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31. 发明授权

US5633004A Granular agent for ruminants and process for producing the same 失效
标题翻译：反刍动物颗粒剂及其制备方法
公开(公告)号：US5633004A
公开(公告)日：1997-05-27
申请号：US480033
申请日：1995-06-07
申请人： Kunio Nishimura , Toshio Morita
发明人： Kunio Nishimura , Toshio Morita
IPC分类号： A23K1/00 , A23K1/18
CPC分类号： A61K9/5073 , A23K40/35 , Y10S426/807
摘要： Disclosed is the feed or feed additive granular agent containing a physiologically active substance and a coating layer having a laminar structure in which the tabular crystals are arranged in a laminated state. The coating layer comprises (a) one or more substances selected from the group consisting of a specific fatty acid or ester thereof, a specific animal or vegetable fat and fatty oil which may be hardened by hydrogenation, and a specific wax, and (b) tabular crystals of a substance which is sparingly water-soluble under a neutral condition but is readily water-soluble under an acidic condition and which has an average particle size of 5 to 30 .mu.m, wherein said coating layer is present in a coating ratio of 5% by weight or more and 50% by weight or less, wherein said first coating material and said second coating material are in a proportion of 3:2 to 1:3 by weight, and process for producing the same. The granular agent has a high mechanical strength, increased durability in the rumen and superiority in solubility and absorption of the physiologically active substance of said agent in the abomasum or downstream thereof resulting in efficient breeding, growth, or lactation of ruminants.
摘要翻译：公开了含有生理活性物质的进料或饲料添加剂颗粒剂和层状结构的层状结构的涂层。涂层包含（a）一种或多种选自特定脂肪酸或其酯的物质，可通过氢化硬化的特定动物或植物脂肪和脂肪油以及特定的蜡，和（b）在中性条件下微溶于水但在酸性条件下容易溶于水并且平均粒度为5〜30μm的物质的片状晶体，其中所述涂层以 5重量％以上且50重量％以下，其中所述第一涂料和所述第二涂料的重量比为3:2至1:3，以及其制备方法。颗粒剂具有高机械强度，瘤胃的耐久性以及所述药物在皱胃或下游的生理活性物质的溶解度和吸收性优异性，从而导致反刍动物的有效育种，生长或哺乳。

32. 发明授权

US07569161B2 Electrically conducting polymer and production method and use thereof 有权
标题翻译：导电聚合物及其制备方法及用途
公开(公告)号：US07569161B2
公开(公告)日：2009-08-04
申请号：US10570140
申请日：2004-09-01
申请人： Yuji Nagao , Ryuji Yamamoto , Toshio Morita
发明人： Yuji Nagao , Ryuji Yamamoto , Toshio Morita
IPC分类号： H01B1/24
CPC分类号： C08K7/06 , C08J3/201 , C08K3/04 , C08K2201/016 , C08L101/12 , H01B1/24
摘要： The invention provides a production method of a conductive polymer, comprising a step of blending a polymer in a state of a melt viscosity of 600 Pa·s or less at a shear rate of 100 s−1 with a vapor grown carbon fiber in 1 to 15 mass at a mixing energy of 1,000 mJ/m3 or less, and a conductive polymer obtained thereby. Preferably, a vapor grown carbon fiber used has an outer fiber diameter of 80 to 500 nm, an aspect ratio of 40 to 1,000, a BET specific surface area of 4: to 30 m2/g, a do02 of 0.345 nm or less according to an X-ray diffraction method, and a ratio (Id/Ig) of 0.1 to 2 wherein Id and Ig each represent peak heights of a band ranging from 1,341 to 1,349 cm−1 and a band ranging from 1,570 to 1,578 cm−1 respectively, according to a Raman scattering spectrum. According to the invention, an excellent conductivity can be attained by compounding vapor grown carbon fiber in a smaller amount than in a conventional method.
摘要翻译：本发明提供一种导电聚合物的制造方法，包括以100s -1的剪切速度将熔融粘度为600Pa·s以下的聚合物与气相生长碳纤维在1〜 15质量份，混合能量为1,000mJ / m 3以下，由此得到的导电性聚合物。优选使用的气相生长碳纤维的外纤维直径为80〜500nm，纵横比为40〜1000，BET比表面积为4〜30m 2 / g，do02为0.345nm以下，根据 X射线衍射法和0.1〜2的比（Id / Ig），其中Id和Ig分别表示1,341〜1349cm -1的谱带的峰高和1,570〜1578cm -1的谱带，根据拉曼散射光谱。根据本发明，可以通过以比常规方法更少的量将气相生长的碳纤维复合而获得优异的导电性。

