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31. 发明授权

US06255513B1 Stable compositions of water-soluble amino-and alkenyl-functional organosiloxanes, process for their preparation and their use 有权
标题翻译：水溶性氨基和烯基官能的有机硅氧烷的稳定组合物，其制备方法及其应用
公开(公告)号：US06255513B1
公开(公告)日：2001-07-03
申请号：US09300448
申请日：1999-04-28
申请人： Burkhard Standke , Jaroslaw Monkiewicz , Albert-Johannes Frings , Ralf Laven , Roland Edelmann , Peter Jenkner , Helmut Mack , Dieter Barfurth , Michael Horn
发明人： Burkhard Standke , Jaroslaw Monkiewicz , Albert-Johannes Frings , Ralf Laven , Roland Edelmann , Peter Jenkner , Helmut Mack , Dieter Barfurth , Michael Horn
IPC分类号： C07F710
CPC分类号： C08G77/20 , C08G77/26 , Y10T428/2995
摘要： The present invention relates to a stable composition of water-soluble organosiloxanes obtained by reacting a) a water-soluble amino-functional alkoxysilane with at least one water-insoluble alkenyl-functional alkoxysilane b) by adding water to form a mixture, and c) removing the alcohol formed during step b) from the mixture, where the amino-functional alkoxysilane and the water are used in the reaction at least in amounts such that substantially all of the alkoxy groups of the water-insoluble silane can react and such that when a resulting composition is diluted with water, essentially no alcohol is liberated by hydrolysis, and the composition, during an/or after the reaction, has a pH of from 2 to 6, the pH being preferably adjusted by adding an organic or inorganic, optionally aqueous, acid. In addition, the present invention discloses a process for the preparation of such a composition and also its use.
摘要翻译：本发明涉及水溶性有机硅氧烷的稳定组合物，该组合物通过使水溶性氨基官能化烷氧基硅烷与至少一种水不溶性烯基官能烷氧基硅烷b）反应而得到，所述组合物通过加入水以形成混合物，和c）除去醇在步骤b）中形成的步骤b）中，其中氨基官能的烷氧基硅烷和水在反应中使用至少使得水不溶性硅烷的基本上所有的烷氧基基本上可以反应，并且使得当得到的组合物用水稀释，基本上没有通过水解释出醇，并且在反应过程中或之后，组合物的pH为2-6，优选通过加入有机或无机的任选含水酸来调节pH 。此外，本发明公开了一种制备这种组合物的方法及其用途。

32. 发明授权

US06251989B1 Oligomerized organopolysiloxane cocondensate, its production and its use for treatment of surfaces 失效
标题翻译：低聚有机聚硅氧烷缩聚物，其生产及其用于表面处理
公开(公告)号：US06251989B1
公开(公告)日：2001-06-26
申请号：US09318839
申请日：1999-05-26
申请人： Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Eckhard Just , Manfred Kaussen , Ralf Laven , Helmut Lohmann , Helmut Mack , Jaroslaw Monkiewicz , Stephan Ramlow , Burkhard Standke , Tilman Taeger
发明人： Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Eckhard Just , Manfred Kaussen , Ralf Laven , Helmut Lohmann , Helmut Mack , Jaroslaw Monkiewicz , Stephan Ramlow , Burkhard Standke , Tilman Taeger
IPC分类号： C08G7718
CPC分类号： C08G77/045 , C08G77/24 , C08G77/26 , C09K3/18
摘要： An oligomerized polyorganosiloxane cocondensate which may be obtained, in part, by mixing an water-soluble amino-functional organosilane represented with at least one of the followoing: a fluoro-functional organosilane, an organosilane, and an organosilane. The cocondensate may be used, for example, in a method of treating surfaces.
摘要翻译：低聚聚有机硅氧烷缩聚物，其部分可以通过混合由至少一个以下代表的水溶性氨基官能的有机硅烷：氟官能的有机硅烷，有机硅烷和有机硅烷而获得。缩聚物可以用于例如处理表面的方法中。

