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31. 发明授权

US07160975B2 Methacrylates as stabilizers for polymer polyols 有权
标题翻译：甲基丙烯酸酯作为聚合物多元醇的稳定剂
公开(公告)号：US07160975B2
公开(公告)日：2007-01-09
申请号：US10909476
申请日：2004-08-02
申请人： Rick L. Adkins , Scott A. Guelcher
发明人： Rick L. Adkins , Scott A. Guelcher
IPC分类号： C08G18/62
CPC分类号： C08G18/635 , C08G18/409 , C08G18/6795
摘要： This invention relates to ethylenically unsaturated macromers which contain reactive unsaturation, and to a process for preparing these ethylenicallly unsaturated macromers which contain reactive unsaturation. The process of preparing these ethylenically unsaturated macromers comprises reacting a monofunctional compound which corresponds to a specific formula with at least one alkylene oxide, in the presence of at least one alkoxylation catalyst. The ethylenically unsaturated macromers correspond to the formula set forth herein. This invention also relates to preformed stabilizers comprising ethylenically unsaturated macromers, to a process for preparing these preformed stabilizers, to polymer polyols comprising these preformed stabilizers, and to a process of preparing these polymer polyols which comprise these preformed stabilizers. Polymer polyols comprising ethylenically unsaturated macromers and a process for their preparation are also described.
摘要翻译：本发明涉及含有反应性不饱和键的烯键式不饱和大分子单体，以及制备这些具有反应性不饱和度的烯属不饱和大单体的方法。制备这些烯属不饱和大分子单体的方法包括在至少一种烷氧基化催化剂的存在下使对应于特定式的单官能化合物与至少一种烯化氧反应。烯键式不饱和大分子单体对应于本文所述的式。本发明还涉及包含烯属不饱和大分子单体的预制稳定剂，制备这些预型稳定剂的方法，包括这些预制稳定剂的聚合物多元醇，以及包含这些预型稳定剂的这些聚合物多元醇的制备方法。还描述了包含烯属不饱和大分子单体的聚合物多元醇及其制备方法。

32. 发明授权

US5914409A Tolyltriazole process 失效
标题翻译：甲苯基三唑工艺
公开(公告)号：US5914409A
公开(公告)日：1999-06-22
申请号：US30790
申请日：1998-02-25
申请人： Rick L. Adkins , Craig M. Young
发明人： Rick L. Adkins , Craig M. Young
IPC分类号： C07D249/18
CPC分类号： C07D249/18
摘要： This invention relates to an improved process for the production of tolyltriazole in which the tolyltriazole is a lighter colored product. The color improvement in the tolyltriazole produced from this process occurs when the ortho-toluenediamine reactant is previously stabilized by treatment with a compound selected from the group consisting of aldehydes, ketones, acetals and ketals. The process of the present invention reduces the need to purify (by, for example, filtration or distillation) the tolyltriazole prior to being used commercially.
摘要翻译：本发明涉及一种生产甲苯基三唑的改进方法，其中甲苯基三唑是较浅的产品。当通过用选自醛，酮，缩醛和缩酮的化合物处理预先稳定邻甲苯二胺反应物时，由该方法产生的甲苯基三唑的颜色改进发生。本发明的方法减少了在商业使用之前纯化（通过例如过滤或蒸馏）甲苯基三唑的需要。

