）：单体A：通过自由基聚合在其主链中产生具有含有环状结构的重复单元的聚合物的全氟单体单体B：CF 2 -CF-（OCF 2 CF 3）m -Op-（CF2）n-SO3H。

38. 发明授权

US07872123B2 Process of making α-aminooxyketone/α-aminooxyaldehyde and α-hydroxyketone/α-hydroxyaldehyde compounds and a process making reaction products from cyclic α,β-unsaturated ketone substrates and nitroso substrates 有权
标题翻译：制备α-氨基氧基酮/α-氨基氧醛和α-羟基酮/α-羟基醛化合物的方法和由环状α，β-不饱和酮基质和亚硝基底物制备反应产物的方法
公开(公告)号：US07872123B2
公开(公告)日：2011-01-18
申请号：US11506590
申请日：2006-08-18
申请人： Norie Momiyama , Hiromi Torii , Susumu Saito , Hisashi Yamamoto , Yuhei Yamamoto
发明人： Norie Momiyama , Hiromi Torii , Susumu Saito , Hisashi Yamamoto , Yuhei Yamamoto
IPC分类号： C07D265/02
CPC分类号： C07C291/04 , C07C2601/14 , C07D207/16 , C07D211/74 , C07D309/30 , C07D317/72 , C07D403/04
摘要： The present invention is directed to a process of making α-aminooxyketone and α-hydroxyketone compounds. The synthetic pathway involves reacting an aldehyde or ketone substrate and a nitroso substrate in the presence of a catalyst of the formula (IV): wherein Xa-Xc represent independently nitrogen, carbon, oxygen or sulfur and Z represents a 4 to 10-membered ring with or without a substituent and optionally a further step to convert the α-aminooxyketone compound formed to the α-hydroxyketone compound which results in α-aminooxyketone and α-hydroxyketone compounds with high enantioselectivity and high purity. The present invention is also directed to a catalytic asymmetric O-nitroso Aldol/Michael reaction involving a cyclic α,β-unsaturated ketone substrate and a nitroso substrate. This methodology involves reacting the cyclic α,β-unsaturated ketone substrate and the nitroso substrate in the presence of a proline-based catalyst, to provide a heterocyclic product.
摘要翻译：本发明涉及制备α-氨基氧基酮和α-羟基酮化合物的方法。合成途径包括在式（Ⅳ）催化剂存在下使醛或酮底物和亚硝基底物反应：其中Xa-Xc独立地表示氮，碳，氧或硫，Z代表4至10元环具有或不具有取代基，以及任选的另一步骤是将形成的α-氨基氧基酮化合物转化成α-羟基酮化合物，得到具有高对映选择性和高纯度的α-氨基氧基酮和α-羟基酮化合物。本发明还涉及涉及环状α，β-不饱和酮底物和亚硝基底物的催化不对称O-亚硝基醇/迈克尔反应。该方法包括在脯氨酸催化剂存在下使环状α，β-不饱和酮底物和亚硝基质反应，得到杂环产物。

39. 发明授权

US07824931B2 Substrate processing control method and storage medium 有权
标题翻译：基板处理控制方法和存储介质
公开(公告)号：US07824931B2
公开(公告)日：2010-11-02
申请号：US12511749
申请日：2009-07-29
申请人： Susumu Saito , Akitaka Shimizu
发明人： Susumu Saito , Akitaka Shimizu
IPC分类号： H01L21/66
CPC分类号： H01L21/67069 , H01L21/67242 , H01L22/12 , H01L22/26 , H01L2924/0002 , H01L2924/00
摘要： In a substrate processing control method, a first process acquires a first-reflectance-spectrum of a beam reflected from the first-fine-structure and a second-reflectance-spectrum of a beam reflected from the second-fine-structure for each of varying-pattern-dimensions of the first-fine-structure when the pattern-dimension of the first-fine-structure is varied. A second process acquires reference-spectrum-data for each of the varying-pattern-dimensions of the first-fine-structure by overlapping the first-reflectance-spectrum with the second-reflectance-spectrum. A third process actually measures beams reflected from the first and the second-fine-structure, respectively, after irradiating light beam on to the substrate and acquiring reflectance-spectrums of the actual-measured beams as actual-measured spectrum data. A fourth process compares the actual-measured spectrum data with the respective reference-spectrum data and acquiring, as the measured pattern-dimension, one of the varying-pattern-dimensions corresponding to reference-spectrum data that is closely matches with the actual-measured spectrum data. A final process ends the processing of the substrate if the measured pattern-dimension reaches a value.
摘要翻译：在基板处理控制方法中，第一处理取得从第一微细结构反射的光束的第一反射光谱和从第二微细结构反射的光束的第二反射光谱，当第一微细结构的图案尺寸变化时，第一微细结构的图案尺寸。第二过程通过将第一反射光谱与第二反射光谱重叠来获取第一精细结构的每个变化图形尺寸的参考光谱数据。第三处理实际上是在将光束照射到衬底上之后分别测量从第一和第二微细结构反射的光束，并且将实测光束的反射光谱作为实测光谱数据进行测量。第四个过程将实际测量的频谱数据与相应的参考频谱数据进行比较，并且将与参考频谱数据相对应的变化模式维度中的一个与实际测量的频谱数据紧密匹配，作为测量的模式维度频谱数据。如果测量的图案尺寸达到一个值，则最后的处理结束衬底的处理。

40. 发明授权

US07662646B2 Plasma processing method and plasma processing apparatus for performing accurate end point detection 有权
标题翻译：用于执行精确终点检测的等离子体处理方法和等离子体处理装置
公开(公告)号：US07662646B2
公开(公告)日：2010-02-16
申请号：US11687428
申请日：2007-03-16
申请人： Kosuke Ogasawara , Susumu Saito , Syuji Nozawa
发明人： Kosuke Ogasawara , Susumu Saito , Syuji Nozawa
IPC分类号： H01L21/00
CPC分类号： H01J37/32935 , H01J37/32963 , H01L22/26
摘要： In a plasma processing method, a correlation between substrate type data and optical data is obtained by using a multivariate analysis; substrate type data is obtained from optical data based on the correlation when initiating a plasma processing; and a substrate type is determined by using the obtained substrate type data. Further, a setting data set corresponding to the determined substrate type is selected from setting data sets, each for detecting a plasma processing end point of the plasma processing, each of the setting data sets being stored in advance in a data storage unit; an end point of the plasma processing is detected based on the selected setting data set; and the plasma processing is terminated at the detected end point.
摘要翻译：在等离子体处理方法中，通过使用多元分析获得基板类型数据和光学数据之间的相关性; 基于等离子体处理时的相关性，从光学数据获得基板型数据; 并且通过使用所获得的基板类型数据来确定基板类型。此外，从设置数据组中选择与所确定的基板类型相对应的设置数据集，每个设置数据组用于检测等离子体处理的等离子体处理结束点，每个设置数据集被预先存储在数据存储单元中; 基于所选择的设置数据集来检测等离子体处理的终点; 并且在检测到的终点处终止等离子体处理。

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