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1. 发明授权

US08658849B2 Process for the separation of unbranched hydrocarbons from their branched isomers 失效
标题翻译：从支链异构体中分离未分支烃的方法
公开(公告)号：US08658849B2
公开(公告)日：2014-02-25
申请号：US12668436
申请日：2008-06-30
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
IPC分类号： C07C7/13
CPC分类号： C07C7/12 , B01J20/22 , B01J20/226 , B01J2220/56 , C07C7/135 , C10G25/003 , C07C9/00
摘要： The present invention relates to a process for the separation of at least one unbranched C4-C2O hydrocarbon from a fluid mixture containing the unbranched hydrocarbon and at least one branched isomer of the unbranched hydrocarbon, which comprises the step of—contacting the fluid mixture with an adsorbent comprising a porous metal organic framework material, which material comprises at least one at least bidentate organic compound coordinately bound to at least one metal ion, to get the unbranched hydrocarbon adsorbed, wherein the at least one at least bidentate organic compound is a monocyclic, bicyclic or polycyclic ring system which is derived from at least one heterocycle selected from the group consisting of pyrrole, alpha-pyridone and gamma-pyridone and has at least two ring nitrogens and is unsubstituted or bears one or more substituents selected independently from the group consisting of halogen, Ci-6-alkyl, phenyl, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl, where the substituents Ci_6-alkyl and phenyl are unsubstituted or bear one or more substituents selected independently from the group consisting of halogen, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl. The present invention also relates to the use of said porous metal-organic framework material in a process for the separation of unbranched hydrocarbons from their branched isomers.
摘要翻译：本发明涉及从含有非支链烃和非支链烃的至少一种支链异构体的流体混合物中分离至少一种未分支的C 4 -C 20烃的方法，其包括使流体混合物与吸附剂，其包含多孔金属有机骨架材料，该材料包含与至少一种金属离子配位结合的至少一种至少二齿有机化合物，以获得非支化烃被吸附，其中至少一种至少二齿有机化合物是单环，衍生自选自吡咯，α-吡啶酮和γ-吡啶酮的至少一种杂环的双环或多环系统，并且具有至少两个环氮并且是未取代的或带有一个或多个独立地选自以下的取代基：的卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，苯基和OC 1-6 - 烷基，其中取代基C 1-6 - 烷基和苯基是未取代的或具有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，和OC 1-6烷基。本发明还涉及所述多孔金属 - 有机骨架材料在从其支化异构体中分离未分支烃的方法中的用途。

2. 发明申请

US20110160504A1 PROCESS FOR PREPARING A C4-OLEFIN MIXTURE BY SELECTIVE HYDROGENATION AND METATHESIS PROCESS FOR USING THIS STREAM 有权
标题翻译：通过选择性氢化和使用本流程的METATHESIS过程制备C4-烯烃混合物的方法
公开(公告)号：US20110160504A1
公开(公告)日：2011-06-30
申请号：US13042142
申请日：2011-03-07
申请人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
发明人： Jürgen Stephan , Andreas Brodhagen , Markus Schubert , Frank Poplow , Michael Röper , Thomas Hill
IPC分类号： C07C5/05
CPC分类号： C07C11/08 , C07C6/04 , C07C2523/44 , C07C11/107 , C07C11/10
摘要： A C4-olefin mixture having a 1,3-butadiene content of from 100 to 500 ppm and a content of 1,2-dienes of less than 10 ppm is described. The present invention further provides a process for preparing this C4-olefin mixture and provides for its use in a metathesis reaction for preparing 2-pentene and/or 3-hexene.
摘要翻译：描述1,3-丁二烯含量为100-500ppm，1,2-二烯含量小于10ppm的C 4 - 烯烃混合物。本发明还提供了一种制备该C 4烯烃混合物的方法，并提供其在复分解反应中用于制备2-戊烯和/或3-己烯的用途。