33. 发明申请

US20080287590A1 RESIN CRYSTALLIZATION PROMOTER AND RESIN COMPOSITION 审中-公开
标题翻译：树脂结晶促进剂和树脂组合物
公开(公告)号：US20080287590A1
公开(公告)日：2008-11-20
申请号：US12177026
申请日：2008-07-21
申请人： Tatsuhiro TAKAHASHI , Toshio Morita
发明人： Tatsuhiro TAKAHASHI , Toshio Morita
IPC分类号： C08K3/04
CPC分类号： C08K7/06 , C08K2201/016
摘要： The present invention relates to a method for producing a resin composition having a crystallized and orderly arranged structure. The method comprises kneading an amorphous thermoplastic resin with a resin crystallization promoter to form a mixture, wherein the resin crystallization promoter comprises vapor grown carbon fibers, each fiber filament of the carbon fibers having a diameter of 0.001 μm to 5 μm and an aspect ratio of 5 to 15,000, the fibers having undergone a graphitization at 1,500° C. or higher, and subsequently subjecting the mixture to annealing at a temperature of from 55° C. higher than the glass transition point of the resin to a temperature 75° C. higher than the glass transition point of the resin. The crystallization promoter and annealing provide a thermoplastic resin composition, which, when molded, exhibits improved strength and tribological characteristics.
摘要翻译：本发明涉及一种具有结晶有序排列结构的树脂组合物的制造方法。该方法包括将无定形热塑性树脂与树脂结晶促进剂混合以形成混合物，其中树脂结晶促进剂包括气相生长碳纤维，碳纤维的每个纤维长丝的直径为0.001μm至5μm，纵横比为 5至15,000，纤维在1500℃或更高温度下经历石墨化，随后将混合物在比树脂的玻璃化转变点高55℃的温度下退火至75℃。高于树脂的玻璃化转变点。结晶促进剂和退火提供了一种热塑性树脂组合物，其在模制时表现出改进的强度和摩擦学特性。

34. 发明申请

US20070258881A1 Production Method of Vapor-Grown Carbon Fiber and Apparatus Therefor 有权
标题翻译：气相生长碳纤维的生产方法及其设备
公开(公告)号：US20070258881A1
公开(公告)日：2007-11-08
申请号：US11658231
申请日：2005-07-22
申请人： Eiji Kambara , Tomoaki Yoshida , Toshio Morita
发明人： Eiji Kambara , Tomoaki Yoshida , Toshio Morita
IPC分类号： D01F9/12 , B32B5/02
CPC分类号： B82Y30/00 , D01F9/127 , D01F9/1272 , D01F9/1276 , D01F9/133
摘要： The invention provides a method of producing vapor grown carbon fiber by vapor-phase reaction conducted by supplying carbon source compounds and a catalyst or a catalyst precursor into a heating zone, wherein at least one of the carbon source compound and the catalyst or the catalyst precursor is solid at room temperature and the solid compound is supplied in gas form into the heating zone from a material supplier filled with the solid material alone at a constant amount. The production method according to the invention enables efficient and stable production of vapor phase carbon fiber even by using a high-volume production equipment.
摘要翻译：本发明提供了一种通过气相反应生产气相生长碳纤维的方法，其通过将碳源化合物和催化剂或催化剂前体供给到加热区中进行，其中至少一种碳源化合物和催化剂或催化剂前体在室温下为固体，固体化合物以固体量从填充有固体材料的材料供应器以气体形式供应到加热区中。根据本发明的制造方法，即使通过使用大批量的生产设备也能够有效且稳定地生产气相碳纤维。

