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21. 发明申请

US20150258538A1 METHOD FOR PRODUCING CATALYST FOR USE IN PRODUCTION OF METHYLAMINE COMPOUND, AND METHOD FOR PRODUCING METHYLAMINE COMPOUND 有权
标题翻译：用于制备用于生产甲基胺化合物的催化剂的方法和用于生产甲基胺化合物的方法
公开(公告)号：US20150258538A1
公开(公告)日：2015-09-17
申请号：US14433500
申请日：2013-10-11
申请人： MITSUBISHI GAS CHEMICAL COMPANY, INC.
发明人： Toshihiro Nomura , Katsumi Higuchi , Akio Hashimoto , Sachiko Arie
IPC分类号： B01J37/10 , C07C209/64 , C07C209/16 , B01J29/85
CPC分类号： B01J37/10 , B01J29/85 , B01J35/023 , B01J37/0063 , B01J37/08 , B01J2229/186 , B01J2229/36 , B01J2229/40 , C07C209/16 , C07C209/64 , C07C211/04
摘要： According to the present invention, a method for producing a catalyst for use in the production of a methylamine compound can be provided, wherein the catalyst comprises a modified crystalline silicoaluminophosphate salt molecular sieve. The method comprises: a moisture control step of adsorbing moisture onto a crystalline silicoaluminophosphate salt molecular sieve in an amount of 5 to 30 wt % of the crystalline silicoaluminophosphate salt molecular sieve; and a step of heating the crystalline silicoaluminophosphate salt molecular sieve having moisture adsorbed thereon under a pressure of 0.1 MPa or more and at a temperature of 130 to 350° C. for 5 to 40 hours.
摘要翻译：根据本发明，可以提供用于生产甲胺化合物的催化剂的制备方法，其中催化剂包含改性的结晶硅铝磷酸盐分子筛。该方法包括：以结晶硅铝磷酸盐分子筛的5〜30重量％的量将水分吸附在结晶硅铝磷酸盐分子筛上的湿度控制步骤; 以及在0.1MPa以上的压力和130〜350℃的温度下加热吸附有水分的结晶硅铝磷酸盐分子筛5〜40小时的工序。

22. 发明授权

US08969608B2 Organometallic compound preparation 有权
标题翻译：有机金属化合物制剂
公开(公告)号：US08969608B2
公开(公告)日：2015-03-03
申请号：US13586679
申请日：2012-08-15
申请人： Curtis D. Modtland
发明人： Curtis D. Modtland
IPC分类号： C07F7/00 , C07F5/00 , B01J14/00 , C07C209/68
CPC分类号： C07F7/003 , B01J14/00 , C07C209/68 , C07F5/00 , C07F5/003 , C07F7/00 , C07C211/04 , C07C211/08
摘要： A method of continuously manufacturing an organometallic compound is provided where two or more reactants are conveyed to a contacting zone of a reactor in a manner so as to maintain a laminar flow of the reactants; and causing the reactants to form the organometallic compound.
摘要翻译：提供连续制造有机金属化合物的方法，其中两种或多种反应物以保持反应物的层流的方式输送到反应器的接触区; 并使反应物形成有机金属化合物。

23. 发明授权

US08664446B1 Purification of trimethylamine 有权
标题翻译：三甲胺的纯化
公开(公告)号：US08664446B1
公开(公告)日：2014-03-04
申请号：US13731297
申请日：2012-12-31
申请人： American Air Liquide, Inc.
发明人： Brian Besancon , Christian Dussarrat , Nathan Stafford , Paul Jantzen
IPC分类号： C07C209/84 , C07C209/86
CPC分类号： C07C209/84 , C07C211/04
摘要： Methods of purifying NMe3 by removing N2, NH2Me, NH3, and H2O are disclosed.
摘要翻译：公开了通过除去N 2，NH 2 Me，NH 3和H 2 O来净化NMe 3的方法。