33. 发明授权

US06177582B1 Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use 失效
标题翻译：基于醇的含氟烷基官能的有机硅氧烷的组合物，其制备方法及其用途
公开(公告)号：US06177582B1
公开(公告)日：2001-01-23
申请号：US08984162
申请日：1997-12-03
申请人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： C07P708
CPC分类号： C03C25/40 , C08G77/24 , C09D183/08 , C09K3/18 , D06M13/513 , D06M15/657 , D21H19/32 , D21H21/16
摘要： An alcoholic fluoroalkyl-functional group containing organosiloxane based composition is prepared by the controlled hydrolysis of at least one fluoroalkyl-functional group containing organosilane of formula I: R1—Y—(CH2)2SiHx(R2)y(OR)3−x−y (I), in which R1 is a mono, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH2, O or S group, R2 and R are each independently a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and x=0, 1 or 2 and y=0, 1 or 2, where (x+y)≦2, at a temperature in the range of 0-120° C. over a period of 0.5-24 hours and with thorough mixing in an alcoholic medium which contains water and a weak mono- or polybasic acid or a weak base or a weak mono- or polybasic acid and a weak base or an acid or basic salt, the water employed and the alkoxysilane employed being in a molar ratio of 2-500:1.
摘要翻译：含有有机硅氧烷的组合物的含氟烷基官能团的组合物是通过控制水解含有式I的有机硅烷的至少一个氟代烷基官能团制备的：其中R 1是具有1-9个C原子的单，低聚或全氟化烷基或单，低聚或全氟化芳基，Y是CH 2，O或S基团，R 2和R 3各自独立地为具有1-8个碳原子或芳基且x = 0的直链，支链或环状的烷基， 1或2，y = 0,1或2，其中（x + y）<= 2，在0〜120℃的温度范围内，在0.5-24小时内，并在酒精中充分混合含有水和弱单或多元酸或弱碱或弱单或多元酸和弱碱或酸或碱性盐的介质，所用的水和使用的烷氧基硅烷的摩尔比为2- 500：1。

34. 发明授权

US06713186B1 Fluoroalkyl-functional organosiloxane-containing compositions based on alcohol, a process for their preparation and their use 失效
标题翻译：基于醇的含氟烷基官能的有机硅氧烷的组合物，其制备方法及其用途
公开(公告)号：US06713186B1
公开(公告)日：2004-03-30
申请号：US09685341
申请日：2000-10-11
申请人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
发明人： Peter Jenkner , Albert-Johannes Frings , Michael Horn , Eckhard Just , Jaroslaw Monkiewicz , Burkhard Standke
IPC分类号： B32B1500
CPC分类号： C09K3/18 , C03C25/40 , C08G77/24 , C09D183/08 , D06M13/513 , D06M15/657 , D21H19/32 , D21H21/16 , Y10T428/31663
摘要： An alcoholic fluoroalkyl-functional group containing organosiloxane based composition prepared is prepared by the controlled hydrolysis of at least one fluoroalkyl-functional group containing organosilane of formula I: R1—Y—(CH2)2SiHx(R2)y(OR)3−x−y (I), in which R1 is a mono, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH2, O or S group, R2 and R are each independently a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and x=0, 1 or 2 and y=0, 1 or 2, where (x+y)≦2, at a temperature in the range of 0-120° C. over a period of 0.5-24 hours and with thorough mixing in an w alcoholic medium which contains water and a weak mono- or polybasic acid or a weak base or a weak mono- or polybasic acid and a weak base or an acid or basic salt, the water employed and the alkoxysilane employed being in a molar ratio of 2-500:1.
摘要翻译：制备的含有机硅氧烷的组合物的含氟烷基官能团的组合物是通过控制水解至少一个含有氟代烷基官能团的式I有机硅烷来制备的：其中R 1是具有1-羟基的单，低聚或全氟化的烷基， 9个C原子或单，低聚或全氟化芳基，Y为CH 2，O或S基团，R 2和R 3各自独立地为具有1-8个C原子的直链，支链或环状烷基或芳基和x = 0,1或2，y = 0,1或2，其中（x + y）<= 2，在0〜120℃的温度下，在0.5-24小时内并且在含有水和弱单或多元酸或弱碱或弱单或多元酸和弱碱或酸或碱性盐的w-醇介质中充分混合，使用的水和使用的烷氧基硅烷摩尔比为2-500:1。