35. 发明申请

US20070042901A1 Porous body, production method thereof and composite material using the porous body 有权
标题翻译：多孔体，其制造方法和使用多孔体的复合材料
公开(公告)号：US20070042901A1
公开(公告)日：2007-02-22
申请号：US10556431
申请日：2004-05-12
申请人： Takashi Kurose , Tatsuhiro Takahashi , Chiaki Sotowa , Toshio Morita
发明人： Takashi Kurose , Tatsuhiro Takahashi , Chiaki Sotowa , Toshio Morita
IPC分类号： B01J21/18
CPC分类号： C08J9/0085 , B01J21/18 , B01J31/06 , B01J31/061 , B01J31/08 , B01J32/00 , B01J35/002 , B01J35/0033 , B01J35/023 , B01J35/026 , B01J35/06 , B01J35/10 , B01J35/1014 , B01J37/32 , B22F2998/10 , C02F1/283 , C02F2303/185 , C04B38/0045 , C04B41/009 , C04B41/48 , C04B41/4888 , C04B41/51 , C04B41/63 , C04B41/69 , C04B41/83 , C04B41/88 , C04B2111/00793 , C04B2111/0081 , C08J9/26 , C08J9/28 , C08J9/40 , C08J2201/038 , C08J2201/048 , C08J2201/0504 , C08J2305/00 , C08J2375/04 , C22C47/08 , H01M4/9083 , H01M4/926 , H01M8/0234 , Y02P70/56 , Y10S977/842 , Y10T428/249927 , Y10T428/24994 , Y10T428/30 , C04B35/52 , C04B38/04 , C04B40/0078 , C04B14/386 , C04B30/02 , C04B38/00 , C04B38/0074 , C04B38/10 , C04B41/457 , C04B41/4523 , C04B35/83 , C22C47/06 , B22F3/114
摘要： A porous material comprising vapor grown carbon fiber in an amount of 10 to 90 mass %, fiber filaments of the carbon fiber forming a three-dimensional network and having a diameter of 1 to 1,000 nm, an aspect ratio of 5 to 15,000, a specific surface area (by BET method) of 2 to 2,000 m2/g, and the ratio of the intensity of the peak at 1,360 cm−1 in a Raman scattering spectrum of the carbon fiber to that of the peak at 1,580 cm−1 in the spectrum(I1360/I1580) is 0.1 to 2.0, wherein the porosity of the porous material (V/V0) is 0.50 to 0.99 and a specific surface area is 5 to 1,000 m2/g; and a production method and use thereof. The vapor grow carbon fiber impregnated in the porous material of the present invention does not contain aggregates and a three-dimensional network is formed between the fiber filaments, wherein length of each of the fiber filaments is maintained. Therefore, the vapor grown carbon fiber enables to readily produce a composite material (porous material), in which even a small amount of addition of vapor grown carbon fiber can exhibit sufficient effect.
摘要翻译： 10.一种多孔材料，其含有10〜90质量％的蒸气生长碳纤维，所述碳纤维的纤维丝形成三维网状物，直径为1〜1000nm，长径比为5〜15000，表面积（BET法）为2〜2000μm2 / g，拉曼散射光谱中1,360cm -1处的峰强度比为在光谱（I 1360/1580℃）中1580cm -1处的峰的碳纤维为0.1〜2.0，其中，多孔材料的孔隙率（V / V 0）为0.50〜0.99，比表面积为5〜1000m 2 / g; 及其制造方法及其用途。浸渍在本发明的多孔材料中的蒸气生长碳纤维不含有聚集体，并且在纤维长丝之间形成三维网络，其中维持每根纤维丝的长度。因此，气相生长碳纤维能够容易地生产即使少量添加气相生长碳纤维也能发挥足够的效果的复合材料（多孔材料）。