24. 发明申请

US20130178541A1 NOVEL LOW MOLECULAR WEIGHT CATIONIC LIPIDS FOR OLIGONUCLEOTIDE DELIVERY 有权
标题翻译：用于寡核苷酸交付的新型低分子量阳离子脂肪
公开(公告)号：US20130178541A1
公开(公告)日：2013-07-11
申请号：US13823830
申请日：2011-09-20
申请人： Matthew G. Stanton , Brian W. Budzik , Gregory L. Beutner , Hongbiao Liao
发明人： Matthew G. Stanton , Brian W. Budzik , Gregory L. Beutner , Hongbiao Liao
IPC分类号： A61K47/18 , C07D207/06 , C07C211/17 , C07C211/21
CPC分类号： A61K47/18 , A61K45/00 , A61K48/00 , C07C211/04 , C07C211/08 , C07C211/17 , C07C211/21 , C07D207/06 , C12N15/88
摘要： The instant invention provides for novel catiomc lipids that can be used in combination with other lipid components such as cholesterol and PEG-lipids to form lipid nanoparticles with oligonucleotides. It is an object of the instant invention to provide a cationic lipid scaffold that demonstrates enhanced efficacy along with lower liver toxicity as a result of lower lipid levels in the liver. The present invention employs low molecular weight cationic lipids with one short lipid chain to enhance the efficiency and tolerability of in vivo delivery of siRNA.
摘要翻译：本发明提供了可以与其它脂质成分如胆固醇和PEG-脂质组合使用以与寡核苷酸形成脂质纳米颗粒的新型细胞脂质。本发明的目的是提供一种阳离子脂质支架，由于肝中脂质水平降低，其表现出增强的功效以及较低的肝毒性。本发明使用具有一个短脂链的低分子量阳离子脂质以增强siRNA的体内递送的效率和耐受性。

25. 发明申请

US20120103413A1 THIN-FILM SOLAR CELL AND METHOD FOR FABRICATING THE SAME 审中-公开
标题翻译：薄膜太阳能电池及其制造方法
公开(公告)号：US20120103413A1
公开(公告)日：2012-05-03
申请号：US13347969
申请日：2012-01-11
申请人： Chin-Yao Tsai , Chih-Wei Chang , Ching-In Wu , Kai-Hsiang Chuang , Chih-Hsiung Chang , Kun-Chih Lin
发明人： Chin-Yao Tsai , Chih-Wei Chang , Ching-In Wu , Kai-Hsiang Chuang , Chih-Hsiung Chang , Kun-Chih Lin
IPC分类号： H01L31/02 , H01L31/18
CPC分类号： H01L31/03767 , C07C211/04 , C07C211/05 , H01L31/048 , H01L31/1864 , Y02E10/50 , Y02P70/521
摘要： A thin-film solar cell includes a body and a polymer layer. The body includes a first electrode layer, a photoelectric conversion layer, and a second electrode layer, and the polymer layer includes a hardening material and an interface material. The photoelectric conversion layer is disposed between the first electrode layer and the second electrode layer, and the polymer layer surrounds the photoelectric conversion layer, in which the interface material is used for bonding to the hardening material and the photoelectric conversion layer respectively. Therefore, the thin-film solar cell may reduce the Staebler-Wronski Effect generated by the photoelectric conversion layer in the photoelectric conversion procedure. Accordingly, the photoelectric conversion efficiency is improved.
摘要翻译：薄膜太阳能电池包括主体和聚合物层。主体包括第一电极层，光电转换层和第二电极层，聚合物层包括硬化材料和界面材料。光电转换层设置在第一电极层和第二电极层之间，聚合物层围绕光电转换层，其中界面材料分别用于与硬化材料和光电转换层接合。因此，薄膜太阳能电池可以减少由光电转换层产生的Staebler-Wronski效应。因此，提高了光电转换效率。

