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21. 发明授权

US5171821A Process for producing a phenolate and process for producing an aromatic polyether ketone employing it 失效
标题翻译：生产苯酚的方法和生产使用其的芳族聚醚酮的方法
公开(公告)号：US5171821A
公开(公告)日：1992-12-15
申请号：US359637
申请日：1989-05-31
申请人： Seiichi Nozawa , Hiroshi Noguchi , Fumitoshi Sakaguchi , Yuko Mihara
发明人： Seiichi Nozawa , Hiroshi Noguchi , Fumitoshi Sakaguchi , Yuko Mihara
IPC分类号： C07C45/64 , C07C45/84 , C07C49/83 , C07C205/38 , C07C205/45
CPC分类号： C07C45/84 , C07C45/64
摘要： A process for preparing a metal phenolate of the formula II:Cl--Ar.sub.1 COAr.sub.2 OM (II)wherein each of Ar.sub.1 and Ar.sub.2 which may be the same or different is a bivalent group of the formula: ##STR1## wherein each of R.sup.1 and R.sup.12 is a hydrogen atom, a halogen atom, an alkoxy group, a phenoxy group, an alkyl group, a cycloalkyl group, a phenyl group, an aralkyl group, an acyl group, a nitrile group, a nitro group or an acyloxy group, each of Y and Z is an oxygen atom or a ketone group, and each of n and m is an integer of from 0 to 4, and M is an alkali metal, which comprises reacting a phenol compound of the formula I:Cl--Ar.sub.1 COAr.sub.2 OH (I)wherein Ar.sub.1 and Ar.sub.2 are as defined above, with an alkali metal compound in the presence of water, and then removing water, characterized in that water is azeotropically distilled off together with an organic solvent capable of forming an azeotropic mixture with water.

22. 发明授权

US5120869A Herbicidal compounds 失效
公开(公告)号：US5120869A
公开(公告)日：1992-06-09
申请号：US432949
申请日：1989-11-07
申请人： David Cartwright
发明人： David Cartwright
IPC分类号： C07D213/64 , A01N31/14 , A01N31/16 , A01N33/22 , A01N35/04 , A01N37/02 , A01N37/10 , A01N37/18 , A01N37/34 , A01N37/40 , A01N39/00 , A01N39/02 , A01N39/04 , A01N41/06 , A01N43/40 , C07C43/263 , C07C43/29 , C07C43/295 , C07C47/277 , C07C47/575 , C07C49/255 , C07C49/84 , C07C51/367 , C07C59/125 , C07C59/68 , C07C65/21 , C07C67/00 , C07C67/31 , C07C69/67 , C07C69/712 , C07C69/92 , C07C201/12 , C07C205/38 , C07C229/20 , C07C231/02 , C07C233/25 , C07C233/43 , C07C235/20 , C07C235/24 , C07C243/28 , C07C253/30 , C07C255/16 , C07C255/54 , C07C255/59 , C07C259/08 , C07C303/40 , C07C311/51 , C07C311/57 , C07D213/643
CPC分类号： C07D213/643 , A01N31/16 , A01N33/22 , A01N35/04 , A01N37/40 , A01N39/00 , A01N39/02 , A01N39/04 , A01N41/06 , A01N43/40 , C07C205/38 , C07C243/28 , C07C255/16 , C07C255/54 , C07C259/08 , C07C311/51 , C07C311/57 , C07C43/29 , C07C43/295 , C07C47/277 , C07C47/575 , C07C49/255 , C07C49/84 , C07C59/68 , C07C69/712 , C07C2101/14
摘要： A herbicidal compound of formula (I): ##STR1## wherein X is O, S(O).sub.n or NR.sup.a where R.sup.a is H or alkyl and n is 0, 1 or 2;R.sup.1 is H or halo;R.sup.2 is N or CR.sup.3 where R.sup.3 is halo or NO.sub.2 ;R.sup.4 is H, halo, NO.sub.2, alkyl, haloalkyl, CN, CO.sub.2 alkyl, cycloalkyl, phenyl, COalkyl, COphenyl, CHO,OH, NH.sub.2, NHCOalkyl or alkoxyR.sup.5 is H, halo or optionally substituted alkyl;R.sup.6 is H, halo or optionally substituted alkyl; provided that at least one of R.sup.5 and R.sup.6 is halo;R.sup.7 is CN, CHO, COOR.sup.8, CONR.sup.8 R.sup.9, where R.sup.8 is H, optionally substituted alkyl, alkenyl, alkynyl or aryl and R.sup.9 is a group R.sup.8, SO.sub.2 alkyl, NR.sup.10 R.sup.11 or N.sup.+ R.sup.10 R.sup.11 R.sup.12 Z.sup.- where Z is an agriculturally acceptable anion e.g. chloride and R.sup.10, R.sup.11 and R.sup.12 are independently selected from hydrogen and alkyl. Processes for the preparation of these compounds and compositions containing them are also described.