36. 发明申请

US20060257309A1 Carbon fiber, method for producing the same and apparatus therefor 审中-公开
标题翻译：碳纤维，其制造方法及其设备
公开(公告)号：US20060257309A1
公开(公告)日：2006-11-16
申请号：US11487459
申请日：2006-07-17
申请人： Toshio Morita , Yoshihisa Sakamoto , Yutaka Suhara , Kunio Nishimura
发明人： Toshio Morita , Yoshihisa Sakamoto , Yutaka Suhara , Kunio Nishimura
IPC分类号： D01F9/12
CPC分类号： D01D10/02 , D01F9/12
摘要： An object of the present invention is to provide a method and apparatus for heat-treating carbon fiber, in which impairment of a furnace caused by solidification of a transition metal impurity serving as a catalyst raw material is prevented, and the amount of the metal, such as Fe, Co, or Ni, contained in the carbon fiber is reduced. In the present invention, a vaporized metal impurity is contained in an inert gas that is passed through a furnace, and the gas is discharged from a high-temperature section of the furnace. The impurity contained in the gas discharged from the furnace is cooled to solidify, and then recovered. The resultant gas is recycled as an inert gas in the furnace.
摘要翻译：本发明的目的是提供一种用于热处理碳纤维的方法和装置，其中防止了由作为催化剂原料的过渡金属杂质的凝固导致的炉的损伤，并且金属的量，例如包含在碳纤维中的Fe，Co或Ni减少。在本发明中，在通过炉的惰性气体中含有汽化金属杂质，从炉的高温部排出气体。将从炉中排出的气体中所含的杂质冷却固化，然后回收。所得气体在炉中作为惰性气体再循环。

37. 发明授权

US06998176B2 Fine carbon fiber, method for producing the same and electrically conducting material comprising the fine carbon fiber 有权
公开(公告)号：US06998176B2
公开(公告)日：2006-02-14
申请号：US10699645
申请日：2003-11-04
申请人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
发明人： Toshio Morita , Hitoshi Inoue , Kunio Nishimura , Yutaka Suhara , Satoshi Ohshima , Motoo Yumura
IPC分类号： D01F9/12
CPC分类号： B82Y30/00 , D01F9/127 , Y10T428/2913 , Y10T428/2918 , Y10T428/2924 , Y10T428/2929 , Y10T428/30
摘要： A fine carbon fiber having an outer diameter of about 1 to about 80 nm and an aspect ratio of 10 to 30,000, comprising a hollow center portion and a multi-layer sheath structure of a plurality of carbon layers, the layers forming annual rings, wherein the sheath-forming carbon layers form an incomplete sheath, i.e., the carbon layers are partially broken or disrupted in a longitudinal direction, and the outer diameter of the carbon fiber and/or the diameter of the hollow center portion are not uniform in a longitudinal direction. The carbon fiber is obtained by instantaneously reacting a carrier gas at a high temperature and an organic compound gas kept at a temperature below the decomposition temperature of the transition metal compound and has a conductivity equivalent to that of a conventional vapor phase method and is useful as a filler material in resins, rubbers, paints and the like.

38. 发明授权

US06998171B2 Fine carbon fiber and method for producing the same 有权
公开(公告)号：US06998171B2
公开(公告)日：2006-02-14
申请号：US10393983
申请日：2003-03-24
申请人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
发明人： Toshio Morita , Hitoshi Inoue , Yutaka Suhara
IPC分类号： B32B27/04
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/162 , C01B2202/34 , C01B2202/36 , D01F9/127 , Y10T428/2419 , Y10T428/24777 , Y10T428/249924 , Y10T428/249927 , Y10T428/249933 , Y10T428/24994 , Y10T428/2916 , Y10T428/2918
摘要： A fine carbon fiber having a multilayer structure having stacked cylindrical carbon sheets and a center axis having a hollow structure. The fine carbon fiber has an outer diameter of 2 to 300 nm and an aspect ratio of 10 to 15,000, and at least one cylindrical carbon sheet layer among the multiple layers is folded at an end part of the carbon fiber and continued to another cylindrical carbon sheet. The folded and continued cylindrical carbon sheets form a cylindrical structure opened at the end part.

