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21. 发明授权

US06552118B2 Curable adhesive composition 有权
标题翻译：可固化粘合剂组成
公开(公告)号：US06552118B2
公开(公告)日：2003-04-22
申请号：US09463652
申请日：2000-04-14
申请人： Masayuki Fujita , Masato Kusakabe , Kenichi Kitano
发明人： Masayuki Fujita , Masato Kusakabe , Kenichi Kitano
IPC分类号： C08L8310
CPC分类号： C08F8/42 , C09D183/04 , C09J143/04 , C09K3/1018 , Y10S524/904
摘要： An adhesive curable composition which comprises, as the main component, a vinyl polymer having at least one crosslinkable silyl group represented by the general formula (1). Said composition can be used as a sealing composition, a pressure sensitive adhesive composition and a coating composition. —[Si(R1)2-b(Y)bO]m—Si(R2)3-a(Y)a (1) wherein R1 and R2 are the same or different and each represents an alkyl group containing 1 to 20 carbon atoms, an aryl group containing 6 to 20 carbon atoms, an aralkyl group containing 7 to 20 carbon atoms or a triorganosiloxy group represented by the formula (R′)3SiO— (in which R′ represents a monovalent hydrocarbon group containing 1 to 20 carbon atoms and the plural R′ groups may be the same or different) and, when there are two or more R1 or R2 groups, they may be the same or different; Y represents a hydroxyl group or a hydrolyzable group and, when there are two or more Y groups, they may be the same or different; a represents 0, 1, 2 or 3; b represents 0, 1 or 2; and m represents an integer of 0 to 19; with the condition that a, b and m satisfy the relation a+mb≧1.
摘要翻译：一种粘合剂可固化组合物，其包含作为主要组分的具有至少一个由通式（1）表示的可交联甲硅烷基的乙烯基聚合物。所述组合物可用作密封组合物，压敏粘合剂组合物和涂料组合物。其中R 1和R 2相同或不同，各自表示含有1至20个碳原子的烷基，含有6至20个碳原子的芳基原子，含有7〜20个碳原子的芳烷基或由式（R'）3 SiO 2表示的三有机甲硅烷氧基（其中R'表示含有1〜20个碳原子的一价烃基，多个R'可以是相同或不同），并且当存在两个或更多个R 1或R 2基团时，它们可以相同或不同; Y表示羟基或可水解基团，当存在两个以上Y基时，它们可以相同或不同; a表示0,1,2或3; b表示0,1或2; m表示0〜19的整数。条件是a，b和m满足关系a + mb> = 1。

22. 发明授权

US06420492B1 Processes for preparing (meth) acrylic polymers having functional groups at the chain ends 失效
标题翻译：制备在链末端具有官能团的（甲基）丙烯酸聚合物的方法
公开(公告)号：US06420492B1
公开(公告)日：2002-07-16
申请号：US09356515
申请日：1999-07-19
申请人： Masato Kusakabe , Kenichi Kitano
发明人： Masato Kusakabe , Kenichi Kitano
IPC分类号： C08F800
CPC分类号： C08F8/26 , C08F8/42 , C08F20/00
摘要： (Meth)acrylic polymers having alkenyl or curable silyl groups at the chain ends in high functionality ratios are prepared by a process which comprises (i) preparing a (meth)acrylic polymer having halogen atoms at the chain ends, using an organohalogenated compound or a halosulfonyl compound as an initiator and a metal complex catalyst wherein the central metal atom is selected from the group consisting of the elements of Groups 8, 9, 10 and 11 of the periodic table; and (ii) transforming the halogen atom into an alkenyl group- or a curable silyl group-containing substituent. The obtained (meth)acrylic polymers form homogeneous curing materials.
摘要翻译：通过包括（i）使用有机卤化化合物或其制备具有卤素原子的（甲基）丙烯酸聚合物的方法制备具有高官能度比的链末端具有烯基或可固化甲硅烷基的（甲基）丙烯酸聚合物卤代磺酰基化合物作为引发剂和金属配合物催化剂，其中中心金属原子选自周期表第8,9,10和11族的元素; 和（ii）将卤素原子转化成烯基或含可固化甲硅烷基的取代基。得到的（甲基）丙烯酸聚合物形成均匀的固化材料。