23. 发明授权

US5117002A Preparation of diphenyl ether 失效
标题翻译：二苯醚的制备
公开(公告)号：US5117002A
公开(公告)日：1992-05-26
申请号：US640781
申请日：1991-01-14
申请人： Robert A. Buchanan , Jeffrey S. Stults
发明人： Robert A. Buchanan , Jeffrey S. Stults
IPC分类号： B01J31/04 , C07B61/00 , C07C41/01 , C07C45/72 , C07C51/367 , C07C201/12 , C07C205/38 , C07C205/44 , C07C205/59 , C07C213/00 , C07C217/90 , C07C255/54 , C08G73/06 , C08G73/10
CPC分类号： C07C255/54 , C07C201/12 , C07C253/30
摘要： A process for the production of diaryl ethers which comprises heating, to a temperature of 80.degree. C. to 220.degree. C., a compound of the formula ##STR1## wherein X and Y are selected from the group consisting of H, CN, CO.sub.2 H, CHO, NO.sub.2, and CF.sub.3, provided that both X and Y may not simultaneously be H, in a solvent, in the presence of an inorganic base selected from the group consisting of the alkali metal carbonates, bicarbonates, and hydroxides, and in the presence of a catalyst selected from the group consisting of benzoic acid, substituted benzoic acids, C2-C4 aliphatic carboxylic acids, and alkali metal salts of said acids.

24. 发明授权

US5110983A Hexafluoroisopropyl-containing monomers, process for their preparation and their use 失效
标题翻译：含六氟异丙基的单体，其制备方法及其应用
公开(公告)号：US5110983A
公开(公告)日：1992-05-05
申请号：US497553
申请日：1990-03-22
申请人： Jurgen Lau , Gunter Siegemund , Freimund Rohrscheid
发明人： Jurgen Lau , Gunter Siegemund , Freimund Rohrscheid
IPC分类号： B01J27/06 , C07B61/00 , C07C37/16 , C07C39/367 , C07C43/29 , C07C51/353 , C07C63/70 , C07C63/72 , C07C65/24 , C07C205/07 , C07C205/38 , C07C211/52 , C07C217/80 , C07C217/90 , C07C229/52 , C07C233/07 , C07C235/42 , C08G69/40 , C08G69/46 , C08G73/10
CPC分类号： C07C205/38 , C07C217/80 , C07C217/90 , C07C235/42 , C07C37/16 , C07C39/367 , C07C43/29 , C07C65/24
摘要： Compounds of the formula I ##STR1## can be prepared by various process steps from 2-(4-methylphenyl)-2-hexafluoroisopropanol.Hexafluoroisopropyl-containing monomers are important starting compounds in the preparation of linear polycarboxamides and polycarboximides.
摘要翻译：式I（I）的化合物可以通过从2-（4-甲基苯基）-2-六氟异丙醇的各种方法步骤制备。含六氟异丙基的单体是制备线性聚酰胺和聚卡马西平的重要起始化合物。