35. 发明授权

US06534667B1 Water-based composition of amino-functional silicon compounds 有权
标题翻译：氨基官能硅化合物的水基组成
公开(公告)号：US06534667B1
公开(公告)日：2003-03-18
申请号：US09514356
申请日：2000-02-28
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz , Günter Switalla
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz , Günter Switalla
IPC分类号： C07F708
CPC分类号： C08K5/544 , C08K5/549 , C09D183/08 , C23C2222/20 , C08L83/08 , C08L2666/34
摘要： A composition which comprises a mixture of water-soluble, amino-functional silicon compounds which are essentially free from alkoxy groups, water, optionally a content of alcohol and optionally a content of acid, the composition comprising silicon compounds of the general formula I: NH2[CH2)2NH]x(CH2)3SiO1.5 (I) in which x is 0, 1 or 2, and of the general formula II: (SiO1.5(CH2)3[NH(CH2)2]yNH[(CH2)2NH]x(CH2)3Si)1.5 (II) in which y and z are 0, 1 or 2 and are identical or different. The compositions are obtainable by mixing corresponding aminoalkoxy silanes, hydrolyzing the mixture and removing the hydrolysis alcohol formed as a result. The invention furthermore relates to a process for the preparation of the compositions and to their use in a wide variety of applications.
摘要翻译：包含基本上不含烷氧基的水溶性，氨基官能的硅化合物的混合物的组合物，水，任选的醇含量和任选的酸的含量，所述组合物包含通式I的硅化合物：在其中x为0,1或2，通式II：其中y和z为0,1或2并且相同或不同。组合物可通过混合相应的氨基烷氧基硅烷，水解混合物并除去水解因此形成酒精。本发明还涉及制备组合物的方法及其在各种应用中的用途。

36. 发明授权

US06403228B1 Functional organylorganyloxysilanes on a carrier in cable compounds 失效
标题翻译：电缆化合物中载体上的功能性有机酰基氧基硅烷
公开(公告)号：US06403228B1
公开(公告)日：2002-06-11
申请号：US09604273
申请日：2000-06-26
申请人： Helmut Mack , Ralf Laven , Peter Jenkner , Roland Edelmann , Dieter Barfurth , Albert-Johannes Frings , Burkhard Standke , Jaroslaw Monkiewicz , Michael Horn
发明人： Helmut Mack , Ralf Laven , Peter Jenkner , Roland Edelmann , Dieter Barfurth , Albert-Johannes Frings , Burkhard Standke , Jaroslaw Monkiewicz , Michael Horn
IPC分类号： B32B904
CPC分类号： H01B3/44 , Y10T428/31663 , Y10T428/31801 , Y10T428/31855
摘要： The invention relates to the use of (1) a liquid functional organylorganyloxysilane bound to a carrier, or of a liquid (co)condensate derived from a functional organylorganyloxysilane and bound to a carrier for preparing cable compounds which comprise (2) a thermoplastic base polymer having polar functional groups and (3) a reinforcing or extending mineral filler.
摘要翻译：本发明涉及（1）与载体或衍生自功能性有机酰基氧基硅烷的液体（共）缩合物结合并结合到用于制备电缆化合物的载体的液体功能性有机羧基氧基硅烷的用途，其包含（2）热塑性基础聚合物具有极性官能团和（3）增强或延伸的矿物填料。

37. 发明授权

US06228936B1 Fluoroalkyl-functional organopolysiloxane-containing compositions 失效
标题翻译：含氟烷基官能的含有机聚硅氧烷的组合物
公开(公告)号：US06228936B1
公开(公告)日：2001-05-08
申请号：US09228641
申请日：1999-01-12
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C08L8308
CPC分类号： C14C9/00 , C03C17/30 , C03C25/40 , C04B41/4961 , C08G77/22 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , C23C2222/20 , D06M15/657 , D06M2101/06 , D06M2200/11 , D06M2200/12 , Y10T428/31663
摘要： The present invention provides an aqueous alcoholic fluoroalkyl functional group containing organopolysiloxane composition, which includes organopolysiloxanes of formula I: RO{Si(A)(CH3)z(OR)1−zO}a{Si(B)(R2)y(OR)1−yO}b{Si(C)(CH3)O}c{Si(D)(OR)O}dR.(HX)e (I) wherein A, B, C, D, R, R2, X, z, y, a, b, c, d and e are defined in the claims. The present invention also provides methods for making the fluoroalkyl functional group containing organopolysiloxane composition as well as methods of using same.
摘要翻译：本发明提供含有有机聚硅氧烷组合物的含水醇的氟代烷基官能团，其包括式I的有机聚硅氧烷：其中A，B，C，D，R，R 2，X，z，y，a，b，c，d和e是在权利要求中限定。本发明还提供了制备含氟烷基官能团的有机聚硅氧烷组合物的方法以及使用它们的方法。