23. 发明授权

US06350345B1 Curable resin composition 有权
标题翻译：可固化树脂组合物
公开(公告)号：US06350345B1
公开(公告)日：2002-02-26
申请号：US09584075
申请日：2000-06-01
申请人： Jun Kotani , Masato Kusakabe , Hiroshi Iwakiri
发明人： Jun Kotani , Masato Kusakabe , Hiroshi Iwakiri
IPC分类号： C09J18304
CPC分类号： C08L33/06 , C08L43/04 , C08L71/02 , C08L2666/14 , C09J143/04 , Y10S528/901
摘要： This invention has its object to provide a curable resin compositions useful as contact adhesives with a prolonged tack retention period, without affecting the final bond strength. This invention is related to a A curable resin composition which comprises (I) a reactive silicon group-containing polyether oligomer, (II) a copolymer comprising a molecular chain substantially composed of one or more acrylate ester monomer units and/or methacrylate ester monomer units and (III) an accelerator.
摘要翻译：本发明的目的是提供可用作具有延长的粘着保持期的接触粘合剂的可固化树脂组合物，而不影响最终粘合强度。本发明涉及一种可固化树脂组合物，其包含（I）含反应性硅基的聚醚低聚物，（II）包含基本上由一种或多种丙烯酸酯单体单元和/或甲基丙烯酸酯单体单元组成的分子链的共聚物和（III）加速器。

24. 发明授权

US06194516B1 Method for producing hydroxyl-terminated (meth) acrylic polymer 有权
标题翻译：羟基封端（甲基）丙烯酸聚合物的制备方法
公开(公告)号：US06194516B1
公开(公告)日：2001-02-27
申请号：US09164338
申请日：1998-10-01
申请人： Masato Kusakabe , Kenichi Kitano , Yoshiki Nakagawa
发明人： Masato Kusakabe , Kenichi Kitano , Yoshiki Nakagawa
IPC分类号： C08F830
CPC分类号： C08F8/14 , C08F8/30 , C08F2810/30 , C08F2810/40 , C08F120/18 , C08F8/42 , C08F8/26
摘要： A method for producing a hydroxyl-terminated (meth) acrylic polymer which comprises converting a halogen atom in a terminal structure of the general formula (1) —CH2—C(R1)(CO2R2)(X) (1) wherein R1 is hydrogen or methyl, R2 is alkyl containing 1 to 20 carbon atoms, aryl containing 6 to 20 carbon atoms or aralkyl containing 7 to 20 carbon atoms, and X is chlorine, bromine or iodine, of a (meth)acrylic polymer obtained by polymerizing a (meth)acrylic monomer using an organic halide or a halogenated sulfonyl compound as an initiator and, as a catalyst, a metal complex with a central metal selected from the elements belonging to the groups 8, 9, 10 and 11 in the periodic table, into a hydroxyl-containing substituent. The present invention can provide, in an easy and simple manner, a (meth)acrylic polymer which is hydroxyl-terminated at both ends in a high proportion and which has been difficult to produce in the prior art. It can give a cured product with good curing characteristics.
摘要翻译：一种羟基封端的（甲基）丙烯酸类聚合物的制造方法，其特征在于，将通式（1）的末端结构中的卤素原子转化为其中R 1为氢或甲基，R 2为含有1〜20个碳原子的烷基，含有6个至20个碳原子或含有7〜20个碳原子的芳烷基，X为氯，溴或碘，通过使用有机卤化物或卤代磺酰化合物作为引发剂使（甲基）丙烯酸单体聚合而得到的（甲基）作为催化剂，将选自元素周期表第8,9,10和11族的元素的中心金属的金属络合物转化为含羟基的取代基。本发明可以简单，简单的方式，在高比例羟基封端的双（甲基）丙烯酸类聚合物，并且在现有技术中难以生产。它可以得到具有良好固化特性的固化产品。

