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31. 发明授权

US4326073A Production of anhydrous or substantially anhydrous formic acid 失效
标题翻译：生产无水或基本无水的甲酸
公开(公告)号：US4326073A
公开(公告)日：1982-04-20
申请号：US131501
申请日：1980-03-18
申请人： Dieter Wolf , Rudolf Schmidt , Ulrich Block , Hartmut Schoenmakers , Kaspar Bott , Gerd Kaibel
发明人： Dieter Wolf , Rudolf Schmidt , Ulrich Block , Hartmut Schoenmakers , Kaspar Bott , Gerd Kaibel
IPC分类号： C07C53/02 , C07C27/02 , C07C51/00 , C07C51/09 , C07C51/44 , C07C51/48 , C07C67/00
CPC分类号： C07C51/09 , C07C51/48
摘要： Anhydrous or substantially anhydrous formic acid is obtained by hydrolysis of methyl formate, in a process wherein(a) methyl formate is hydrolyzed,(b) the methanol and excess methyl formate are distilled from the hydrolysis mixture obtained,(c) the bottom product of distillation (b), consisting of formic acid and water, is extracted, in a liquid-liquid extraction, with an extractant which in the main takes up the formic acid,(d) the resulting extract phase, consisting of formic acid, the extractant and a part of the water, is subjected to distillation,(e) the top product obtained from this distillation and consisting of all or part of the water introduced into the distillation, and part of the formic acid, is recycled, as vapor, into the lower part of the distillation column of stage (b),(f) the bottom product of distillation stage (d), consisting of the extractant, with or without part of the water, and the greater part of the formic acid, is separated by distillation into anhydrous or substantially anhydrous formic acid and the extractant, and(g) the extractant leaving stage (f) is recycled to the process.
摘要翻译：在（a）甲酸甲酯水解的过程中，（甲）甲醇和过量的甲酸甲酯从得到的水解混合物中蒸馏得到，（c）甲酸叔丁酯的底部产物蒸馏（b）由甲酸和水组成，在液 - 液萃取中用主要萃取甲酸的萃取剂萃取，（d）所得提取相由甲酸，萃取剂和一部分水进行蒸馏，（e）由该蒸馏获得的顶部产物，并且由引入蒸馏的全部或部分水和部分甲酸作为蒸气循环进入阶段（b）的蒸馏塔的下部，（f）蒸馏阶段（d）的底部产物，由萃取剂组成，有或没有部分水和大部分甲酸分离通过蒸馏成无水粗粉或基本上无水的甲酸和萃取剂，和（g）离开阶段（f）的萃取剂再循环到该方法中。

32. 发明授权

US4289676A Binders, impregnating agents and coating agents based on an aqueous dispersion of an amide-containing copolymer 失效
标题翻译：基于含酰胺共聚物的水分散体的粘合剂，浸渍剂和包衣剂
公开(公告)号：US4289676A
公开(公告)日：1981-09-15
申请号：US145695
申请日：1980-05-01
申请人： Bernhard Czauderna , Andreas Einwiller , Kaspar Bott
发明人： Bernhard Czauderna , Andreas Einwiller , Kaspar Bott
IPC分类号： C08F8/00 , C08F8/28 , C08F220/58 , C08L9/00 , C08L21/02 , C08L25/00 , C08L25/10 , C08L27/06 , C08L31/04 , C08L33/04 , C08L33/06 , C08L33/18 , C08L33/20 , C09D201/02 , D04H1/4258 , D04H1/4334 , D04H1/435 , D04H1/587 , D04H1/645 , D04H1/65 , D04H1/74 , D06M15/29 , C08L33/24
CPC分类号： D04H1/587 , C08F220/58 , D04H1/4258 , D04H1/4334 , D04H1/435 , D04H1/645 , D04H1/65 , D04H1/74 , D06M15/29
摘要： Binders, impregnating agents and coating agents based on an aqueous dispersion of an amide-containing copolymer, wherein the copolymer contains recurring units of the general formula I ##STR1## where R is H and/or CH.sub.3, eliminate virtually no formaldehyde in use and may advantageously be used as binders for bonding nonwovens.
摘要翻译：基于含酰胺共聚物的水性分散体的粘合剂，浸渍剂和涂布剂，其中所述共聚物含有通式I的重复单元，其中R是H和/或CH 3，实际上在使用中消除了甲醛，并且可以有利地用作粘合无纺布的粘合剂。

