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21. 发明授权

US07264888B2 Coating systems containing gamma-prime nickel aluminide coating 有权
标题翻译：涂覆体系含有γ-钇铝镍镀层
公开(公告)号：US07264888B2
公开(公告)日：2007-09-04
申请号：US10904220
申请日：2004-10-29
申请人： Ramgopal Darolia , Joseph David Rigney , William Scott Walston
发明人： Ramgopal Darolia , Joseph David Rigney , William Scott Walston
IPC分类号： B32B15/00 , B63H1/26
CPC分类号： F01D5/288 , F05C2201/0466 , F05D2230/90 , F05D2300/611 , Y10T428/12611 , Y10T428/12618 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944
摘要： An overlay coating for articles used in hostile thermal environments. The coating has a predominantly gamma prime-phase nickel aluminide (Ni3Al) composition suitable for use as an environmental coating and as a bond coat for a thermal barrier coating. The coating has a composition of, by weight, at least 6% to about 15% aluminum, about 2% to about 5% chromium, optionally one or more reactive elements in individual or combined amounts of up to 4%, optionally up to 2% silicon, optionally up to 60% of at least one platinum group metal, and the balance essentially nickel. A thermal-insulating ceramic layer may be deposited on the coating.
摘要翻译：用于敌对热环境中的物品的覆盖涂层。该涂层主要具有适合用作环境涂层和用作热障涂层的粘合涂层的γ初始相铝酸镍（Ni 3 Al 3 Al）组合物。该涂层具有按重量计至少6％至约15％的铝，约2％至约5％的铬，任选的一种或多种反应性元素的组合物，其个体或组合量可达4％，任选至多2 ％硅，任选至多60％的至少一种铂族金属，余量基本上为镍。绝热陶瓷层可以沉积在涂层上。

22. 发明授权

US07172820B2 Strengthened bond coats for thermal barrier coatings 失效
标题翻译：加强热障涂层的粘合层
公开(公告)号：US07172820B2
公开(公告)日：2007-02-06
申请号：US11248249
申请日：2005-10-13
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： B32B15/04 , F03B3/12
CPC分类号： C23C28/3215 , C23C28/34 , C23C28/341 , C23C28/345 , C23C28/3455 , C23C28/36 , Y10T428/12493 , Y10T428/12535 , Y10T428/12576 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12806 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944 , Y10T428/25 , Y10T428/252 , Y10T428/256 , Y10T428/265
摘要： A strengthened bond coat for improving the adherence of a thermal barrier coating to an underlying metal substrate to resist spallation without degrading oxidation resistance of the bond coat. The bond coat comprises a bond coating material selected from the group consisting of overlay alloy coating materials, aluminide diffusion coating materials and combinations thereof. Particles comprising a substantially insoluble bond coat strengthening compound and having a relatively fine particle size of about 2 microns or less are dispersed within at least the upper portion of the bond coat in an amount sufficient to impart strengthening to the bond coat, and thus limit ratcheting or rumpling thereof.
摘要翻译：一种增强的粘合涂层，用于改善热障涂层对底层金属基材的粘附性，以抵抗剥离而不降低粘结涂层的抗氧化性。粘合涂层包括选自覆盖合金涂层材料，铝化物扩散涂层材料及其组合的粘合涂层材料。包含基本上不溶性的粘合涂层强化化合物并且具有约2微米或更小的相对较细的粒度的颗粒以足以赋予粘结涂层强化的量分散在粘合涂层的至少上部内部，从而限制棘轮或其皱纹。

23. 发明授权

US06979498B2 Strengthened bond coats for thermal barrier coatings 失效
公开(公告)号：US06979498B2
公开(公告)日：2005-12-27
申请号：US10721853
申请日：2003-11-25
申请人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
发明人： Ramgopal Darolia , Joseph David Rigney , Gillion Herman Marijnissen , Eric Richard Irma Carolus Vergeldt , Annejan Bernard Kloosterman
IPC分类号： C23C28/00 , F01D5/28 , B32B15/04 , F03B3/12
CPC分类号： C23C28/3215 , C23C28/34 , C23C28/341 , C23C28/345 , C23C28/3455 , C23C28/36 , Y10T428/12493 , Y10T428/12535 , Y10T428/12576 , Y10T428/12611 , Y10T428/12618 , Y10T428/12736 , Y10T428/12806 , Y10T428/12875 , Y10T428/12931 , Y10T428/12937 , Y10T428/12944 , Y10T428/25 , Y10T428/252 , Y10T428/256 , Y10T428/265
摘要： A strengthened bond coat for improving the adherence of a thermal barrier coating to an underlying metal substrate to resist spallation without degrading oxidation resistance of the bond coat. The bond coat comprises a bond coating material selected from the group consisting of overlay alloy coating materials, aluminide diffusion coating materials and combinations thereof. Particles comprising a substantially insoluble bond coat strengthening compound and having a relatively fine particle size of about 2 microns or less are dispersed within at least the upper portion of the bond coat in an amount sufficient to impart strengthening to the bond coat, and thus limit ratcheting or rumpling thereof.

