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21. 发明授权

US08574505B2 Reactor and plant for the continuous preparation of high-purity silicon tetrachloride or high-purity germanium tetrachloride 有权
标题翻译：反应器和设备用于连续制备高纯四氯化硅或高纯四氯化锗
公开(公告)号：US08574505B2
公开(公告)日：2013-11-05
申请号：US13447703
申请日：2012-04-16
申请人： Juergen Erwin Lang , Rainer Nicolai , Hartwig Rauleder
发明人： Juergen Erwin Lang , Rainer Nicolai , Hartwig Rauleder
IPC分类号： B01J19/08
CPC分类号： C01B33/10778 , B01J19/0093 , B01J19/088 , B01J2219/0002 , B01J2219/00033 , B01J2219/00788 , B01J2219/00822 , B01J2219/00853 , B01J2219/00867 , B01J2219/00869 , B01J2219/00871 , B01J2219/00873 , B01J2219/0093 , B01J2219/0807 , B01J2219/0828 , B01J2219/083 , B01J2219/0841 , B01J2219/0871 , B01J2219/0875 , B01J2219/0896 , C01G17/04 , C01P2006/80
摘要： A reactor and a plant containing the reactor for conducting a continuous, industrial process for preparing high-purity silicon tetrachloride or high-purity germanium tetrachloride is provided. The plant contains a plasma reactor having a dielectric, a high voltage electrode and an earthed, metallic heat exchanger, in which the longitudinal axes of the dielectric, of the high-voltage electrode and of the earthed, metallic heat exchanger are oriented parallel to one another and at the same time parallel to the force vector of gravity.
摘要翻译：提供了一种反应器和含有反应器的反应器，用于进行用于制备高纯度四氯化硅或高纯度四氯化锗的连续工业方法。该装置包含具有电介质，高压电极和接地金属热交换器的等离子体反应器，其中高压电极和接地金属热交换器的电介质的纵向轴线平行于一个另一个并且同时平行于重力的力矢量。

22. 发明申请

US20090099004A1 CONTINUOUS PRODUCTION OF CARBON NANOMATERIALS USING A HIGH TEMPERATURE INDUCTIVELY COUPLED PLASMA 有权
标题翻译：使用高温电感耦合等离子体连续生产碳纳米管
公开(公告)号：US20090099004A1
公开(公告)日：2009-04-16
申请号：US10865677
申请日：2004-06-10
申请人： Mark Henderson , John Vavruska , Andreas Blutke , Robert Ferguson
发明人： Mark Henderson , John Vavruska , Andreas Blutke , Robert Ferguson
IPC分类号： B01J38/72 , D01F9/12
CPC分类号： B82Y40/00 , B01J19/088 , B01J2219/0807 , B01J2219/0869 , B01J2219/0871 , B01J2219/0886 , B01J2219/0892 , B01J2219/0894 , B82Y30/00 , C01B32/05 , C01B32/162 , C01B2202/02 , C01B2202/06 , D01F9/12 , Y10S977/844
摘要： High-power inductively coupled plasma technology is used for thermal cracking and vaporization of continuously fed carbonaceous materials into elemental carbon, for reaction with separate and continuously fed metal catalysts inside a gas-phase high-temperature reactor system operating at or slightly below atmospheric pressures. In one particularly preferred embodiment, in-flight growth of carbon nanomaterials is initiated, continued, and controlled at high flow rates, enabling continuous collection and product removal via gas/solid filtration and separation methods, and/or liquid spray filtration and solid collection methods suitable for producing industrial-scale production quantities. In another embodiment, the reaction chamber and/or filtration/separation media include non-catalytic or catalytic metals to simultaneously or separately induce on-substrate synthesis and growth of carbon nanomaterials. The on-substrate grown carbon nanomaterials are produced in secondary chambers that are selectively isolated for periodic removal of the product.
摘要翻译：大功率电感耦合等离子体技术用于将连续进料的碳质材料热裂解和蒸发成元素碳，用于与在大气压力或略低于大气压力运行的气相高温反应器系统内的分离和连续供给的金属催化剂反应。在一个特别优选的实施方案中，碳纳米材料的飞行内生长开始，继续并以高流速控制，使得能够通过气/固过滤和分离方法和/或液体喷雾过滤和固体收集方法连续收集和除去产物适合生产工业规模生产。在另一个实施方案中，反应室和/或过滤/分离介质包括非催化或催化金属，以同时或分别诱导碳纳米材料的底物合成和生长。在衬底上生长的碳纳米材料在二次室中产生，其被选择性分离以定期去除产物。