33. 发明申请

US20140066536A1 POLYMER POLYOLS HAVING IMPROVED QUALITY 审中-公开
标题翻译：具有改进质量的聚合物多元醇
公开(公告)号：US20140066536A1
公开(公告)日：2014-03-06
申请号：US13598832
申请日：2012-08-30
申请人： Rick L. Adkins , Shriniwas S. Chauk , James R. Charron
发明人： Rick L. Adkins , Shriniwas S. Chauk , James R. Charron
IPC分类号： C08G65/26 , C08G18/50 , C08J9/04
CPC分类号： C08J9/04 , C08F283/06 , C08G18/632 , C08G18/636 , C08J2375/08 , C08F212/08 , C08F220/44
摘要： This invention relates to polymer polyols comprising one or more base polyols; one or more ethylenically unsaturated monomers in which at least one of the monomers is styrene which contains less than or equal to 1000 ppm of impurities; with one or more preformed stabilizers; in the presence of at least one free radical polymerization initiator; and optionally, one or more chain transfer agents.
摘要翻译：本发明涉及包含一种或多种碱性多元醇的聚合物多元醇; 一种或多种烯键式不饱和单体，其中至少一种单体是含有小于或等于1000ppm杂质的苯乙烯; 与一个或多个预制稳定剂; 在至少一种自由基聚合引发剂的存在下; 和任选的一种或多种链转移剂。

34. 发明授权

US07423112B2 Polyether polyols containing pendant amine groups and a process for their preparation 有权
标题翻译：含有侧基胺基团的聚醚多元醇及其制备方法
公开(公告)号：US07423112B2
公开(公告)日：2008-09-09
申请号：US10855712
申请日：2004-05-27
申请人： Rick L. Adkins
发明人： Rick L. Adkins
IPC分类号： C08G65/34
CPC分类号： C08G65/2663 , C08G65/2696 , C08G65/325
摘要： The present invention relates to novel polyether polyols containing pendant amine group and to a process for their preparation. These polyether polyols have molecular weights of from about 105 to about 35,000, and contain at least one terminal hydroxyl group and at least one pendant amine group. The process for their preparation comprises reacting a compound containing from 1 to 10 hydroxyl groups and a molecular weight of about 32 to about 15,000 with at least one epoxide which contains one or more halogen atoms, in the presence of one or more DMC catalysts, to form an intermediate polyether polyol which contains halogenated carbon atoms; then reacting this intermediate polyether polyol with an amine group containing compound having from 1 to 3 primary, secondary and/or tertiary amine groups.
摘要翻译：本发明涉及含有侧基胺基的新型聚醚多元醇及其制备方法。这些聚醚多元醇的分子量为约105至约35,000，并且含有至少一个末端羟基和至少一个侧基胺基。其制备方法包括在一种或多种DMC催化剂的存在下，将含有1至10个羟基和分子量为约32至约15,000的化合物与至少一种含有一个或多个卤素原子的环氧化物反应至形成含有卤代碳原子的中间聚醚多元醇; 然后使该中间聚醚多元醇与含有1至3个伯，仲和/或叔胺基团的含胺基化合物反应。

35. 发明申请

US20080132724A1 Allophanate modified isocyanates which contain reactive unsaturation 审中-公开
标题翻译：含有反应性不饱和度的脲基甲酸酯改性异氰酸酯
公开(公告)号：US20080132724A1
公开(公告)日：2008-06-05
申请号：US11633242
申请日：2006-12-04
申请人： Rick L. Adkins
发明人： Rick L. Adkins
IPC分类号： C07C265/12 , C07C263/16
CPC分类号： C08G18/7671 , C08G18/672 , C08G18/7837
摘要： This invention relates to a novel liquid, storage-stable diphenylmethane diisocyanate which contains allophanate and reactive unsaturation. These novel storage-stable liquids comprise the reaction product of diphenylmethane diisocyanate with an ethylenically unsaturated alcohol, in the presence of an allophanate catalyst and a suitable inhibitor.
摘要翻译：本发明涉及含有脲基甲酸酯和反应性不饱和度的新型液体储存稳定的二苯基甲烷二异氰酸酯。这些新型储存稳定液体包含二苯基甲烷二异氰酸酯与烯键式不饱和醇的反应产物，在脲基甲酸酯催化剂和合适的抑制剂存在下。