24. 发明授权

US06924002B2 Coating and coating process incorporating raised surface features for an air-cooled surface 失效
标题翻译：涂覆和涂覆工艺，包括风冷表面的凸起表面特征
公开(公告)号：US06924002B2
公开(公告)日：2005-08-02
申请号：US10248846
申请日：2003-02-24
申请人： Ching-Pang Lee , Robert Edward Schafrik , Ramgopal Darolia , Joseph David Rigney
发明人： Ching-Pang Lee , Robert Edward Schafrik , Ramgopal Darolia , Joseph David Rigney
IPC分类号： B32B15/16 , C08F2/48 , C23C4/02 , C23C4/08 , C23C14/02 , C23C14/04 , C23C14/16 , C23C16/06 , C23C28/00 , F23M5/00 , F23R3/00 , F28F13/18
CPC分类号： C23C4/02 , C23C4/073 , C23C4/08 , C23C14/025 , C23C14/044 , C23C14/16 , C23C28/021 , C23C28/022 , F05B2240/11 , F05B2250/60 , F05B2260/224 , F05C2253/12 , F23M5/00 , F23M2900/05004 , F23R3/002 , F28F13/18 , F28F13/185 , Y10T428/12063 , Y10T428/12493 , Y10T428/12639 , Y10T428/12646 , Y10T428/12931 , Y10T428/12944 , Y10T428/12993
摘要： A coating and coating process for incorporating surface features on an air-cooled substrate surface of a component for the purpose of promoting heat transfer from the component. The coating process generally comprises depositing a first metallic coating material on the surface of the component using a first set of coating conditions to form a first environmental coating layer, and then depositing a second metallic coating material using a second set of coating conditions that differ from the first set, such that an outer environmental coating layer is formed having raised surface features that cause the surface of the outer environmental coating layer to be rougher than the surface of the first environmental coating layer.
摘要翻译：用于将部件的空气冷却基板表面上的表面特征引入到涂层和涂覆方法中，以促进从部件的热传递。涂覆方法通常包括使用第一组涂覆条件在组件的表面上沉积第一金属涂层材料以形成第一环境涂层，然后使用第二组涂覆条件沉积第二金属涂层材料第一组，使得外部环境涂层形成具有使外部环境涂层的表面比第一环境涂层的表面更粗糙的凸起表面特征。

25. 发明授权

US06617049B2 Thermal barrier coating with improved erosion and impact resistance 有权
标题翻译：具有改善侵蚀和耐冲击性的热障涂层
公开(公告)号：US06617049B2
公开(公告)日：2003-09-09
申请号：US09765227
申请日：2001-01-18
申请人： Ramgopal Darolia , Joseph David Rigney
发明人： Ramgopal Darolia , Joseph David Rigney
IPC分类号： B32B1504
CPC分类号： C23C28/3215 , C23C28/345 , C23C28/3455 , Y10T428/12611 , Y10T428/12618 , Y10T428/12944 , Y10T428/26
摘要： A thermal barrier coating (TBC) for a component intended for use in a hostile environment, such as the superalloy turbine, combustor and augmentor components of a gas turbine engine. The TBC is formed of at least partially stabilized zirconia, preferably yttria-stabilized zirconia (YSZ), and exhibits improved erosion and impact resistance as a result of containing a dispersion of alumina precipitates or particles. The TBC preferably consists essentially of YSZ and the alumina particles, which are preferably dispersed throughout the microstructure of the TBC, including the YSZ grains and grain boundaries. The alumina particles are present in an amount sufficient to increase the impact and erosion resistance of the TBC, preferably at least 5 volume percent of the TBC.
摘要翻译：用于在敌对环境中使用的组件的热障涂层（TBC），例如燃气轮机的超级合金涡轮机，燃烧器和增压器部件。 TBC由至少部分稳定的氧化锆，优选氧化钇稳定的氧化锆（YSZ）形成，并且由于含有氧化铝沉淀物或颗粒的分散体而表现出改善的耐冲击和抗冲击性。 TBC优选基本上由YSZ和氧化铝颗粒组成，其优选分散在整个TBC的微结构中，包括YSZ晶粒和晶界。氧化铝颗粒以足以增加TBC的冲击和耐冲蚀性，优选至少5体积％的TBC的量存在。