23. 发明授权

US06531704B2 Nanotechnology for engineering the performance of substances 有权
标题翻译：纳米技术用于工程物质的表现
公开(公告)号：US06531704B2
公开(公告)日：2003-03-11
申请号：US09730053
申请日：2000-12-05
申请人： Tapesh Yadav , Bijan K. Miremadi
发明人： Tapesh Yadav , Bijan K. Miremadi
IPC分类号： G21G400
CPC分类号： C07D307/20 , B01D53/32 , B01D53/86 , B01J8/00 , B01J8/02 , B01J19/087 , B01J19/12 , B01J23/002 , B01J23/08 , B01J23/14 , B01J37/18 , B01J2219/0807 , B01J2523/00 , B82Y30/00 , C01B3/0084 , C01B3/0089 , C01B3/16 , C01B3/323 , C01B3/326 , C01B3/40 , C01B3/586 , C01B17/78 , C01B21/265 , C01B2203/0445 , C01B2203/047 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1094 , C01C1/0411 , C01C1/0482 , C07D213/57 , C07D301/00 , Y02E60/324 , Y02P20/52 , Y10S977/775 , Y10S977/834 , Y10S977/882 , B01J2523/33 , B01J2523/43
摘要： Illustrations are provided on applications and usage of electrically activated catalysts. Methods are disclosed for preparing catalysts from nanomaterials. Processes and devices are described that utilize catalysts. The invention can also be applied to improve the performance of existing catalysts, to enhance the performance of substances by inducing or applying charge in nanostructured forms of substances, and to prepare novel devices. Example processes for hydrogen production are discussed. Finally, the invention can be utilized to engineer the thermal, structural, electrical, magnetic, electrochemical, optical, photonic, and other properties of nanoscale substances.
摘要翻译：提供了电活化催化剂的应用和使用的插图。公开了从纳米材料制备催化剂的方法。描述了利用催化剂的方法和装置。本发明还可以用于提高现有催化剂的性能，通过在纳米结构形式的物质中诱导或施加电荷来提高物质的性能，并且制备新颖的装置。讨论了氢气生产的实例过程。最后，本发明可用于设计纳米级物质的热，结构，电，磁，电化学，光学，光子学和其他性质。

24. 发明授权

US06267864B1 Field assisted transformation of chemical and material compositions 有权
标题翻译：化学和材料成分的现场辅助转化
公开(公告)号：US06267864B1
公开(公告)日：2001-07-31
申请号：US09286698
申请日：1999-04-06
申请人： Tapesh K. Yadav , Bijan K. Meramadi
发明人： Tapesh K. Yadav , Bijan K. Meramadi
IPC分类号： C25B100
CPC分类号： B01J8/02 , B01D53/32 , B01D53/86 , B01J19/087 , B01J2219/0807 , C01B3/16 , C01B3/323 , C01B3/326 , C01B17/78 , C01B21/265 , C01B2203/1041 , C01B2203/1047 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1094 , C01C1/0411 , C01C1/0482 , Y02P20/52
摘要： Methods and devices for transforming less desirable chemical species into more desirable or useful chemical forms are disclosed. The specifications can be used to treat pollutants into more benign compositions and to produce useful chemicals from raw materials and wastes. The methods and devices disclosed utilize continuous or temporary pulse of electrical current induced by electromagnetic field and high surface area formulations. The invention can also be applied to improve the performance of existing catalysts and to prepare novel devices.
摘要翻译：公开了将不期望的化学物质转化成更理想或有用的化学形式的方法和装置。规格可用于将污染物处理成更良性的组合物，并从原料和废物中生产有用的化学物质。所公开的方法和装置利用由电磁场和高表面积配方引起的电流的连续或临时脉冲。本发明也可以用于改进现有催化剂的性能并制备新的装置。