26. 发明授权

US07518020B2 Method for controlling the reactor admission temperature during the production of methylamine 有权
标题翻译：在甲胺生产过程中控制反应器入口温度的方法
公开(公告)号：US07518020B2
公开(公告)日：2009-04-14
申请号：US10573185
申请日：2004-09-24
申请人： Werner Reutemann , Rolf Wambsganβ , Frank Poplow , Theodor Weber , Karl-Heinz Roβ , Manfred Julius
发明人： Werner Reutemann , Rolf Wambsganβ , Frank Poplow , Theodor Weber , Karl-Heinz Roβ , Manfred Julius
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/04
摘要： The invention relates to a process for preparing methylamines by gas-phase reaction of methanol and ammonia as starting materials at a pressure in the range from 15 to 30 bar in the presence of heterogeneous catalyst. The starting materials are vaporized in one or more heat exchangers (1, 2, 3), superheated to produce a feed gas stream and subsequently fed into a reactor (4), with the mixing of the starting materials being able to be carried out in the feed stream to one of the heat exchangers (1, 2, 3) or at any desired position in a heat exchanger (1, 2, 3). A product gas stream comprising monomethylamine, dimethylamine and trimethylamine and also reaction by-products is taken off from the reactor (4). To control the reactor inlet temperature of the starting materials to a temperature in the range from 360° C. to 370° C., all or some of the feed gas stream or the product gas stream is passed through an adjustable valve (5) in order to vary the pressure and thus the condensation temperature.
摘要翻译：本发明涉及通过甲醇和氨作为起始原料在非均相催化剂存在下在15至30巴的压力下气相反应制备甲胺的方法。起始材料在一个或多个热交换器（1,2,3）中蒸发，过热以产生进料气流，并随后进料到反应器（4）中，原料的混合能够进行到一个热交换器（1,2,3）或在热交换器（1,2,3）中的任何期望位置的进料流。从反应器（4）中取出包含一甲胺，二甲胺和三甲胺以及反应副产物的产物气流。为了将原料的反应器入口温度控制在360℃至370℃的温度范围内，所有或一些进料气流或产物气流通过可调节阀（5），其中以改变压力，从而改变冷凝温度。

27. 发明授权

US07435855B2 Process for the continuous synthesis of methylamines 有权
标题翻译：连续合成甲胺的方法
公开(公告)号：US07435855B2
公开(公告)日：2008-10-14
申请号：US11629801
申请日：2005-06-16
申请人： Marco Bosch , Jan Kurt Eberhardt , Roderich Röttger , Thomas Krug , Johann-Peter Melder
发明人： Marco Bosch , Jan Kurt Eberhardt , Roderich Röttger , Thomas Krug , Johann-Peter Melder
IPC分类号： C07C209/14
CPC分类号： C07C209/16 , C07C211/04
摘要： Process for the continuous synthesis of methylamines by reaction of methanol and/or dimethyl ether with ammonia in the presence of a heterogeneous catalyst, wherein the catalyst used is a shaped body which comprises a microporous material and at least one organosilicon compound as binder and can be produced by a process comprising the steps (I) preparation of a mixture comprising the microporous material, the binder, a pasting agent and a solvent, (II) mixing and densification of the mixture, (III) shaping of the densified mixture to give a shaped body, (IV) drying of the shaped body and (V) calcination of the dried shaped body.
摘要翻译：在多相催化剂存在下，通过甲醇和/或二甲醚与氨的反应连续合成甲胺的方法，其中使用的催化剂是成形体，其包含微孔材料和至少一种有机硅化合物作为粘合剂，并且可以是通过包括步骤（I）制备包含微孔材料，粘合剂，粘贴剂和溶剂的混合物的方法制备的方法制备，（II）混合和混合物的致密化，（III）使致密混合物成形，得到（IV）成型体的干燥和（V）干燥成型体的煅烧。

28. 发明申请

US20080033226A1 Protecting catalytic sites of metalloaluminophosphate molecular sieves 有权
标题翻译：保护金属铝磷酸盐分子筛的催化位点
公开(公告)号：US20080033226A1
公开(公告)日：2008-02-07
申请号：US11818496
申请日：2007-06-14
申请人： Marcel Janssen , Luc Martens
发明人： Marcel Janssen , Luc Martens
IPC分类号： C07C2/00
CPC分类号： C10G3/49 , B01J29/84 , B01J29/85 , B01J2229/24 , C07C1/20 , C07C209/16 , C07C2529/85 , C10G3/48 , C10G2300/802 , C10G2300/805 , C10G2400/20 , Y02P20/52 , Y02P30/20 , Y02P30/42 , C07C11/06 , C07C211/04
摘要： Metalloaluminophosphate molecular sieves and metalloaluminophosphate molecular sieve catalyst particles are protecting from degradation by water by maintaining said molecular sieves or catalysts in contact with a liquid mixture of alcohol and water, the mixture of alcohol and water containing from 45 wt % to 99.8 wt % alcohol. The metalloaluminophosphate molecular sieves and metalloaluminophosphate molecular sieve catalyst particles which have been protected in such fashion catalyze the conversion of feedstocks to hydrocarbons.
摘要翻译：金属铝磷酸盐分子筛和金属铝磷酸盐分子筛催化剂颗粒通过保持所述分子筛或催化剂与醇和水的液体混合物（含有45重量％至99.8重量％的醇的水和水的混合物）接触来防止水分降解。以这种方式被保护的金属铝磷酸盐分子筛和金属铝磷酸盐分子筛催化剂颗粒催化原料转化为烃。