26. 发明授权

US06571857B2 Processing of nickel aluminide material 失效
标题翻译：镍铝材料的加工
公开(公告)号：US06571857B2
公开(公告)日：2003-06-03
申请号：US10037127
申请日：2001-11-07
申请人： Ramgopal Darolia , Joseph David Rigney
发明人： Ramgopal Darolia , Joseph David Rigney
IPC分类号： B22D2700
CPC分类号： C22C1/023
摘要： A process for casting and preparing an ingot of a beta-phase NiAl-based material, particularly for use in PVD coating processes. The method entails melting a nickel-aluminum composition having an aluminum content below that required for stoichiometric beta-phase NiAl intermetallic so as to form a melt that includes nickel and Ni3Al. Aluminum is then added to the melt, causing an exothermic reaction between nickel and aluminum as the melt equilibrium shifts from Ni3Al to NiAl. However, the aluminum is added at a rate sufficiently low to avoid a violent exothermic reaction. The addition of aluminum continues until sufficient aluminum has been added to the melt to yield a beta-phase NiAl-based material. The beta-phase NiAl-based material is then solidified to form an ingot, which is then heated and pressed to close porosity and homogenize the microstructure of the ingot.
摘要翻译：一种用于铸造和制备β相NiAl基材料的锭的方法，特别是用于PVD涂覆工艺。该方法需要熔化铝含量低于化学计量的β相NiAl金属间化合物所需的铝 - 铝组合物，以形成包括镍和Ni3Al的熔体。然后将铝加入到熔体中，当熔体平衡从Ni3Al转变为NiAl时，引起镍和铝之间的放热反应。然而，以足够低的速率加入铝以避免剧烈的放热反应。继续加入铝，直到足够的铝加入到熔体中以产生β相NiAl基材料。然后将β相NiAl基材料固化以形成锭，然后将其加热和压制以闭合孔隙并均匀化锭的微观结构。

27. 发明授权

US06291084B1 Nickel aluminide coating and coating systems formed therewith 失效
标题翻译：由此形成的铝化镍涂层和涂层系统
公开(公告)号：US06291084B1
公开(公告)日：2001-09-18
申请号：US09608114
申请日：2000-06-30
申请人： Ramgopal Darolia , Joseph David Rigney , Richard John Grylls
发明人： Ramgopal Darolia , Joseph David Rigney , Richard John Grylls
IPC分类号： B32B1500
CPC分类号： C23C14/16 , C23C28/021 , C23C28/321 , C23C28/345 , C23C28/3455 , C23C30/00 , Y10T428/12535 , Y10T428/12618 , Y10T428/1275 , Y10T428/12944
摘要： An environmental overlay coating for articles used in hostile thermal environments, such as turbine, combustor and augmentor components of a gas turbine engine. The overlay coating is predominantly beta-phase NiAl with limited alloying additions of zirconium and chromium. The overlay coating is useful as an environmental coating and as a bond coat that improves the spallation resistance of a thermal barrier coating (TBC) system.
摘要翻译：用于恶劣热环境中的制品的环境覆盖涂层，例如燃气轮机的涡轮机，燃烧器和增压器部件。覆盖层主要是β相NiAl，并且锆和铬的合金添加有限。覆盖涂层可用作环境涂层和作为粘合涂层，其改善了热障涂层（TBC）系统的耐剥离性。