25. 发明公开

US20230264167A1 Plasmalysis Apparatus For The Corona Discharge-Induced Cracking Of Hydrogen-Containing Gas 审中-公开
公开(公告)号：US20230264167A1
公开(公告)日：2023-08-24
申请号：US18011374
申请日：2021-06-23
申请人： GRAFORCE GMBH
发明人： Jens Hanke , Sascha Knist
IPC分类号： B01J19/08
CPC分类号： B01J19/088 , B01J2219/0807 , B01J2219/0849 , B01J2219/0869 , B01J2219/0875
摘要： The present invention relates to the corona discharge-induced cracking of hydrogen-containing gas into molecular hydrogen and at least one by-product, or the production of molecular hydrogen and at least one by-product, or the production of downstream products from the molecular hydrogen and/or the at least one by-product. To this end, hydrogen-containing gas is fed via a gas supply line into a gas-tight reaction chamber with exactly one plasma electrode. The gas-tight reaction chamber is enclosed by a wall that is designed to electrically insulate the plasma electrode from an outside of the wall. The plasma electrode is connected to a high-frequency generator that provides high-frequency alternating voltage and generates corona discharges in the reaction chamber by means of the high-frequency alternating voltage. This results in the cracking of hydrogen-containing gas into molecular hydrogen and at least one by-product. The molecular hydrogen is discharged from the reaction chamber via a gas discharge line. The hydrogen-containing gas can contain, for example, methane, biogas, natural gas, hydrogen sulfide, or cyclohexane, heptane, toluene, gasoline, JP-8, or diesel that have been converted into the gaseous aggregate state.

26. 发明申请

US20180236426A1 Energy Conversion and Reaction System and Method 审中-公开
公开(公告)号：US20180236426A1
公开(公告)日：2018-08-23
申请号：US15753712
申请日：2016-08-22
申请人： Alan Finlay
发明人： Alan Finlay
IPC分类号： B01J19/00 , H01M14/00 , H01M8/06
CPC分类号： B01J19/0093 , B01J19/085 , B01J19/088 , B01J2219/00788 , B01J2219/00853 , B01J2219/00927 , B01J2219/0093 , B01J2219/00948 , B01J2219/0807 , B01J2219/0849 , B01J2219/0875 , B01J2219/0883 , C01B2203/04 , C01B2203/066 , H01M8/06 , H01M14/00
摘要： A system is described that is capable of operating as an energy conversion system that functions as a fuel cell and generates electrical current from a fuel or fuels, or as a reactor for conversion of starter materials into more complex molecules through ion-ion and ion-molecules and which may preferably be adapted to operate as a gas to liquid (GTL) process. The system ionises at least one fuel or starter material and manipulates, selects and transports ions for reaction by means of suitable electrostatic or electrodynamic ion guides, filters or drift tubes. The system of the present application replaces the electrolyte, catalyst and/or membrane found in classic fuel cells or GTL processes with an electrostatic or electrodynamic ion manipulation region such as an ion guide, analyser, drift tube or filter.