38. 发明授权

US6054601A Fluoroalkyl-functional organopolysiloxane-containing compositions based on water, a process for their preparation and their use 失效
标题翻译：基于水的含氟烷基官能的有机聚硅氧烷的组合物，其制备方法及其应用
公开(公告)号：US6054601A
公开(公告)日：2000-04-25
申请号：US93681
申请日：1998-06-09
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C08L83/08 , B27K3/15 , C03C17/30 , C04B41/49 , C04B41/64 , C04B41/84 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , D06M15/643 , D06M15/657 , D21H17/59 , D21H21/16 , C07F7/08
CPC分类号： C04B41/009 , C03C17/30 , C04B41/4961 , C04B41/64 , C04B41/84 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , D06M15/6436 , D06M15/657 , D21H17/59 , B05D1/18 , B05D2201/00 , B05D2202/00 , B05D2203/20 , B05D2203/22 , B05D2203/24 , B05D2203/30 , B05D2203/35 , B05D5/08 , B05D5/083 , C04B2111/1012 , C04B2111/203 , C04B2111/27 , C23C2222/20 , D06M2101/06 , D21H21/16 , Y10T428/24355 , Y10T428/24372 , Y10T428/2438 , Y10T428/24388 , Y10T428/24405 , Y10T428/24994 , Y10T428/249946 , Y10T428/249947 , Y10T428/249974 , Y10T428/8305
摘要： Organopolysiloxane containing compositions are prepared by mixing an organopolysiloxane containing an aminoalkyl group, an organopolysiloxane containing a fluoroalkyl group, and optionally, organopolysiloxanes containing alkyl groups, together with water, or a water/acid mixture, or a water/acid/alcohol mixture, where the mixture is adjusted to have a pH in the range of 1-8, then removing the alcohol already present or formed during reaction.
摘要翻译：含有机聚硅氧烷的组合物通过将含有氨基烷基的有机聚硅氧烷，含氟烷基的有机聚硅氧烷和任选的含有烷基的有机聚硅氧烷，水或水/酸混合物或水/酸/醇混合物混合而制备，其中将混合物调节至pH在1-8范围内，然后除去反应中已经存在或形成的醇。

39. 发明授权

US5885341A Organopolysiloxane-containing, water-based compositions containing glycidal ether, acrylic and/or methacrylic functional groups, process for their preparation, and their use 失效
标题翻译：含有有机聚硅氧烷的含有缩水甘油醚，丙烯酸和/或甲基丙烯酸官能团的水基组合物，其制备方法及其用途
公开(公告)号：US5885341A
公开(公告)日：1999-03-23
申请号：US927283
申请日：1997-09-11
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Michael Horn , Peter Jenkner , Ralf Laven , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C08L83/07 , C08G77/18 , C08G77/20 , C08G77/26 , C08L83/08 , C09D183/08 , C09D183/06 , C09D183/07
CPC分类号： C08G77/18 , C08G77/20 , C08G77/26
摘要： Organopolysiloxane-containing, water-based compositions which are essentially free from organic solvents, have a flash point of above 70.degree. C. and liberate essentially no alcohols through hydrolysis on dilution with water, and which contain, as functional groups, glycidyl ether alkyl, acryloxyalkyl and/or methacryloxyalkyl groups, where each silicon in the organopolysiloxane carries one functional group, as well to a process for the preparation of such organopolysiloxane-containing compositions and to their use.
摘要翻译：基本上不含有机溶剂的含有机聚硅氧烷的水基组合物具有高于70℃的闪点，并且在用水稀释时通过水解基本上不释放醇，并且其含有作为官能团的缩水甘油醚烷基，丙烯酰氧基烷基和/或甲基丙烯酰氧基烷基，其中有机聚硅氧烷中的每个硅都带有一个官能团，以及制备这种含有机聚硅氧烷的组合物的方法及其应用。