36. 发明授权

US07179882B2 Low viscosity polymer polyols 有权
标题翻译：低粘度聚合物多元醇
公开(公告)号：US07179882B2
公开(公告)日：2007-02-20
申请号：US10909492
申请日：2004-08-02
申请人： Rick L. Adkins , Scott A. Guelcher , James R. Charron , John E. Hayes
发明人： Rick L. Adkins , Scott A. Guelcher , James R. Charron , John E. Hayes
IPC分类号： C08G63/02
CPC分类号： C08G18/4883 , C08F283/06 , C08F290/062 , C08G18/632 , C08G18/636 , C08G18/8108 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： The present invention relates to low viscosity polymer polyols and to a process for the preparation of these low viscosity polymer polyols. These polymer polyols comprise the free-radical polymerization product of (A) a base polyol, (B) a pre-formed stabilizer, and (C) at least one ethylenically unsaturated monomer, in the presence of (D) at least one free-radical polymerization initiator, and (E) at least one polymer control agent. The total amount of polymer control agent present in the polymer polyols of the present invention ranges from greater than about 5.0% up to about 20% by weight, based on 100% by weight of the polymer polyol.
摘要翻译：本发明涉及低粘度聚合物多元醇和制备这些低粘度聚合物多元醇的方法。这些聚合物多元醇包含（A）基础多元醇，（B）预成形稳定剂和（C）至少一种烯键式不饱和单体的自由基聚合产物，在（D）至少一种游离 - 自由基聚合引发剂，和（E）至少一种聚合物控制剂。存在于本发明的聚合物多元醇中的聚合物控制剂的总量基于100重量％的聚合物多元醇的大于约5.0重量％至约20重量％。

37. 发明授权

US06841585B2 Tetralin isocyanates 失效
标题翻译：四氢萘异氰酸酯
公开(公告)号：US06841585B2
公开(公告)日：2005-01-11
申请号：US10752243
申请日：2004-01-06
申请人： Rick L. Adkins , Harold R. Parsons
发明人： Rick L. Adkins , Harold R. Parsons
IPC分类号： C07B61/00 , C07C263/10 , C07C263/18 , C07C265/12 , C07C265/14 , C07C267/00 , C08G18/00 , C08G18/06 , C08G18/70 , C08G18/76 , C08G101/00 , C08J9/00
CPC分类号： C07C265/14 , C07C265/12 , C07C2602/10 , C08G18/7614 , C08G2101/0008 , C08G2101/005 , C08G2101/0083
摘要： The present invention relates to novel aromatic isocyanates obtained by partially hydrogenating naphthalene as well as the processes for preparing the same, and to their use as an isocyanate component in the production of polyurethanes.
摘要翻译：本发明涉及通过部分氢化萘获得的新型芳族异氰酸酯及其制备方法，以及它们在聚氨酯生产中作为异氰酸酯组分的用途。

38. 发明授权

US6004482A Stable aromatic amine composition, and a process for preparing color stable aromatic amines 失效
标题翻译：稳定的芳族胺组合物，和制备颜色稳定的芳族胺的方法
公开(公告)号：US6004482A
公开(公告)日：1999-12-21
申请号：US998141
申请日：1997-12-24
申请人： Rick L. Adkins , Steven L. Schilling , Keith J. Headley
发明人： Rick L. Adkins , Steven L. Schilling , Keith J. Headley
IPC分类号： C07C209/90 , C07C211/51 , C07C213/10 , C07C215/76 , C08G18/50 , C08G65/26 , C08G65/333 , C08K3/30 , C08K3/38 , C09K15/32
CPC分类号： C08K3/30 , C07C209/90 , C08G18/5033 , C08G65/2627 , C08G65/33313 , C08K3/38
摘要： This invention relates to stable aromatic amine compositions. These compositions comprise a) a compound selected from the group consisting of alkali metal salts of sulfur compounds, hydrates thereof and aldehydes thereof, aluminum hydrides, borates and boron compounds; and b) an aromatic amine. This invention also relates to a process for stabilizing the color of aromatic amines, and to the production of polyether polyols from these stable aromatic amine compositions.
摘要翻译：本发明涉及稳定的芳族胺组合物。这些组合物包含a）选自硫化合物的碱金属盐，其水合物和其醛，氢化铝，硼酸盐和硼化合物的化合物的化合物; 和b）芳族胺。本发明还涉及一种稳定芳族胺颜色的方法，以及由这些稳定的芳族胺组合物生产聚醚多元醇的方法。