28. 发明授权

US06533875B1 Protecting a surface of a nickel-based article with a corrosion-resistant aluminum-alloy layer 失效
标题翻译：用耐腐蚀的铝合金层保护镍基制品的表面
公开(公告)号：US06533875B1
公开(公告)日：2003-03-18
申请号：US09693077
申请日：2000-10-20
申请人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Michael James Weimer
发明人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Michael James Weimer
IPC分类号： B05D722
CPC分类号： C23C28/321 , C23C10/18 , C23C10/26 , C23C10/30 , C23C10/48 , C23C10/52 , C23C10/56 , C23C28/3215 , C23C28/325 , C23C28/345 , C23C28/3455 , Y02T50/67
摘要： A surface of a nickel-base article such as an internal surface of a gas turbine airfoil is protected with a donor layer of aluminum and at least one other element. To form the protective layer, a donor alloy is contacted to the protected surface of the article, and simultaneously the article and the donor alloy are heated to a coating temperature that is greater than about 0.7 of the absolute solidus temperature of the donor alloy but is such that the donor alloy remains in the form of a condensed phase contacting the protected surface of the article. The donor alloy is thereafter interdiffused into the protected surface of the article.
摘要翻译：诸如燃气轮机翼型件的内表面的镍基制品的表面由铝的供体层和至少一个其它元件保护。为了形成保护层，供体合金与制品的被保护表面接触，并且同时将制品和供体合金加热至比供体合金的绝对固相线温度大约0.7的涂层温度，但是使得供体合金保持为与受保护的表面接触的凝聚相的形式。然后，供体合金相互扩散到制品的受保护表面。

29. 发明授权

US06676992B2 Article protected by a diffusion aluminide coating applied by painting techniques 失效
标题翻译：用喷涂技术涂覆的扩散铝化物涂层进行保护
公开(公告)号：US06676992B2
公开(公告)日：2004-01-13
申请号：US09934752
申请日：2001-08-22
申请人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
发明人： Jeffrey Allan Pfaendtner , Michael James Weimer , William Evan McCormack , Joseph David Rigney , Mark Lloyd Miller , John Lewis Lackman
IPC分类号： B05D302
CPC分类号： C23C26/00 , C23C24/08 , C25D3/50 , F01D5/288 , Y02T50/67
摘要： A method for coating an article includes preparing a coating precursor paint including aluminum-containing pigment particles, a temporary organic binder comprising an acrylic, and a solvent for the temporary organic binder. The coating precursor paint is applied to a surface of the article and thereafter heated to a temperature of from about 1200° F. to about 2100° F. in a non-oxidizing environment.
摘要翻译：一种涂布物品的方法包括制备包括含铝颜料颗粒的涂料前体涂料，包含丙烯酸的临时有机粘合剂和用于临时有机粘合剂的溶剂。将涂层前体涂料施加到制品的表面，然后在非氧化环境中加热至约1200°F至约2100°F的温度。

30. 发明授权

US06497920B1 Process for applying an aluminum-containing coating using an inorganic slurry mix 有权
标题翻译：使用无机浆料混合物涂覆含铝涂层的方法
公开(公告)号：US06497920B1
公开(公告)日：2002-12-24
申请号：US09656287
申请日：2000-09-06
申请人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Nripendra Nath Das , Michael James Weimer , John Lewis Lackman
发明人： Jeffrey Allan Pfaendtner , Joseph David Rigney , Nripendra Nath Das , Michael James Weimer , John Lewis Lackman
IPC分类号： B05D302
CPC分类号： C23C10/30 , C23C10/20 , Y02T50/67
摘要： An internal passage of an article such as a gas turbine airfoil is coated with an aluminum-containing coating. To accomplish this coating process, a coating slurry of a mixture of a carrier component of water and a hectorite clay or a bentonite clay, together with a solids component of a source of aluminum, a halide activator, and an oxide dispersant, is prepared. The coating slurry is applied to the internal passage of the gas turbine airfoil and dried. The gas turbine airfoil and the applied coating slurry are heated to form an aluminum-containing coating bonded to the internal passage of the gas turbine airfoil. Excess coating material is removed from the article internal passage.
摘要翻译：诸如燃气轮机翼片的制品的内部通道涂覆有含铝涂层。为了完成这种涂覆工艺，制备了水的载体组分和锂蒙脱石粘土或膨润土之间的混合物与铝源的固体组分，卤化物活化剂和氧化物分散剂的混合物的涂料浆料。将涂布浆料施加到燃气轮机翼型件的内部通道并干燥。燃气轮机翼型件和涂覆的涂料浆料被加热以形成结合到燃气轮机翼型件的内部通道的含铝涂层。从制品内部通道中除去过量的涂层材料。

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