25. 发明授权

US5986014A Processes for preparing (meth)acrylic polymers having functional groups at the chain ends 失效
标题翻译：制备在链末端具有官能团的（甲基）丙烯酸聚合物的方法
公开(公告)号：US5986014A
公开(公告)日：1999-11-16
申请号：US798034
申请日：1997-02-06
申请人： Masato Kusakabe , Kenichi Kitano
发明人： Masato Kusakabe , Kenichi Kitano
IPC分类号： C08L83/04 , C08F8/00 , C08F8/26 , C08F8/42 , C08F20/10 , C08F20/12 , C08F299/00 , C08L83/07
CPC分类号： C08F8/26 , C08F8/42
摘要： (Meth)acrylic polymers having alkenyl or curable silyl groups at the chain ends high functionality ratios are prepared by a process which comprises (i) preparing a (meth)acrylic polymer having halogen atoms at the chain ends, using an organohalogenated compound or a halosulfonyl compound as an initiator and a metal complex catalyst wherein the central metal atom is selected from the group consisting of the elements of Groups 8, 9, 10 and 11 of the periodic table; and (ii) transforming the halogen atom into an alkenyl group- or a curable silyl group-containing substituent. The obtained (meth)acrylic polymers form homogeneous curing materials.
摘要翻译：通过包括（i）在链末端使用有机卤化化合物或卤代磺酰基制备具有卤素原子的（甲基）丙烯酸聚合物的方法制备在链末端具有链烯基或可固化甲硅烷基的（甲基）丙烯酸聚合物，化合物作为引发剂和金属配合物催化剂，其中中心金属原子选自周期表第8,9,10和11族的元素; 和（ii）将卤素原子转化成烯基或含可固化甲硅烷基的取代基。得到的（甲基）丙烯酸聚合物形成均匀的固化材料。

26. 发明授权

US09601780B2 Multilayer conductive film, current collector using same, battery and bipolar battery 有权
公开(公告)号：US09601780B2
公开(公告)日：2017-03-21
申请号：US14119290
申请日：2012-05-22
申请人： Yusuke Kato , Masahiro Kojima , Ryutaro Mukai , Masato Kusakabe , Hiroyuki Ogino , Takashi Kikuchi , Takashi Ito , Satoshi Oku , Akiko Waki , Shiho Inoue , Yuji Muroya , Norihisa Waki , Yasuyuki Tanaka , Shigeo Ibuka , Yoshio Shimoida
发明人： Yusuke Kato , Masahiro Kojima , Ryutaro Mukai , Masato Kusakabe , Hiroyuki Ogino , Takashi Kikuchi , Takashi Ito , Satoshi Oku , Akiko Waki , Shiho Inoue , Yuji Muroya , Norihisa Waki , Yasuyuki Tanaka , Shigeo Ibuka , Yoshio Shimoida
IPC分类号： H01M4/66 , H01M10/0525 , C08K3/04 , C08J7/04 , B32B27/08 , B32B27/20 , B32B27/28 , B32B27/32 , H01M4/02
CPC分类号： H01M4/668 , B32B27/08 , B32B27/20 , B32B27/281 , B32B27/325 , B32B2264/10 , B32B2264/105 , B32B2307/202 , B32B2307/206 , B32B2457/10 , C08G2261/3324 , C08G2261/418 , C08J7/047 , C08J2379/08 , C08J2465/00 , C08K3/04 , C08K2201/001 , H01M4/661 , H01M4/663 , H01M4/666 , H01M4/667 , H01M10/0525 , H01M2004/029 , Y02E60/122 , C08L65/00
摘要： A multilayer conductive film includes a layer 1 including a conductive material containing a polymer material 1 having an alicyclic structure and conductive particles 1 and a layer 2 including a material having durability against positive electrode potential. The multilayer conductive film has stability in an equilibrium potential environment in a negative electrode and stability in an equilibrium potential environment in a positive electrode, has low electric resistance per unit area in the thickness direction, and has excellent barrier properties for a solvent of an electrolytic solution. A battery including a current collector employing the multilayer conductive film can achieve both weight reduction and durability.