3. 发明授权

US07518020B2 Method for controlling the reactor admission temperature during the production of methylamine 有权
标题翻译：在甲胺生产过程中控制反应器入口温度的方法
公开(公告)号：US07518020B2
公开(公告)日：2009-04-14
申请号：US10573185
申请日：2004-09-24
申请人： Werner Reutemann , Rolf Wambsganβ , Frank Poplow , Theodor Weber , Karl-Heinz Roβ , Manfred Julius
发明人： Werner Reutemann , Rolf Wambsganβ , Frank Poplow , Theodor Weber , Karl-Heinz Roβ , Manfred Julius
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/04
摘要： The invention relates to a process for preparing methylamines by gas-phase reaction of methanol and ammonia as starting materials at a pressure in the range from 15 to 30 bar in the presence of heterogeneous catalyst. The starting materials are vaporized in one or more heat exchangers (1, 2, 3), superheated to produce a feed gas stream and subsequently fed into a reactor (4), with the mixing of the starting materials being able to be carried out in the feed stream to one of the heat exchangers (1, 2, 3) or at any desired position in a heat exchanger (1, 2, 3). A product gas stream comprising monomethylamine, dimethylamine and trimethylamine and also reaction by-products is taken off from the reactor (4). To control the reactor inlet temperature of the starting materials to a temperature in the range from 360° C. to 370° C., all or some of the feed gas stream or the product gas stream is passed through an adjustable valve (5) in order to vary the pressure and thus the condensation temperature.
摘要翻译：本发明涉及通过甲醇和氨作为起始原料在非均相催化剂存在下在15至30巴的压力下气相反应制备甲胺的方法。起始材料在一个或多个热交换器（1,2,3）中蒸发，过热以产生进料气流，并随后进料到反应器（4）中，原料的混合能够进行到一个热交换器（1,2,3）或在热交换器（1,2,3）中的任何期望位置的进料流。从反应器（4）中取出包含一甲胺，二甲胺和三甲胺以及反应副产物的产物气流。为了将原料的反应器入口温度控制在360℃至370℃的温度范围内，所有或一些进料气流或产物气流通过可调节阀（5），其中以改变压力，从而改变冷凝温度。

4. 发明申请

US20080254976A1 ACTIVATED METATHESIS CATALYSTS 失效
标题翻译：活化的METATHESIS催化剂
公开(公告)号：US20080254976A1
公开(公告)日：2008-10-16
申请号：US12098165
申请日：2008-04-04
申请人： Markus SCHUBERT , Michael Hesse , Jurgen Stephan , Volker Bohm , Andreas Brodhagen , Frank Poplow , Martina Sinner-Lang , Uwe Diehlmann , Gerhard Cox , Jochen Pfeifer
发明人： Markus SCHUBERT , Michael Hesse , Jurgen Stephan , Volker Bohm , Andreas Brodhagen , Frank Poplow , Martina Sinner-Lang , Uwe Diehlmann , Gerhard Cox , Jochen Pfeifer
IPC分类号： B01J21/08
CPC分类号： C07C6/04 , B01J21/08 , B01J23/28 , B01J23/30 , B01J23/36 , B01J27/22 , B01J37/0203 , B01J37/082 , C07C2523/28 , C07C2523/30 , C07C2523/36 , Y02P20/52 , C07C11/02 , C07C11/107 , C07C11/06
摘要： The present invention provides a process for preparing a supported catalyst (catalyst C) having a support (support S) selected from among oxides, phosphates, silicates, carbides, borides and nitrides of main group elements and elements of transition groups VI and II and mixtures of the abovementioned compounds and an active component (activator A) comprising one or more compounds containing one or more elements of transition groups V, VI and VII customary for the catalysis of metathesis reactions.
摘要翻译：本发明提供一种制备负载型催化剂（催化剂C）的方法，所述负载型催化剂（催化剂C）具有选自主要元素的氧化物，磷酸盐，硅酸盐，碳化物，硼化物和氮化物中的载体（载体S）和转变基团VI和II的元素以及混合物的上述化合物和包含一种或多种含有一种或多种通常用于复分解反应催化的过渡基团V，VI和VII元素的化合物（活化剂A）。