39. 发明申请

US20050110499A1 High-sensitivity measuring instrument 有权
标题翻译：高灵敏度测量仪器
公开(公告)号：US20050110499A1
公开(公告)日：2005-05-26
申请号：US10508225
申请日：2003-03-19
申请人： Yoshio Sunaoka , Shinichi Ohashi , Toshio Morita , Masashi Fujita
发明人： Yoshio Sunaoka , Shinichi Ohashi , Toshio Morita , Masashi Fujita
IPC分类号： G01R27/22 , G01N27/06 , G01N27/08 , G01N30/64 , G01N27/02
CPC分类号： G01N27/06
摘要： A high-sensitivity measuring instrument comprising at least two sensors for detecting the same characteristics by touching a substance being measured with a specified time difference, wherein the between detection signals taken out simultaneously from respective sensors is determined, the difference between characteristic values upon elapsing the specified time difference is determined from the difference between detection signals, a reference time of measurement and a reference characteristic value at that time are preset, a time axis having a time pitch of a specified time difference is set, and a measurement value is obtained at a point in time elapsing an arbitrary time pitch from the reference time. Objective measurement characteristics can be detected by the measuring instrument not in the form of difference or variation but as an absolute value with high accuracy and sensitivity.
摘要翻译：一种高灵敏度测量仪器，包括至少两个传感器，用于通过以指定的时间差触摸被测量的物质来检测相同的特性，其中确定从各个传感器同时取出的检测信号之间的差值，根据检测信号之间的差异来确定规定的时间差，测量的基准时间和此时的基准特性值被预先设定为具有指定时间间隔的时间间隔的时间轴，并且在从参考时间经过一个任意时间间隔的时间点。客观测量特性可以通过测量仪器检测，不是以差异或变化的形式，而是以高精度和高灵敏度的绝对值。

40. 发明授权

US06844061B2 Fine carbon fiber and composition thereof 有权
标题翻译：细碳纤维及其组成
公开(公告)号：US06844061B2
公开(公告)日：2005-01-18
申请号：US10220817
申请日：2002-07-31
申请人： Toshio Morita , Ryuji Yamamoto
发明人： Toshio Morita , Ryuji Yamamoto
IPC分类号： C08K7/06 , D01F9/127 , D01F6/00
CPC分类号： B82Y30/00 , C08K7/06 , C08K2201/016 , D01F9/127 , Y10T428/2918 , Y10T428/2929 , Y10T428/2935 , Y10T428/2975
摘要： A fine carbon fiber, the main body of each fiber filament of the fiber having an outer diameter of about 1 to about 500 nm and an aspect ratio of about 10 to about 15,000 and comprising a hollow space extending along its center axis and a multi-layer sheath structure consisting of a plurality of carbon layers, the layers forming concentric rings, wherein the fiber filament has a nodular portion which is formed of outwardly protruding carbon layers or formed of a locally increased number of carbon layers. A similar fine carbon fiber, in which the fiber filament has repeatedly enlarged protruding portions and the filament diameter varies along with the length of the filament, the ratio of the diameter (d″) of a fiber filament of the fiber as measured at the outwardly enlarged portions to the diameter (d) of a fiber filament of the fiber as measured at a position at which no outwardly enlarged portions is present; i.e., d″/d, being about 1.05 to about 3, is also provided.
摘要翻译：一种细碳纤维，纤维的每个纤维长丝的主体具有约1至约500nm的外径和约10至约15,000的纵横比，并且包括沿着其中心轴延伸的中空空间，由多个碳层组成的层鞘结构，所述层形成同心环，其中所述纤维丝具有由向外突出的碳层形成或由局部增加数量的碳层形成的结节部分。类似的细碳纤维，其中纤维丝具有反复扩大的突出部分，并且丝直径随着丝的长度而变化，纤维长丝的直径（d“）在纤维长度在不存在向外扩大的部分的位置处测量的纤维的纤维长丝的直径（d）向外扩大部分; 即d“/ d，为约1.05至约3。

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