25. 发明授权

US5053544A Diamino compound and its intermediates 失效
标题翻译：二氨基化合物及其中间体
公开(公告)号：US5053544A
公开(公告)日：1991-10-01
申请号：US631448
申请日：1990-12-21
申请人： Shizuo Murata , Minoru Nakayama
发明人： Shizuo Murata , Minoru Nakayama
IPC分类号： C07C39/16 , C07C39/17 , C07C205/38 , C07C217/90 , C08G69/02 , C08G69/26 , C08G73/10
CPC分类号： C07C205/38 , C07C217/90 , C07C2101/14
摘要： A novel diamino compound and a dinitro compound and a diol compound as its derivatives are provided,which diamino compound is useful as a raw material for polyimide compounds for an aligning film in a liquid crystal display element exhibiting a high pretilt angle, and expressed by the formula ##STR1## wherein R.sub.1 to R.sub.6 each are H or 1-22C alkyl and may be the same as or different from one another, and R.sub.7 to R.sub.14 each are H or 1-3C alkyl and may be the same as or different from one another.
摘要翻译：提供了一种新的二氨基化合物和二硝基化合物和二醇化合物作为其衍生物，该二氨基化合物可用作表现出高预倾角的液晶显示元件中用于取向膜的聚酰亚胺化合物的原料，并且由式（1）其中R1至R6各自为H或1-22C烷基并且可以彼此相同或不同，并且R7至R14各自为H或1-3C烷基，并且可以与彼此不同

26. 发明授权

US5041604A Process for producing di(aryloxy)alkane 失效
标题翻译：制备二（芳氧基）烷烃的方法
公开(公告)号：US5041604A
公开(公告)日：1991-08-20
申请号：US540872
申请日：1990-06-20
申请人： Toranosuke Saito , Masakatu Kitani , Takashi Ishibashi
发明人： Toranosuke Saito , Masakatu Kitani , Takashi Ishibashi
IPC分类号： C07C65/21 , B01J23/02 , C07B31/00 , C07B41/04 , C07B61/00 , C07C41/00 , C07C41/01 , C07C41/16 , C07C43/20 , C07C45/00 , C07C49/84 , C07C51/00 , C07C67/00 , C07C201/00 , C07C201/12 , C07C205/38 , C07C253/00 , C07C253/30 , C07C255/37 , C07C255/54
CPC分类号： C07C41/16
摘要： A process for producing a high quality di(aryloxy)alkane with a high yield by the use of readily commercially available materials, without using any particular solvent or agent and by means of a simple operation and a general apparatus is provided, which process comprises subjecting a halogenated alkane of the formula (II)X--A--Y (II)wherein X and Y each represent a halogen atom and A represents a lower alkylene group, and a phenol of the formula (III) ##STR1## wherein R.sub.1 to R.sub.5 each are same or different, represent hydrogen, halogen, lower alkyl, lower alkoxy, carboxylic acid salt, acyl or nitro group, and may form a ring in conjunction of two adjacent groups,to condensation reaction in the presence of an alkali in an aqueous medium to form a di(aryloxy)alkane of the formula (I) ##STR2## and is characterized (i) by carrying out the condensation reaction in a molar ratio of the compound of the formula (II): the phenol of the formula (III): the alkali in terms of monovalent base of 1:1.5 to 3.0:1.5 to 3.0; or(ii) by carrying out the condensation reaction of the above (i) and adjusting the quantity of the aqueous medium phase after completion of the reaction can be 35% or less based on the oily phase; or(iii) by carrying out the condensation reaction of the above (i), feeding at least the alkali among the reaction components with progress of the reaction and adjusting the quantity of the aqueous medium phase as described in the above (ii).
摘要翻译：提供了一种通过使用容易商业化的材料生产高质量的二（芳氧基）烷烃的方法，而不使用任何特定的溶剂或试剂，并且通过简单的操作和一般的设备，该方法包括式（II）XAY（II）的卤化烷烃，其中X和Y各自表示卤素原子，A表示低级亚烷基，和式（III）的苯酚（III）其中R1至R5各自相同或不同，表示氢，卤素，低级烷基，低级烷氧基，羧酸盐，酰基或硝基，并且可以与两个相邻基团结合形成环，在碱的存在下在水性介质中进行缩合反应形成式（I）的二（芳氧基）烷烃（I），其特征在于（i）通过以式（II）的化合物与式（II）的苯酚的摩尔比进行缩合反应：式（III）：以碱为一价碱为1：1.5至3.0：1.5至3.0; 或者（ii）通过进行上述（i）的缩合反应，并且在反应完成后调整水介质相的量可以基于油相为35％以下。或者（iii）通过进行上述（i）的缩合反应，至少将反应成分中的碱与反应进行同时进行，并且如上述（ii）所述调节水相介质相的量。