27. 发明申请

US20150174550A1 ELECTROMAGNETIC ENERGY-INITIATED PLASMA REACTOR SYSTEMS AND METHODS 有权
标题翻译：电磁能量启发式等离子体反应器系统及方法
公开(公告)号：US20150174550A1
公开(公告)日：2015-06-25
申请号：US14415294
申请日：2013-07-18
申请人： Atlantic Hydrogen Inc.
发明人： James Tranquilla
IPC分类号： B01J19/12 , B01J19/10
CPC分类号： B01J19/088 , B01J19/006 , B01J19/26 , B01J2219/00774 , B01J2219/0807 , B01J2219/083 , B01J2219/0869 , B01J2219/0871 , B01J2219/0883 , H05H1/30
摘要： There is provided a method of processing a reaction product generated from a plasma-based reactive process within a material processing zone of a reactor. The method includes supplying a first electromagnetic energy, from a first energy source, to a flowing primary gaseous feed material, such that at least a fraction of the flowing primary gaseous feed material is excited by the supplied first electromagnetic energy into a first plasma within a first plasma zone, and such that at least a fraction of the flowing primary gaseous feed material is converted to a first plasma zone-conditioned product while flowing through the first plasma and the first plasma zone-conditioned product is flowed to a downstream reaction zone, wherein the flowing of the first plasma zone-conditioned product is effected through a fluid passage that effects fluid communication between the first plasma zone and the downstream reaction zone. A second gaseous material is then introduced to the downstream reaction zone. The first plasma zone-conditioned product is contacted with the second gaseous material within the downstream reaction zone. The geometry of the fluid pas sage at least upstream of the downstream reaction zone inhibits, or substantially inhibits, the supplied first electromagnetic energy from propagating from the first plasma zone to the downstream reaction zone.
摘要翻译：提供了一种处理由反应器的材料处理区内的等离子体反应过程产生的反应产物的方法。该方法包括从第一能量源提供第一电磁能量到流动的初级气体进料，使得至少一部分流动的初级气体进料物质被所提供的第一电磁能量激发到第一等离子体内并且使得至少一部分流动的初级气体进料在流过第一等离子体时转化为第一等离子体区调节产物，并且第一等离子体区调节产物流入下游反应区，其中所述第一等离子体区域调节产物的流动通过影响所述第一等离子体区域和所述下游反应区域之间的流体连通的流体通道来实现。然后将第二气态物质引入下游反应区。第一等离子体区调节产物与下游反应区内的第二气态物质接触。至少在下游反应区的上游的流体的几何形状抑制或基本上抑制所提供的第一电磁能从第一等离子体区传播到下游反应区。

28. 发明授权

US08221593B2 Reactor, plant and industrial process for the continuous preparation of high-purity silicon tetrachloride or high-purity germanium tetrachloride 有权
标题翻译：反应器，工厂和工业过程中连续制备高纯四氯化硅或高纯度四氯化锗
公开(公告)号：US08221593B2
公开(公告)日：2012-07-17
申请号：US12065126
申请日：2006-06-06
申请人： Juergen Erwin Lang , Rainer Nicolai , Hartwig Rauleder
发明人： Juergen Erwin Lang , Rainer Nicolai , Hartwig Rauleder
IPC分类号： H05F3/04
CPC分类号： C01B33/10778 , B01J19/0093 , B01J19/088 , B01J2219/0002 , B01J2219/00033 , B01J2219/00788 , B01J2219/00822 , B01J2219/00853 , B01J2219/00867 , B01J2219/00869 , B01J2219/00871 , B01J2219/00873 , B01J2219/0093 , B01J2219/0807 , B01J2219/0828 , B01J2219/083 , B01J2219/0841 , B01J2219/0871 , B01J2219/0875 , B01J2219/0896 , C01G17/04 , C01P2006/80
摘要： A reactor, a plant, and a continuous, industrial process carried out therein for preparing high-purity silicon tetrachloride or high-purity germanium tetrachloride by treating the silicon tetrachloride or germanium tetrachloride to be purified, which is contaminated by at least one hydrogen-containing compound, by a cold plasma and isolating purified high-purity silicon tetrachloride or germanium tetrachloride from the resulting treated phase by fractional distillation. The treatment is carried out in a plasma reactor in which longitudinal axes of a dielectric, of a high-voltage electrode, and of a grounded, metallic heat exchanger are oriented parallel to one another and at the same time parallel to the force vector of gravity.
摘要翻译：在其中进行的反应器，工厂和连续的工业方法，用于通过处理待纯化的四氯化硅或四氯化锗来制备高纯度四氯化硅或高纯度四氯化锗，其被至少一种含氢的化合物，通过冷等离子体，并通过分馏从所得处理相中分离纯化的高纯度四氯化硅或四氯化锗。处理在等离子体反应器中进行，其中电介质的高压电极和接地的金属热交换器的纵向轴线彼此平行取向并且同时平行于重力的力矢量。