5. 发明申请

US20100197990A1 PROCESS FOR THE SEPARATION OF UNBRANCHED HYDROCARBONS FROM THEIR BRANCHED ISOMERS 失效
标题翻译：从分散式异构体中分离出未结合的烃类的方法
公开(公告)号：US20100197990A1
公开(公告)日：2010-08-05
申请号：US12668436
申请日：2008-06-30
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , B01J20/22 , B01J20/226 , B01J2220/56 , C07C7/135 , C10G25/003 , C07C9/00
摘要： The present invention relates to a process for the separation of at least one unbranched C4-C2O hydrocarbon from a fluid mixture containing the unbranched hydrocarbon and at least one branched isomer of the unbranched hydrocarbon, which comprises the step of—contacting the fluid mixture with an adsorbent comprising a porous metal organic framework material, which material comprises at least one at least bidentate organic compound coordinately bound to at least one metal ion, to get the unbranched hydrocarbon adsorbed, wherein the at least one at least bidentate organic compound is a monocyclic, bicyclic or polycyclic ring system which is derived from at least one heterocycle selected from the group consisting of pyrrole, alpha-pyridone and gamma-pyridone and has at least two ring nitrogens and is unsubstituted or bears one or more substituents selected independently from the group consisting of halogen, Ci-6-alkyl, phenyl, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl, where the substituents Ci_6-alkyl and phenyl are unsubstituted or bear one or more substituents selected independently from the group consisting of halogen, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl. The present invention also relates to the use of said porous metal-organic framework material in a process for the separation of unbranched hydrocarbons from their branched isomers.
摘要翻译：本发明涉及从含有非支链烃和非支链烃的至少一种支链异构体的流体混合物中分离至少一种未分支的C 4 -C 20烃的方法，其包括使流体混合物与吸附剂，其包含多孔金属有机骨架材料，该材料包含与至少一种金属离子配位结合的至少一种至少二齿有机化合物，以获得非支化烃被吸附，其中至少一种至少二齿有机化合物是单环，衍生自选自吡咯，α-吡啶酮和γ-吡啶酮的至少一种杂环的双环或多环系统，并且具有至少两个环氮并且是未取代的或带有一个或多个独立地选自以下的取代基：的卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，Ophenyl和OCi-6-alk 其中取代基C 1-6 - 烷基和苯基是未取代的或具有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，苯基和OC 1-6烷基。本发明还涉及所述多孔金属 - 有机骨架材料在从其支化异构体中分离未分支烃的方法中的用途。

6. 发明申请

US20100048959A1 METHOD FOR THE HYDROFORMYLATION OF OLEFINS 有权
标题翻译：烯烃氢化方法
公开(公告)号：US20100048959A1
公开(公告)日：2010-02-25
申请号：US12516855
申请日：2007-11-29
申请人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
发明人： Marcus Sigl , Frank Poplow , Rainer Papp , Thomas Mackewitz , Dag Wiebelhaus , Rocco Paciello , Thomas Heldemann , Frank Heimann , Stefan Bitterlich , Martin Volland , Sven Crone , Christoph Obler
IPC分类号： C07C45/41 , C07C29/151
CPC分类号： C07C45/50 , C07C5/2506 , C07C29/141 , C07C45/74 , C07C47/02 , C07C11/08 , C07C31/125 , C07C47/21
摘要： The present invention relates to a process for preparing hydroformylation products of olefins having at least four carbon atoms, in which a high proportion of both the linear Ci-olefins having a terminal double bond comprised in the olefin-comprising feed used and of the linear Ci-olefins having an internal double bond is converted into hydroformylation products. Furthermore, the invention relates to a process for preparing 2-propylheptanol which comprises such a hydroformylation process.
摘要翻译：本发明涉及一种制备具有至少四个碳原子的烯烃的加氢甲酰化产物的方法，其中在所用含烯烃的原料中包含的具有末端双键的直链C 1 -C 20烯烃和线性C 1 具有内部双键的烯烃转化为加氢甲酰化产物。此外，本发明涉及一种制备2-丙基庚醇的方法，其包括这种加氢甲酰化方法。