29. 发明授权

US07115238B2 Crystalline silicoaluminophosphate salt molecular sieve having octaoxygen-membered ring pore, process for producing the same and process for producing methylamine with the molecular sieve as catalyst 有权
标题翻译：具有八氧环元环的结晶硅铝磷酸盐分子筛，其制备方法和用分子筛作催化剂制备甲胺的方法
公开(公告)号：US07115238B2
公开(公告)日：2006-10-03
申请号：US10515380
申请日：2003-05-23
申请人： Katsumi Higuchi , Akio Hashimoto , Toshihiro Nomura , Sachiko Arie , Takuo Ohshida , Takashi Kojima
发明人： Katsumi Higuchi , Akio Hashimoto , Toshihiro Nomura , Sachiko Arie , Takuo Ohshida , Takashi Kojima
IPC分类号： B01J29/85 , C01B37/08 , C07C209/00
CPC分类号： C01B37/08 , B01J29/85 , B01J2229/12 , B01J2229/36 , B01J2229/62 , C07C209/64 , Y10S423/30 , C07C211/04
摘要： Problems on catalyst production and catalyst performance with respect to conventional 8-oxygen-membered ring micropore-containing crystalline silicoaluminophosphate molecular sieves as non-equilibrium methylamine synthesis catalysts, are resolved. A chabazite type crystalline silicoaluminophosphate molecular sieve having high purity and high crystallinity and having, on a crystal grain surface, an amorphous oxide layer whose Si/Al atomic ratio is greater than that of the whole crystal grain can be stably produced with high yield with the use of a small amount of structure directing agents by the present method characterized in that hydrothermal treatment conducted in the production of 8-oxygen-membered ring micropore-containing crystalline silicoaluminophosphate sieves is controlled under specified treating conditions. The thickness and composition of the amorphous oxide layer, which exert marked influence on the yield of dimethylamine synthesis, can be easily controlled and reproduced under the conditions of catalyst synthesis according to the invention. Thus, the catalyst of high performance can be stably supplied by the present invention at a low cost with reduced output of waste.
摘要翻译：解决了关于作为非平衡甲胺合成催化剂的常规8-氧元素环微孔结晶硅铝磷酸盐分子筛的催化剂生产和催化剂性能的问题。具有高纯度和高结晶度的菱沸石型结晶硅铝磷酸盐分子筛可以在晶粒表面上具有Si / Al原子比大于整个晶粒的非晶氧化物层的稳定的高产率，通过本方法使用少量的结构导向剂，其特征在于在规定的处理条件下控制在8-氧元环微孔结晶硅铝磷酸盐筛的生产中进行的水热处理。可以在根据本发明的催化剂合成条件下容易地控制和再现无定形氧化物层的厚度和组成，其对二甲胺合成的收率具有显着影响。因此，通过本发明可以以低成本稳定地提供高性能的催化剂，同时减少废弃物的产出。

30. 发明申请

US20060079718A1 Continuous methods and reactor used for the production of alkylamines 审中-公开
标题翻译：用于生产烷基胺的连续方法和反应器
公开(公告)号：US20060079718A1
公开(公告)日：2006-04-13
申请号：US10536498
申请日：2003-11-24
申请人： Marco Bosch , Roderich Rottger , Bernd Stein , Thomas Krug , Johann-Peter Melder , Theodor Weber
发明人： Marco Bosch , Roderich Rottger , Bernd Stein , Thomas Krug , Johann-Peter Melder , Theodor Weber
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , B01J8/0221 , B01J8/0285 , B01J2208/00132 , B01J2208/00353 , B01J2208/0053 , C07C211/04
摘要： In the continuous process for preparing alkylamines by reacting C1-4-alkanols with ammonia in the gas phase in the presence of a shape-selective fixed-bed catalyst in a cooled reactor, the shape-selective fixed-bed catalyst is present in a single contiguous fixed bed in the reactor and tubes through which coolants are passed run within the fixed bed to regulate the temperature of the fixed bed.
摘要翻译：在冷却反应器中，在形状选择性固定床催化剂存在下，在气相中使C 1-4烷基链烷醇与氨反应制备烷基胺的连续方法中，形状选择性固定催化剂存在于反应器中的单个连续的固定床中，冷却剂通过该管通过固定床的管道以调节固定床的温度。

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