33. 发明授权

US5656688A Carbamoylhydroxylamines and polymer-containing solution or dispersion thereof 失效
标题翻译：氨基甲酰羟基胺和含聚合物的溶液或其分散体
公开(公告)号：US5656688A
公开(公告)日：1997-08-12
申请号：US535054
申请日：1995-10-30
申请人： Gerhard Bauer , Karl Haeberle , Roland Baumstark , Kaspar Bott
发明人： Gerhard Bauer , Karl Haeberle , Roland Baumstark , Kaspar Bott
IPC分类号： C07C291/02 , C07C271/60 , C08F16/34 , C08F212/00 , C08F216/34 , C08F218/02 , C08F218/04 , C08G18/80 , C08K5/32 , C08L25/00 , C08L31/04 , C08L33/04 , C08L33/06 , C08L101/00 , C09D7/12 , C08L39/00 , C08L75/00 , C08F8/32 , C07C271/00
CPC分类号： C08G18/807 , C07C271/60 , C08G18/80 , Y10S528/905 , Y10T428/31551
摘要： A compound of the formula ##STR1## where A is an n-valent organic radical and n is an integer greater than 1.
摘要翻译： PCT No.PCT / EP94 / 01283第 371 1995年10月30日第 102（e）1995年10月30日PCT PCT 1994年4月25日PCT公布。公开号WO94 / 25433 日期：1994年11月10日A式为其中A为n价有机基团且n为大于1的整数的化合物。

34. 发明授权

US5597466A Preparation of substantially salt-free aqueous solutions of bisaminoxyalkanes 失效
标题翻译：制备基本上无盐的双氨基链烷烃水溶液
公开(公告)号：US5597466A
公开(公告)日：1997-01-28
申请号：US279888
申请日：1994-07-26
申请人： Gerhard Bauer , Roland Baumstark , Kaspar Bott , Hartwig Voss
发明人： Gerhard Bauer , Roland Baumstark , Kaspar Bott , Hartwig Voss
IPC分类号： C07C239/20 , C08K5/32 , C25B3/00 , B65D83/04
CPC分类号： C07C239/20 , C08K5/32
摘要： Salt-free aqueous solutions of bisaminoxyalkanes (I) are prepared by a process in whicha) a dihaloalkane (II) is converted with a ketoxime (III) in an aqueous solution of a strong mineral base into the alkylene bisoxime ether (IV),b) the alkylene bisoxime ether (IV) is cleaved with a strong mineral acid and water to give the ketone and the salt of the mineral acid with the bisaminoxyalkane (I), and the ketone is separated off in a conventional manner,c) an alkali metal hydroxide is added to the remaining aqueous solution to liberate the bisaminoxyalkane (I) andd) the ionic components are removed from the resulting aqueous solution by electrodialysis.
摘要翻译：通过以下方法制备双氨基链烷烃（I）的无盐水溶液：其中a）将二卤代烷（II）在强矿物碱的水溶液中用酮肟（III）转化成亚烷基双肟醚（IV）， b）亚烷基双肟醚（Ⅳ）用强无机酸和水分解，得到酮和无机酸的盐与双氨基链烷烃（I），并以常规方式分离酮，c）将碱金属氢氧化物加入到剩余的水溶液中以释放出双氨基链烷烃（I），和d）通过电渗析从所得水溶液中除去离子组分。

35. 发明授权

US5175364A Preparation of carbonyl halides 失效
标题翻译：制备羰基卤化物
公开(公告)号：US5175364A
公开(公告)日：1992-12-29
申请号：US707840
申请日：1991-05-30
申请人： Kaspar Bott
发明人： Kaspar Bott
IPC分类号： C07C51/58
CPC分类号： C07C51/58
摘要： Carbonyl halides I ##STR1## where R.sup.1 is H, alkyl, cycloalkyl, haloalkyl or halocycloalkyl, R.sup.2 and R.sup.3 are each alkyl, cycloalkyl, haloalkyl or halocycloalkyl and may furthermore be bonded to one another to form a 5-membered to 7-membered ring andX is halogen,are prepared by reacting an alkyl halide II ##STR2## with carbon monoxide under superatmospheric pressure in the presence of a catalytic amount ofa) aluminum bromide and in the presence or absence of a solvent orb) aluminum chloride or bromide and in the presence of a halohydrocarbon and a carbonyl halide of the formula IIIR.sup.4 --CH.sub.2 --CO--Hal III, where R.sup.4 is hydrogen or C.sub.1 -C.sub.4 -alkyl and Hal is halogen.
摘要翻译：羰基卤化物I，其中R 1是H，烷基，环烷基，卤代烷基或卤代环烷基，R 2和R 3各自是烷基，环烷基，卤代烷基或卤代环烷基，并且还可以彼此键合形成5元至7元环和X是卤素，通过烷基卤化物II II与一氧化碳在超大气压下在催化量的溴化铝存在下和在存在或不存在溶剂的情况下反应制备，或b）氯化铝或溴化物存在下，并且在式III R 4 -CH 2 -CO-Hal III的卤代烃和羰基卤存在下，其中R 4是氢或C 1 -C 4 - 烷基，而Hal是卤素。

