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31. 发明授权

US4931572A Aromatic carboxylic anhydride catalyst 失效
标题翻译：芳香族羧酸酐催化剂
公开(公告)号：US4931572A
公开(公告)日：1990-06-05
申请号：US353252
申请日：1989-05-17
申请人： Ramzi Y. Saleh , Israel E. Wachs
发明人： Ramzi Y. Saleh , Israel E. Wachs
IPC分类号： B01J23/04 , B01J23/22 , C07C51/265
CPC分类号： B01J23/22 , B01J23/04 , C07C51/265
摘要： In accordance with the process of this invention, an improved titanium dioxide rutile-based catalyst for molecular oxidation of a hydrocarbon to form the corresponding carboxylic anhydrides is prepared by the steps of (a) forming a catalyst precursor by depositing on titanium dioxide solids in the rutile form a discontinuous monolayer amount of at least one source of a Group IA metal oxide; (b) calcining the thus-formed catalyst precursor under conditions sufficient to convert the Group IA metal oxide source into the corresponding Group IA metal oxide; (c) depositing upon the calcined catalyst precursor a catalytically effective amount of at least one vanadium oxide source which is convertible into vanadium oxide upon heating; and (d) calcining the vanadium-deposited solids under conditions sufficient to convert the vanadium compound into vanadium oxide.
摘要翻译：根据本发明的方法，通过以下步骤制备用于烃的分子氧化以形成相应的羧酸酐的改进的二氧化钛金红石型催化剂：（a）通过沉积在二氧化钛固体中形成催化剂前体金红石形成不连续单层量的至少一种IA族金属氧化物源; （b）在足以将IA族金属氧化物源转化成相应的IA族金属氧化物的条件下煅烧如此形成的催化剂前体; （c）在煅烧的催化剂前体上沉积催化有效量的至少一种氧化钒源，其在加热时可转化成氧化钒; 和（d）在足以将钒化合物转化为氧化钒的条件下煅烧钒沉积固体。

32. 发明授权

US4864036A Process for preparing aromatic carboxylic anhydride 失效
标题翻译：制备芳香族羧酸酐的方法
公开(公告)号：US4864036A
公开(公告)日：1989-09-05
申请号：US213524
申请日：1988-06-30
申请人： Ramzi Y. Saleh , Isreal E. Wachs
发明人： Ramzi Y. Saleh , Isreal E. Wachs
IPC分类号： B01J23/20 , B01J23/22 , B01J37/02 , C07C51/265
CPC分类号： C07C51/265 , B01J23/20 , B01J23/22 , B01J37/024
摘要： In accordance with the process of this invention, an improved catalyst for molecular oxidation of a hydrocarbon to form the corresponding carboxylic anhydrides is prepared by the steps of (a) forming a catalyst precursor by depositing on titanium dioxide solids in the anatase form a discontinuous monolayer amount of at least one source of a Group VIB metal oxide; (b) calcining the thus-formed catalyst precursor under conditions sufficient to convert the Group VIB metal oxide source into the corresponding group VIB metal oxide; (c) depositing upon amount of at least one vanadium oxide source which is calcining the vanadium-deposited solids under conditions sufficient to convert the vanadium compound into vanadium oxide.
摘要翻译：根据本发明的方法，通过以下步骤制备用于烃的分子氧化以形成相应的羧酸酐的改进的催化剂：（a）通过在锐钛矿的二氧化钛固体上沉积形成不连续的单层形成催化剂前体至少一种VIB族金属氧化物源的量; （b）在足以将VIB族金属氧化物源转化为相应的VIB族金属氧化物的条件下煅烧如此形成的催化剂前体; （c）在足以将钒化合物转化为氧化钒的条件下，沉积一定量的至少一种钒氧化物源，该钒氧化物源正在煅烧钒沉积固体。