40. 发明授权

US5849942A Fluoroalkyl-functional organopolysiloxane-containing compositions 失效
标题翻译：含氟烷基官能的含有机聚硅氧烷的组合物
公开(公告)号：US5849942A
公开(公告)日：1998-12-15
申请号：US984163
申请日：1997-12-03
申请人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
发明人： Burkhard Standke , Roland Edelmann , Albert-Johannes Frings , Ralf Laven , Michael Horn , Peter Jenkner , Helmut Mack , Jaroslaw Monkiewicz
IPC分类号： C09K3/00 , C03C17/30 , C03C25/40 , C04B41/49 , C08G77/22 , C08G77/24 , C08G77/26 , C08L83/08 , C09D5/00 , C09D183/08 , C09K3/18 , C14C9/00 , C23C30/00 , D06M15/657 , C07F7/08
CPC分类号： C14C9/00 , C03C17/30 , C03C25/40 , C04B41/4961 , C08G77/22 , C08G77/24 , C08G77/26 , C09D183/08 , C09K3/18 , C23C30/00 , D06M15/657 , C23C2222/20 , D06M2101/06 , D06M2200/11 , D06M2200/12 , Y10T428/31663
摘要： An aqueous alcoholic fluoroalkyl functional group containing organopolysiloxane- composition, comprising: organopolysiloxanes of formula I: RO�Si(A)(CH.sub.3).sub.z (OR).sub.1-z O!.sub.a �Si(B)(R.sup.2).sub.y (OR).sub.1-y O!.sub.b �Si(C)(CH.sub.3)O!.sub.c �Si(D)(OR)O!.sub.d R.multidot.(HX)(I) wherein A is an aminoalkyl radical derived from the compound of formula II:H.sub.2 N(CH.sub.2).sub.f (NH).sub.g (CH.sub.2).sub.h Si(OR).sub.3-z (CH.sub.3).sub.z (II) wherein 0.ltoreq.f.ltoreq.6, 9=0 if f=0 and g=1 if f>0, 0.ltoreq.h.ltoreq.6 and 0.ltoreq.z.ltoreq.1, and B is a fluoroalkyl radical derived from the compound of formula III: R.sup.1 --Y--(CH.sub.2).sub.2 Si(R.sup.2)y(OR).sub.3-y (III) wherein R.sup.1 is a mono-, oligo- or perfluorinated alkyl group having 1-9 C atoms or a mono-, oligo- or perfluorinated aryl group, Y is a CH.sub.2, O or S group, R.sub.2 is a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group and 0.ltoreq.y.ltoreq.1, and C is an alkyl radical derived from the compound of formula IV: R.sup.3 --Si(CH.sub.3)(OR).sub.2 (IV) and D is also an alkyl radical derived from the compound of formula V: R.sup.3 --Si(OR).sub.3 (V) wherein R.sup.3 in the preceding formulae is in each case identical or different, and is a linear, branched or cyclic alkyl group having 1-8 C atoms, R in the preceding formulae is in each case identical or different, and is a linear, branched or cyclic alkyl group having 1-8 C atoms or an aryl group, and HX is an acid, in which X is an inorganic or organic acid radical, and 0.ltoreq.y.ltoreq.1, 0.ltoreq.z.ltoreq.1, a>0, b>0, c>0, d>0, e>0 and (a+b+c+d).gtoreq.2.
摘要翻译：含有有机聚硅氧烷组合物的含水醇的氟代烷基官能团包括：式I的有机聚硅氧烷：RO [Si（A）（CH3）z（OR）1-zO] a [Si（B）（R2）y（OR） yO] b [Si（C）（CH3）O] c [Si（D）（OR）O] dRx（HX）（I）其中A是衍生自式II化合物的氨基烷基：H 2 N（CH 2）f （NH）g（CH 2）h Si（OR）3-z（CH 3）z（II）其中0 0，则g = R =（Y） - （CH 2）2 Si（R 2）y（OR）3-y （III）其中R1是具有1-9个C原子的单，低聚或全氟烷基或单，低聚或全氟化的芳基，Y是CH 2，O或S基团，R 2是直链，支链或具有1-8个碳原子或芳基且0≤y≤1的环状烷基，C是衍生自式IV化合物的烷基：R3-Si（CH3）（OR）2（ IV），D也是衍生自式V化合物的烷基：R 3 -Si（OR）3（V）其中前述通式中的R 3在每种情况下相同或者不同的是具有1-8个C原子的直链，支链或环状的烷基，前述式中的R各自相同或不同，为具有1-8个C原子的直链，支链或环状的烷基或芳基，HX是酸，其中X是无机或有机酸基，且0≤z≤1，a> 0，b> 0， c> 0，d> 0，e> 0和（a + b + c + d）> / = 2。

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