39. 发明授权

US5872292A Stable aromatic amine composition, a process for preparing color stable aromatic amines, and the production of light colored aromatic amine-based polyether polyols 失效
标题翻译：稳定的芳族胺组合物，制备色稳定性芳族胺的方法，以及制备浅色芳族胺基聚醚多元醇
公开(公告)号：US5872292A
公开(公告)日：1999-02-16
申请号：US788788
申请日：1997-01-24
申请人： Rick L. Adkins , Steven L. Schilling , Keith J. Headley
发明人： Rick L. Adkins , Steven L. Schilling , Keith J. Headley
IPC分类号： C07C211/49 , C08G65/26 , C07C209/90
CPC分类号： C08G65/2627
摘要： This invention relates to stable aromatic amine compositions. These compositions comprise a) a compound selected from the group consisting of aldehydes, ketones, acetals and ketals, and b) an aromatic amine. This invention also relates to a process for stabilizing the color of aromatic amines, and to the use of these aromatic amines as initiators for the preparation of polyether polyols.
摘要翻译：本发明涉及稳定的芳族胺组合物。这些组合物包含a）选自醛，酮，缩醛和缩酮的化合物，和b）芳族胺。本发明还涉及稳定芳族胺颜色的方法，以及这些芳族胺作为制备聚醚多元醇的引发剂的用途。

40. 发明申请

US20130158142A1 HYBRID PHD/PMPO POLYOLS FOR POLYURETHANE FOAM APPLICATIONS 有权
标题翻译：用于聚氨酯泡沫应用的HYBRID PHD / PMPO POLYOLS
公开(公告)号：US20130158142A1
公开(公告)日：2013-06-20
申请号：US13327879
申请日：2011-12-16
申请人： Rick L. Adkins , Brian L. Neal
发明人： Rick L. Adkins , Brian L. Neal
IPC分类号： C08G18/32 , C08J9/04
CPC分类号： C08G18/4072 , C08F283/006 , C08G18/0876 , C08G18/3231 , C08G18/632 , C08G18/636 , C08G18/7621 , C08G2101/0008 , C08G2101/0083 , C08F212/08 , C08F220/44
摘要： This invention relates to hybrid polymer polyols. These hybrid polymer polyols comprise the free-radical polymerization product of (A) a base polyol comprising (1) a polymer modified polyol selected from (a) dispersions of polyureas and/or polyhydrazodicarbonamides in a hydroxyl group containing compound and (b) polyisocyanate polyaddition polyols, and (2) optionally, a polyol having a functionality of 2 to 6 and an OH number of from 20 to 500; (B) optionally, a preformed stabilizer; and (C) one or more ethylenically unsaturated monomers, in the presence of (D) a free-radical polymerization initiator, and (E) optionally, a polymer control agent. The present invention also relates to a process for the preparation of these hybrid polymer polyols, foams prepared from these hybrid polymer polyols and to a process for the preparation of these foams.
摘要翻译：本发明涉及杂化聚合物多元醇。这些杂化聚合物多元醇包含（A）基础多元醇的自由基聚合产物，其包含（1）聚合物改性的多元醇，其选自（a）在含羟基的化合物中的聚脲和/或聚二氢二碳酰胺的分散体和（b）聚异氰酸酯加聚多元醇，和（2）任选的官能度为2至6且OH数为20至500的多元醇; （B）任选的预成型稳定剂; 和（C）一种或多种烯属不饱和单体，在（D）自由基聚合引发剂存在下，和（E）任选的聚合物控制剂。本发明还涉及制备这些杂化聚合物多元醇的方法，由这些杂化聚合物多元醇制备的泡沫和制备这些泡沫的方法。

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