27. 发明申请

US20140186699A1 MULTILAYER CONDUCTIVE FILM, CURRENT COLLECTOR USING SAME, BATTERY AND BIPOLAR BATTERY 有权
标题翻译：多层导电膜，使用相同的电流收集器，电池和双极电池
公开(公告)号：US20140186699A1
公开(公告)日：2014-07-03
申请号：US14119290
申请日：2012-05-22
申请人： Yusuke Kato , Masahiro Kojima , Ryutaro Mukai , Masato Kusakabe , Hiroyuki Ogino , Takashi Kikuchi , Takashi Ito , Satoshi Oku , Akiko Waki , Shiho Inoue , Yuji Muroya , Norihisa Waki , Yasuyuki Tanaka , Shigeo Ibuka , Yoshio Shimoida
发明人： Yusuke Kato , Masahiro Kojima , Ryutaro Mukai , Masato Kusakabe , Hiroyuki Ogino , Takashi Kikuchi , Takashi Ito , Satoshi Oku , Akiko Waki , Shiho Inoue , Yuji Muroya , Norihisa Waki , Yasuyuki Tanaka , Shigeo Ibuka , Yoshio Shimoida
IPC分类号： H01M4/66
CPC分类号： H01M4/668 , B32B27/08 , B32B27/20 , B32B27/281 , B32B27/325 , B32B2264/10 , B32B2264/105 , B32B2307/202 , B32B2307/206 , B32B2457/10 , C08G2261/3324 , C08G2261/418 , C08J7/047 , C08J2379/08 , C08J2465/00 , C08K3/04 , C08K2201/001 , H01M4/661 , H01M4/663 , H01M4/666 , H01M4/667 , H01M10/0525 , H01M2004/029 , Y02E60/122 , C08L65/00
摘要： A multilayer conductive film includes a layer 1 including a conductive material containing a polymer material 1 having an alicyclic structure and conductive particles 1 and a layer 2 including a material having durability against positive electrode potential. The multilayer conductive film has stability in an equilibrium potential environment in a negative electrode and stability in an equilibrium potential environment in a positive electrode, has low electric resistance per unit area in the thickness direction, and has excellent barrier properties for a solvent of an electrolytic solution. A battery including a current collector employing the multilayer conductive film can achieve both weight reduction and durability.
摘要翻译：多层导电膜包括含有包含具有脂环结构的聚合物材料1和导电粒子1的导电材料的层1和包含具有对正极电位具有耐久性的材料的层2。多层导电膜在负极中的平衡势环境中具有稳定性，并且在正极中的平衡势环境中的稳定性，在厚度方向上的每单位面积的电阻低，并且对于电解质的溶剂具有优异的阻隔性解。包括使用多层导电膜的集电体的电池可以实现重量减轻和耐久性。

28. 发明申请

US20140099537A1 CONDUCTIVE FILM, CURRENT COLLECTOR USING SAME, BATTERY AND BIPOLAR BATTERY 审中-公开
标题翻译：导电膜，使用相同的电流收集器，电池和双极电池
公开(公告)号：US20140099537A1
公开(公告)日：2014-04-10
申请号：US14119308
申请日：2012-05-22
申请人： Yusuke Kato , Takashi Ito , Masami Yanagida , Satoshi Oku , Hiroyuki Ogino , Masato Kusakabe , Ryutaro Mukai , Masahiro Kojima , Takashi Kikuchi , Akiko Waki , Shiho Inoue , Shigeo Ibuka , Yasuyuki Tanaka , Yoshio Shimoida , Yuji Muroya , Norihisa Waki
发明人： Yusuke Kato , Takashi Ito , Masami Yanagida , Satoshi Oku , Hiroyuki Ogino , Masato Kusakabe , Ryutaro Mukai , Masahiro Kojima , Takashi Kikuchi , Akiko Waki , Shiho Inoue , Shigeo Ibuka , Yasuyuki Tanaka , Yoshio Shimoida , Yuji Muroya , Norihisa Waki
IPC分类号： H01M4/66
CPC分类号： H01M4/667 , H01M4/668 , H01M10/052 , H01M2004/029
摘要： A conductive film includes a layer 1 formed by a conductive material 1 that includes a polymer material 1 containing any of (1) an amine and an epoxy resin (where the epoxy resin and the amine are mixed in a ratio of 1.0 or more in terms of the ratio of the number of active hydrogen atoms in the amine with respect to the number of functional groups in the epoxy resin), (2) a phenoxy resin and an epoxy resin, (3) a saturated hydrocarbon polymer having a hydroxyl group, and (4) a curable resin and an elastomer and conductive particles 1. The conductive film has excellent stability in an equilibrium potential environment in a negative electrode and low electric resistance per unit area in the thickness direction. A multilayer conductive film including the conductive film achieves excellent interlayer adhesion, and using them as a current collector enables the production of a battery satisfying both weight reduction and durability.
摘要翻译：导电膜包括由导电材料1形成的层1，其包括聚合物材料1，其包含（1）胺和环氧树脂（其中环氧树脂和胺以1.0或更大的比例混合（2）苯氧基树脂和环氧树脂，（3）具有羟基的饱和烃聚合物，（3）具有羟基的饱和烃聚合物，和（4）可固化树脂和弹性体和导电颗粒1.导电膜在负极中的平衡电位环境中具有优异的稳定性，并且在厚度方向上具有每单位面积的低电阻。包括导电膜的多层导电膜具有优异的层间粘合性，并且作为集电体使用它们能够制造满足重量减轻和耐久性的电池。

