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31. 发明授权

US5554710A Conductive polymers and process for preparing the same 失效
标题翻译：导电聚合物及其制备方法
公开(公告)号：US5554710A
公开(公告)日：1996-09-10
申请号：US197986
申请日：1994-02-17
申请人： Shigeru Mori , Motoo Fukushima , Eiichi Tabei , Yoshitaka Hamada , Seizi Katayama
发明人： Shigeru Mori , Motoo Fukushima , Eiichi Tabei , Yoshitaka Hamada , Seizi Katayama
IPC分类号： C08G77/60 , C08L83/16 , C09D183/16 , H01M6/18 , C08G77/20 , B05D5/12 , H01M4/70
CPC分类号： C09D183/16 , C08G77/60 , C08L83/16 , H01M6/181
摘要： A conductive polymer comprises a silicon-containing polymer having, in the main chain thereof, Si--Si bonds or both Si--Si bonds and C--C multiple bonds, and ferric chloride doped in said polymer through vapor phase doping. A method for preparing such a conductive polymer is also described.
摘要翻译：导电聚合物包括在其主链中具有Si-Si键或Si-Si键和C-C多键的含硅聚合物，以及通过气相掺杂掺杂在所述聚合物中的氯化铁。还描述了制备这种导电聚合物的方法。

32. 发明授权

US5374758A Hydro-terminated polysilane and process for making 失效
标题翻译：水解端基聚硅烷和制备方法
公开(公告)号：US5374758A
公开(公告)日：1994-12-20
申请号：US96259
申请日：1993-07-26
申请人： Shigeru Mori , Eiichi Tabei
发明人： Shigeru Mori , Eiichi Tabei
IPC分类号： C07F7/08 , C08G77/48 , C08G77/60
CPC分类号： C07F7/0896
摘要： A both end hydro-terminated polysilane is of the formula: H[(R.sup.1 R.sup.2 Si).sub.n (R.sup.3 R.sup.4 Si).sub.m ].sub.k H wherein R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are independently C.sub.1 -C.sub.12 alkyl groups or aryl groups and letters n, m and k are numbers in the range: 0.ltoreq.n.ltoreq.10, 0.ltoreq.m.ltoreq.10, n+m.gtoreq.10, and k.gtoreq.1. It is prepared by dissolving a corresponding chloro-terminated polysilane in a solvent and reducing with LiAlH.sub.4 in an inert gas atmosphere.
摘要翻译：两末端加氢封端的聚硅烷具有下式：H [（R 1 R 2 Si）n（R 3 R 4 Si）m] k H其中R 1，R 2，R 3和R 4独立地为C 1 -C 12烷基或芳基，并且字母n，m和k为范围内的数字：0 / = 10，k> / = 1。通过将相应的氯封端的聚硅烷溶解在溶剂中并在惰性气体气氛中用LiAlH 4还原制备。

33. 发明授权

US5359106A Terminally reactive polysilane and process for making 失效
标题翻译：端反应性聚硅烷和制备方法
公开(公告)号：US5359106A
公开(公告)日：1994-10-25
申请号：US171437
申请日：1993-12-22
申请人： Eiichi Tabei , Shigeru Mori
发明人： Eiichi Tabei , Shigeru Mori
IPC分类号： C07F7/08 , C07F7/18 , C08G77/48 , C08G77/60 , C07F7/10
CPC分类号： C08G77/60 , C07F7/0818 , C07F7/1836
摘要： Terminally reactive polysilanes of formula (1) are novel. ##STR1## R.sup.1, R.sup.2, R.sup.3, and R.sup.4 are independently C.sub.1-12 alkyl or aryl groups, R.sup.5 is an organic group containing an alkoxysilyl, epoxy, glycidyloxy, acryl, methacryl, acetoxysilyl or amino group, A is a C.sub.2-6 alkylene group, n, m and k are numbers in the range: 0.ltoreq.n.ltoreq.10, 0.ltoreq.m.ltoreq.10, n+m.gtoreq.10, and k.gtoreq.1. The polysilanes are prepared by effecting addition reaction between a hydro-terminated polysilane and an unsaturated group-containing reactive compound in the presence of a hydrosilylation catalyst.
摘要翻译：式（1）的末端反应性聚硅烷是新颖的。（1）R1，R2，R3和R4分别是C1-12烷基或芳基，R5是含有烷氧基甲硅烷基，环氧基，缩水甘油氧基，丙烯酰基，甲基丙烯酰基，乙酰氧基甲硅烷基或氨基的有机基团，A是C2 -6亚烷基，n，m和k是以下范围内的数字：0≤n≤10,0≤m≤10，n + m> = 10，k> / = 1 。聚硅烷通过在氢化硅烷化催化剂的存在下进行加氢封端的聚硅烷和含不饱和基团的反应性化合物之间的加成反应来制备。