33. 发明授权

US4728744A Catalysts for preparation of aromatic carboxylic anhydrides 失效
标题翻译：用于制备芳族羧酸酐的催化剂
公开(公告)号：US4728744A
公开(公告)日：1988-03-01
申请号：US782966
申请日：1985-10-02
申请人： Ramzi Y. Saleh , Israel E. Wachs
发明人： Ramzi Y. Saleh , Israel E. Wachs
IPC分类号： B01J23/22 , C07B61/00 , C07C51/215 , C07C51/25 , C07C51/265 , C07C51/31 , C07D307/89
CPC分类号： C07C51/313 , B01J23/22 , C07C51/215 , C07C51/25 , C07C51/252 , C07C51/265
摘要： In accordance with the process of this invention, an improved catalyst for molecular oxidation of an aromatic hydrocarbon to form the corresponding aromatic carboxylic anhydrides is prepared by the steps of forming a catalyst precursor by depositing on titanium dioxide solids in the anatase form a continuous monolayer amount of at least one source of zirconium dioxide, calcining the thus-formed catalyst precursor under conditions sufficient to convert the zirconium oxide source into the oxide form, depositing upon the calcined catalyst precursor a catalytically effective amount of at least one vanadium compound which is convertible into vanadium oxide upon heating and calcining the vanadium-deposited solids under conditions sufficient to convert the vanadium compound into vanadium oxide.
摘要翻译：根据本发明的方法，通过以下步骤制备用于分子氧化芳族烃以形成相应的芳族羧酸酐的改进的催化剂：通过以锐钛矿形式的二氧化钛固体沉积形成连续单层量形成催化剂前体的至少一种二氧化锆源，在足以将氧化锆源转化为氧化物形式的条件下煅烧由此形成的催化剂前体，在煅烧的催化剂前体上沉积催化有效量的至少一种钒化合物，其可转化为氧化钒加热并在足以将钒化合物转化为氧化钒的条件下煅烧钒沉积固体。

34. 发明授权

US4582912A Process for preparing carboxylic anhydride using improved catalysts 失效
标题翻译：使用改进的催化剂制备羧酸酐的方法
公开(公告)号：US4582912A
公开(公告)日：1986-04-15
申请号：US655745
申请日：1984-10-01
申请人： Ramzi Y. Saleh , Israel E. Wachs
发明人： Ramzi Y. Saleh , Israel E. Wachs
IPC分类号： C07D307/89 , B01J23/20 , B01J23/22 , B01J37/02 , C07B61/00 , C07C51/265 , C07D493/04
CPC分类号： C07C51/265 , B01J23/20 , B01J23/22 , B01J37/024
摘要： In accordance with the process of this invention, an improved catalyst for molecular oxidation of a hydrocarbon to form the corresponding carboxylic anhydrides is prepared by the steps of (a) forming a catalyst precursor by depositing on titanium dioxide solids in the anatase form at least a monolayer amount of at least one source of vanadium oxide, (b) calcining the thus-formed catalyst precursor under conditions sufficient to convert the vanadium oxide source into the oxide form, (c) depositing upon the calcined catalyst precursor a catalytically effective amount of at least one vanadium oxide source which is convertible into vanadium oxide upon heating and at least one metal oxide source selected from the group consisting of oxides of Sb, Ga, Ge, In, Tl, Pb, Se, Te, P and Bi, which is convertible into the corresponding metal oxide upon heating and which is reactive with V.sub.2 O.sub.5, and (d) calcining the vanadium and reactive metal containing catalyst solids under conditions sufficient to form the corresponding vanadium oxide and reactive metal oxides.
摘要翻译：根据本发明的方法，通过以下步骤制备用于烃的分子氧化以形成相应的羧酸酐的改进的催化剂：（a）通过以锐钛矿形式沉积在二氧化钛固体上至少形成催化剂前体单层量的至少一种氧化钒源，（b）在足以将钒氧化物源转化为氧化物形式的条件下煅烧由此形成的催化剂前体，（c）在煅烧的催化剂前体上沉积催化有效量的至少一种氧化钒源，其在加热时可转化为氧化钒，以及选自Sb，Ga，Ge，In，Tl，Pb，Se，Te，P和Bi的氧化物中的至少一种金属氧化物源，其是加热时可转化成相应的金属氧化物，并与V2O5反应，和（d）在足以满足以下条件的条件下煅烧含钒和活性金属的催化剂固体：形成相应的氧化钒和活性金属氧化物。

35. 发明授权

US4410453A Ethylene oxide catalyst 失效
标题翻译：环氧乙烷催化剂
公开(公告)号：US4410453A
公开(公告)日：1983-10-18
申请号：US344461
申请日：1982-02-01
申请人： Joseph R. Kiovsky , George W. Young , Ramzi Y. Saleh
发明人： Joseph R. Kiovsky , George W. Young , Ramzi Y. Saleh
IPC分类号： B01J23/50 , B01J23/68 , C07D301/10 , B01J21/04 , B01J21/12
CPC分类号： B01J23/50 , B01J23/68 , C07D301/10
摘要： The performance of a silver on alumina catalyst for the oxidation of ethylene to ethylene oxide is improved by the inclusion, in the raw mix for the carrier of an oxide, or oxide precursor, of zinc, lanthanum, or magnesium in the amount of 7 to 40%, calculated as the oxide.
摘要翻译：在氧化乙烯到氧化乙烯的氧化铝催化剂上的银的性能通过在氧化物的载体或氧化物前体的锌，镧或镁的原料混合物中包含7至 40％，以氧化物计算。

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