36. 发明授权

US4490558A Preparation of thioethers 失效
标题翻译：硫醚的制备
公开(公告)号：US4490558A
公开(公告)日：1984-12-25
申请号：US510934
申请日：1983-07-05
申请人： Kaspar Bott
发明人： Kaspar Bott
IPC分类号： C07C149/30
CPC分类号： C07C319/14 , C07C2101/14
摘要： Thioethers are prepared by a process wherein an alkali metal mercaptide is reacted with an alcohol and carbon monoxide or with a formate, and are useful starting materials for the preparation of dyes, crop protection agents, drugs and rubber auxiliaries.
摘要翻译：硫醚通过其中碱金属硫醇盐与醇和一氧化碳或与甲酸盐反应的方法制备，并且是制备染料，作物保护剂，药物和橡胶助剂的有用的起始材料。

37. 发明授权

US4370491A Continuous preparation of acetic acid esters 失效
标题翻译：连续制备乙酸酯
公开(公告)号：US4370491A
公开(公告)日：1983-01-25
申请号：US263470
申请日：1981-05-14
申请人： Kaspar Bott , Gerd Kaibel , Herwig Hoffmann , Rudolf Irnich , Eberhard Schaefer
发明人： Kaspar Bott , Gerd Kaibel , Herwig Hoffmann , Rudolf Irnich , Eberhard Schaefer
IPC分类号： C07C67/03 , B01D3/36 , C07C67/02 , C07C69/14 , C07C67/06
CPC分类号： C07C67/03 , Y10S203/06
摘要： A process for the preparation of acetic acid esters CH.sub.3 --CO--O--R.sup.1 (I, R.sup.1 =an organic radical other than methyl and ethyl) by alkali-catalyzed trans-esterification of an acetic acid ester CH.sub.3 --CO--O--R.sup.2 (II, R.sup.2 =methyl or ethyl) with an alcohol R.sup.1 --OH (III), accompanied by elimination of the alcohol R.sup.2 --OH (IV), wherein(a) the trans-esterification reaction is carried out in the middle section K.sub.M of a distillation column K, the alcohol III being fed as liquid into the upper zone and the ester II into the lower zone of K.sub.M,(b) the alkaline catalyst is introduced into the upper part K.sub.U of K,(c) the alcohol IV, or a mixture of IV and the ester II, is taken off the top of the column,(d) the mixture obtained from (c) (unless the alcohol IV alone is obtained) is separated in the column section K.sub.U or in a stripper column K.sub.S into IV and the azeotrope of II and IV, and the latter is recycled to the lower zone of K.sub.M,(e) the ester I is taken as vapor or liquid from the lower zone of the lower section K.sub.L of K and(f) the catalyst is either removed, or recycled to K.sub.U, in a conventional manner.
摘要翻译：通过乙酸酯CH3-CO-O-R2的碱催化反式酯化制备乙酸酯CH 3 -CO-O-R 1（I，R 1 =甲基和乙基以外的有机基）的方法 II，R 2 =甲基或乙基）与醇R 1 -OH（III）反应，同时除去醇R 2 -OH（Ⅳ），其中（a）酯交换反应在蒸馏塔K，醇III作为液体进料到上部区域，酯II进入KM的下部区域，（b）将碱性催化剂引入K的上部KU，（c）醇IV，或将IV和酯II的混合物从柱顶部取出，（d）从（c）获得的混合物（除非单独获得醇IV）在柱部分KU或汽提塔KS中分离进入IV和II和IV的共沸物，后者再循环到KM的下部区域，（e）将酯I作为蒸汽或液体从下部KL的下部区域中取出的K和（f）催化剂以常规方式被去除或再循环至KU。

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