34. 发明授权

US5159043A Preparation of polyorganosilanes 失效
标题翻译：聚有机硅烷的制备
公开(公告)号：US5159043A
公开(公告)日：1992-10-27
申请号：US812279
申请日：1991-12-23
申请人： Shigeru Mori , Eiichi Tabei , Motoo Fukushima , Yoshinori Hida
发明人： Shigeru Mori , Eiichi Tabei , Motoo Fukushima , Yoshinori Hida
IPC分类号： C08G77/48 , C08G77/60
CPC分类号： C08G77/60
摘要： Polyorganosilanes are prepared through contact reaction of an organodihalosilane with alkali metal fine particles dispersed in an organic solvent. the reaction solution is adjusted to an acidity of pH 3 to 7 before or after the step of deactivating the excess alkali metal in the reaction solution. The alkali metal halide is removed from the reaction solution by dissolving it in water. Formation of insoluble components is minimized.
摘要翻译：聚有机硅烷通过有机二卤硅烷与分散在有机溶剂中的碱金属微粒的接触反应制备。在使反应溶液中过量的碱金属失活的步骤之前或之后将反应溶液调节至pH 3至7的酸度。将碱金属卤化物溶解在水中从反应溶液中除去。不溶性组分的形成最小化。

35. 发明授权

US5132047A Organopolysiloxane emulsion composition 失效
标题翻译：有机聚硅氧烷乳液组合物
公开(公告)号：US5132047A
公开(公告)日：1992-07-21
申请号：US650994
申请日：1991-02-04
申请人： Masaki Tanaka , Teiichi Mutoh , Noriyuki Meguriya , Eiichi Tabei
发明人： Masaki Tanaka , Teiichi Mutoh , Noriyuki Meguriya , Eiichi Tabei
IPC分类号： B01F17/54 , C08J3/03
CPC分类号： C08J3/03 , B01F17/0071 , C08J2383/04 , Y10S516/01 , Y10S516/906
摘要： An organopolysiloxane emulsion composition comprising:a silicone emulsifying agent comprising a compound represented by the general formula (I): ##STR1## wherein a plurality of R.sup.1 may be the same or different and each represent a substituted or unsubstituted monovalent hydrocarbon group having 1 to 20 carbon atoms; R.sup.2 represents a divalent hydrocarbon group having 1 to 6 carbon atoms; R.sup.3 represents an atom or group selected from the group consisting of a hydrogen atom, an acetyl group, R.sup.1, and --Si(R.sup.1).sub.3 ; A represents a divalent hydrocarbon group having 1 to 4 carbon atoms; and x and y are numbers of 5.ltoreq.x.ltoreq.50 and 1.ltoreq.y.ltoreq.100, respectively;an organopolysiloxane which is liquid at room temperature; andwater.This emulsion composition can be prepared as either w/o emulsion or o/w emulsion with good stability.
摘要翻译：一种有机聚硅氧烷乳液组合物，其包含：含有由通式（I）表示的化合物的硅氧烷乳化剂：其中多个R 1可以相同或不同，并且各自表示取代或未取代的一价烃基，其具有 1至20个碳原子; R2表示碳原子数为1〜6的二价烃基; R3表示选自氢原子，乙酰基，R1和-Si（R1）3的原子或基团; A表示具有1至4个碳原子的二价烃基; 并且x和y分别为5≤x≤50和1≤y≤100的数字; 在室温下为液体的有机聚硅氧烷; 和水。该乳液组合物可以制备成w / o乳液或o / w乳液，具有良好的稳定性。

36. 发明授权

US5128430A Preparation of polysilanes 失效
标题翻译：聚硅烷的制备
公开(公告)号：US5128430A
公开(公告)日：1992-07-07
申请号：US794979
申请日：1991-11-20
申请人： Eiichi Tabei , Motoo Fukushima , Yoshinori Hida , Akira Hayashida , Shigeru Mori
发明人： Eiichi Tabei , Motoo Fukushima , Yoshinori Hida , Akira Hayashida , Shigeru Mori
IPC分类号： C08G77/48 , C08G77/60
CPC分类号： C08G77/60
摘要： Polysilanes are produced by reacting dihalosilanes in the presence of alkali metals, By carrying out the dihalosilane reaction in the presence of copper halide catalysts at temperatures of at least 100.degree. C., higher molecular weight polysilanes are obtained in acceptable yields.
摘要翻译：聚硅烷通过在碱金属的存在下使二卤代硅烷反应来制备。通过在卤化铜催化剂存在下，在至少100℃的温度下进行二氯硅烷反应，得到较高分子量的聚硅烷以可接受的产率。

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