27. 发明授权

US4914244A Process for preparing difluorochloromethoxybenzenes 失效
标题翻译：制备二氟氯甲氧基苯的方法
公开(公告)号：US4914244A
公开(公告)日：1990-04-03
申请号：US3096
申请日：1987-01-14
申请人： Albrecht Marhold
发明人： Albrecht Marhold
IPC分类号： B01J27/00 , C07B61/00 , C07C41/00 , C07C41/16 , C07C43/225 , C07C43/263 , C07C67/00 , C07C205/38 , C07C301/00 , C07C303/22 , C07C309/87 , C07C313/00 , C07C319/20 , C07C323/20
CPC分类号： C07C41/16 , C07C201/12
摘要： Difluorochloromethoxybenzenes are prepared by reacting phenols with trichloromethyl chloroformate (=di-phosgene) in the presence of hydrogen fluoride.
摘要翻译：在氟化氢存在下，苯酚与氯甲酸三氯甲酯（=二光气）反应制备二氟氯甲氧基苯。

28. 依法登记的发明

USH726H 2,4-bis-aryloxy-m-phenylenediamines and their use as couplers in oxidation dye compositions 失效
标题翻译： 2,4-二芳氧基 - 间苯二胺及其作为氧化染料组合物中的成色剂的用途
公开(公告)号：USH726H
公开(公告)日：1990-01-02
申请号：US1721
申请日：1987-01-09
申请人： Keith C. Brown , James E. Kijek
发明人： Keith C. Brown , James E. Kijek
IPC分类号： C07C205/12 , C07C205/38 , C07C217/90
CPC分类号： A61K8/411 , A61K8/415 , A61Q5/10 , C07C205/12 , C07C205/38 , C07C217/90
摘要： Compounds of formula: ##STR1## and oxidation hair dye compositions containing the same; also includes a process for dyeing hair with such compositions; Ar being an aryl radical.

29. 发明授权

US4522647A Substituted phenoxyalkanediones and their herbicidal method of use 失效
标题翻译：取代苯氧烷基二酮类及其除草方法
公开(公告)号：US4522647A
公开(公告)日：1985-06-11
申请号：US508971
申请日：1983-06-29
申请人： Richard J. Anderson , Shy-Fuh Lee
发明人： Richard J. Anderson , Shy-Fuh Lee
IPC分类号： C07D241/40 , A01N39/00 , A01N39/02 , A01N43/40 , A01N43/42 , A01N43/60 , A01N43/74 , C07C45/30 , C07C45/51 , C07C45/67 , C07C49/255 , C07C59/68 , C07C69/716 , C07C205/38 , C07D213/64 , C07D213/643 , C07D213/69 , C07D213/70 , C07D213/72 , C07D215/22 , C07D215/227 , C07D241/44 , C07D263/58 , C07D277/68 , C07D213/26
CPC分类号： C07D213/643 , A01N39/00 , A01N43/40 , A01N43/42 , A01N43/60 , A01N43/74 , C07C205/38 , C07C251/72 , C07C323/00 , C07C45/30 , C07C45/516 , C07C45/676 , C07C49/255 , C07C59/68 , C07D213/69 , C07D213/70 , C07D215/227 , C07D241/44 , C07D263/58 , C07D277/68
摘要： Substituted phenoxyalkanediones and intermediates therefor, and the use of said compounds for the control of weeds.
摘要翻译：取代的苯氧基烷二酮及其中间体，以及所述化合物用于防治杂草的用途。

30. 发明授权

US4501924A Herbicidally active substituted diphenyl ether acetals or ketals 失效
标题翻译：除草活性取代二苯醚缩醛或缩酮
公开(公告)号：US4501924A
公开(公告)日：1985-02-26
申请号：US490818
申请日：1983-05-02
申请人： Dennis K. Krass
发明人： Dennis K. Krass
IPC分类号： A01N35/04 , A01N37/42 , C07C205/38 , C07C43/30
CPC分类号： A01N37/42 , A01N35/04 , C07C205/38
摘要： This invention relates to certain herbicidally active substituted diphenyl ether acetals or ketals, herbicidal compositions of the same and the use thereof for preemergence postemergence control of noxious plants, i.e., weeds.
摘要翻译：本发明涉及某些除草活性的取代的二苯醚缩醛或缩酮，其除草组合物及其用于对有害植物（即杂草）进行芽前芽防治的用途。

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