7. 发明申请

US20090032023A1 CLOSED REVERSIBLE BREATHING APPARATUS HAVING A METAL ORGANIC FRAMEWORK 审中-公开
标题翻译：关闭具有金属有机框架的可反向呼吸装置
公开(公告)号：US20090032023A1
公开(公告)日：2009-02-05
申请号：US12282289
申请日：2007-02-26
申请人： Jorg Pastre , Ulrich Muller , Markus Schubert , Christoph Kiener , Friedhelm Teich , Frank Poplow
发明人： Jorg Pastre , Ulrich Muller , Markus Schubert , Christoph Kiener , Friedhelm Teich , Frank Poplow
IPC分类号： A61M16/22 , B01J49/00
CPC分类号： B01D53/02 , A62D9/00 , B01D2253/204 , B01D2257/504 , B01J20/226 , B01J20/3425 , B01J20/3483 , B01J20/3491 , B01J2220/56 , B63C11/24 , C25B3/12 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to methods for removing carbon dioxide and, if appropriate, water from breathing air in closed or partially closed systems using a porous metal-organic framework material, such systems having at least one breathing apparatus and also their use and methods for regenerating the porous metal-organic framework material.
摘要翻译：本发明涉及使用多孔金属 - 有机骨架材料从闭合或部分封闭的系统中的呼吸空气中除去二氧化碳和适当的水的方法，这种系统具有至少一种呼吸器，并且其用途和再生方法多孔金属 - 有机骨架材料。

8. 发明申请

US20080045766A1 Supported Catalyst Comprising Delta- Or Theta-Modified Aluminium Oxide Supports 审中-公开
标题翻译：负载型催化剂包括三角形或者改性氧化铝载体
公开(公告)号：US20080045766A1
公开(公告)日：2008-02-21
申请号：US10590979
申请日：2005-02-24
申请人： Markus Schubert , Jurgen Stephan , Volker Bohn , Andreas Brodhagen , Frank Poplow
发明人： Markus Schubert , Jurgen Stephan , Volker Bohn , Andreas Brodhagen , Frank Poplow
IPC分类号： B01J21/04 , B01J23/36 , B01J32/00 , B01J37/08
CPC分类号： B01J21/04 , B01J23/36 , B01J35/002 , B01J35/1019 , B01J35/1042 , B01J35/1061 , B01J37/08 , C07C5/333 , C10G45/00 , C07C11/08 , C07C11/02
摘要： Process for producing a supported catalyst which comprises at least 75% by weight of Al2O3, whose proportion of Al2O3 in the delta or theta modification is, based on the proportion of Al2O3, at least 1% and which comprises a rhenium compound and, if appropriate, a promoter as active component (A), which comprises a) converting a customary support (S) which comprises at least 75% by weight of Al2O3 and to which a promoter may, if appropriate, have been applied is converted into a modified support (S) whose proportion of Al2O3 in the delta or theta modification is, based on the proportion of Al2O3, at least 1% by calcining the customary support (S) at a temperature of from 750 to 1100°C., b) producing a supported catalyst precursor from the modified support (S) by applying the active component (A) comprising the rhenium compound to the modified support (S) and c) calcining the supported catalyst precursor at a temperature of from 500 to 750° C.
摘要翻译：负载催化剂的制备方法，其包含至少75重量％的Al 2 O 3 O 3，其比例为Al 2 O 3 O 3， δ或θ改性中的3 N是基于Al 2 O 3 3 3％至少1％的比例，并且其包含铼化合物，如果合适的作为活性组分（A）的促进剂，其包括a）转化常规载体（S），其包含至少75重量％的Al 2 O 3 3和如果合适的话，启动子可以被施加到其上，转化成其在δ或θ改性中的Al 2 O 3 O 3比例为的改性载体（S）基于Al 2 O 3 3 3％的比例，通过在750至1100℃的温度下煅烧常规载体（S）至少1％，b）通过将包含铼化合物的活性组分（A）施加到改性载体（S）上，由改性载体（S）制备负载型催化剂前体，和c）在500-750℃的温度下煅烧负载的催化剂前体