29. 发明申请

US20100155219A1 PLASMA-ENHANCED SYNTHESIS 审中-公开
标题翻译：等离子体增强合成
公开(公告)号：US20100155219A1
公开(公告)日：2010-06-24
申请号：US12530662
申请日：2008-03-17
申请人： Norbert Auner , Sven Holl , Christian Bauch , Gerd Lippold , Rumen Deltschew
发明人： Norbert Auner , Sven Holl , Christian Bauch , Gerd Lippold , Rumen Deltschew
IPC分类号： C08G77/12 , B01J19/08 , C08G79/00
CPC分类号： B01J19/087 , B01J19/088 , B01J2219/0807 , B01J2219/0847 , B01J2219/0849 , B01J2219/0852 , B01J2219/0854 , B01J2219/0869 , B01J2219/0894 , C08G77/60
摘要： The invention is based on the aim of developing a device and a method for the plasma-enhanced synthesis of halogenated polysilanes and polygermanes, wherein at least one reaction partner is present in a gaseous form and is excited by reactive particles from a plasma zone, and is subsequently reacted by means of at least one further reaction partner which is present in the reaction chamber in vaporous or gaseous form. Reactions of halogen silanes or germanes of the group SiCl4, SiF4, GeCl4, GeF4 with H2 are possible.
摘要翻译：本发明是基于开发用于等离子体增强合成卤代聚硅烷和多晶硅的装置和方法的目的，其中至少一个反应对象以气态存在并被来自等离子体区的反应性颗粒激发，以及随后通过至少一种另外的反应配对物反应，该反应伴侣以蒸气或气态的形式存在于反应室中。 SiCl4，SiF4，GeCl4，GeF4与H2的卤素硅烷或锗烷的反应是可能的。

30. 发明申请

US20070056841A1 System and method for the manufacture of hydrogen cyanide and acrylonitrile with simultaneous recovery of hydrogen 审中-公开
标题翻译：同时回收氢气的氰化氢和丙烯腈的制造方法
公开(公告)号：US20070056841A1
公开(公告)日：2007-03-15
申请号：US10528370
申请日：2003-09-17
申请人： Pradeep Agarwal , John Ackerman , Ron Borgialli , Jerry Hamman , Suresh Muknahallipatna , Ji-Jun Zhang
发明人： Pradeep Agarwal , John Ackerman , Ron Borgialli , Jerry Hamman , Suresh Muknahallipatna , Ji-Jun Zhang
IPC分类号： H05F3/00 , B01J19/08
CPC分类号： B01J19/088 , B01J8/009 , B01J8/0221 , B01J19/2475 , B01J2219/0004 , B01J2219/0807 , B01J2219/083 , B01J2219/0849 , B01J2219/0869 , B01J2219/0883 , B01J2219/0892 , B01J2219/0896 , B01J2219/182 , C01B3/342 , C01B2203/0861 , C01C3/0212 , C01C3/0225 , C07C253/24 , C07C255/08 , C07C255/03
摘要： A system and method for the manufacture of hydrogen cyanide, acrylonitrile, and acetonitrile are provided. The system comprises at least one pulsed corona discharge reactor with each pulsed corona discharge reactor having a reaction zone. At least one reactant feed stream containing hydrogen is introduced into the pulsed corona discharge reactor and contacting the catalyst wherein hydrogen is removed from the reactant to form hydrogen cyanide, acrylonitrile, and acetonitrile.
摘要翻译：提供了制造氰化氢，丙烯腈和乙腈的系统和方法。该系统包括至少一个脉冲电晕放电反应器，每个脉冲电晕放电反应器具有反应区。将含有氢的至少一种反应物进料流引入到脉冲电晕放电反应器中并与催化剂接触，其中从反应物中除去氢以形成氰化氢，丙烯腈和乙腈。

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