9. 发明申请

US20070270614A1 Method for Controlling the Reactor Admission Temperature During the Production of Methylamine 有权
标题翻译：控制甲胺生产过程中反应器进口温度的方法
公开(公告)号：US20070270614A1
公开(公告)日：2007-11-22
申请号：US10573185
申请日：2004-09-24
申请人： Werner Reutemann , Rolf Wambsganss , Frank Poplow , Theodor Weber , Karl-Heinz Ross , Manfred Julius
发明人： Werner Reutemann , Rolf Wambsganss , Frank Poplow , Theodor Weber , Karl-Heinz Ross , Manfred Julius
IPC分类号： C07C209/14
CPC分类号： C07C209/16 , C07C211/04
摘要： The invention relates to a process for preparing methylamines by gas-phase reaction of methanol and ammonia as starting materials at a pressure in the range from 15 to 30 bar in the presence of heterogeneous catalyst. The starting materials are vaporized in one or more heat exchangers (1, 2, 3), superheated to produce a feed gas stream and subsequently fed into a reactor (4), with the mixing of the starting materials being able to be carried out in the feed stream to one of the heat exchangers (1, 2, 3) or at any desired position in a heat exchanger (1, 2, 3). A product gas stream comprising monomethylamine, dimethylamine and trimethylamine and also reaction by-products is taken off from the reactor (4). To control the reactor inlet temperature of the starting materials to a temperature in the range from 360° C. to 370° C., all or some of the feed gas stream or the product gas stream is passed through an adjustable valve (5) in order to vary the pressure and thus the condensation temperature.
摘要翻译：本发明涉及通过甲醇和氨作为起始原料在非均相催化剂存在下在15至30巴的压力下气相反应制备甲胺的方法。起始材料在一个或多个热交换器（1,2,3）中蒸发，过热以产生进料气流，并随后进料到反应器（4）中，原料的混合能够进行到一个热交换器（1,2,3）或在热交换器（1,2,3）中的任何期望位置的进料流。从反应器（4）中取出包含一甲胺，二甲胺和三甲胺以及反应副产物的产物气流。为了将原料的反应器入口温度控制在360℃至370℃的温度范围内，所有或一些进料气流或产物气流通过可调节阀（5），其中以改变压力，从而改变冷凝温度。

10. 发明授权

US08530717B2 Process for the industrial isolation of propene 失效
标题翻译：丙烯工业隔离工艺
公开(公告)号：US08530717B2
公开(公告)日：2013-09-10
申请号：US13003839
申请日：2009-07-17
申请人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
发明人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , C07C11/06
摘要： A process for the industrial isolation of propene from a gas stream comprising at least propene and propane, which involves contacting of the gas stream with an adsorbent having a porous metal organic framework having at least one at least bidentate organic compound coordinated to at least one metal ion, with the adsorbent becoming laden with propane and the gas stream therefore having an increased proportion of propene, wherein the W least bidentate organic compound is an imidazolate which is unsubstituted or has one or more substituents selected independently from of halogen, C1-6-alkyl, phenyl, NH2, NH(C1-6-alkyl), N(C1-6-alkyl)2, OH, O-phenyl and O—C1-6-alkyl.
摘要翻译：一种用于从包含至少丙烯和丙烷的气流中工业分离丙烯的方法，其包括使气流与具有多孔金属有机骨架的吸附剂接触，所述多孔金属有机骨架具有与至少一种金属配位的至少二齿有机化合物离子，吸附剂变得装满丙烷，因此气流具有增加的丙烯比例，其中W最小二齿有机化合物是未被取代的或具有一个或多个独立地选自卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，O-苯基和O-C 1-6 - 烷基。

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