29. 发明授权

US07625990B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US07625990B2
公开(公告)日：2009-12-01
申请号：US11579630
申请日：2005-04-25
申请人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08G77/00
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： A curable composition having good curability and adhesion comprising: (A) an reactive silicon group-containing organic polymer, (B) a titanium chelate represented by the general formula (1) or (2) and (C) a high molecular weight plasticizer having a number average molecular weight of 1,000 to 15,000. General formula (1): wherein each of n R1s is independently a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, each of (4-n) R2s is independently hydrogen atom or a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, each of (4-n) A1s and (4-n) A2s is independently —R3 or —OR3 where R3 is a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, n is 1, 2 or 3. General formula (2): wherein R2, A1 and A2 are the same as defined above, R4 is a substituted or unsubstituted divalent hydrocarbon group having 1 to 20 carbon atoms.
摘要翻译：具有良好固化性和粘合性的可固化组合物包含：（A）含反应性硅基的有机聚合物，（B）由通式（1）或（2）表示的钛螯合物和（C）具有高分子量增塑剂数均分子量为1,000〜15,000。通式（1）：其中，n个R 1各自独立地为取代或未取代的碳原子数1〜20的烃基，（4-n）R 2各自独立地为氢原子或取代或未取代的碳原子数1〜20的烃基（4-n）A1和（4-n）A2中的每一个独立地为-R 3或-OR 3，其中R 3为取代或未取代的具有1至20个碳原子的烃基，n为1,2或3.通式（2）：其中R2，A1和A2与上述定义相同，R4为取代或未取代的碳原子数1〜20的二价烃基。

30. 发明申请

US20080194773A1 Curable Composition Having Improved Adhesion 有权
标题翻译：具有改善粘合性的可固化组合物
公开(公告)号：US20080194773A1
公开(公告)日：2008-08-14
申请号：US11579587
申请日：2005-04-25
申请人： Masayuki Wakioka , Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
发明人： Masayuki Wakioka , Katsuyu Wakabayashi , Toshihiko Okamoto , Masato Kusakabe
IPC分类号： C08F20/06 , C08F283/00
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [Problems] There is provided a curable composition having good adhesion by using a non-organotin catalyst.[Means to Solve Problems] The curable composition comprises (A) an organic polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds and (B) one or more kinds selected from a titanium catalyst, an aluminum catalyst and a zirconium catalyst, and is characterized in that a stress at 50% tension is within a range from 0.01 MPa to 0.20 MPa, when determined by adding and mixing 1.5 parts of tin octylate, 0.25 part by weight of laurylamine and 0.6 part by weight of pure water to 100 parts by weight of the component (A), subjecting the mixture to centrifugal defoaming, pouring the mixture carefully into a polyethylene frame not to mix air bubbles thereto, aging the mixture at 23° C. for one hour, and further at 70° C. for 20 hours, punching the obtained 3 mm thick cured sheet according to JIS K6251 to obtain No. 3 dumbbell, and carrying out a tension test (tensile speed: 200 mm/min) at 23° C. at 50% RH.
摘要翻译： [问题]提供了通过使用非有机锡催化剂具有良好粘附性的可固化组合物。 [解决问题的方法]固化性组合物包含（A）具有能够通过形成硅氧烷键交联的含硅基团的有机聚合物和（B）选自钛催化剂，铝催化剂和锆的一种或多种催化剂，其特征在于，当通过加入和混合1.5份辛酸锡，0.25重量份月桂胺和0.6重量份纯水测定时，50％张力下的应力在0.01MPa至0.20MPa的范围内至100重量份的组分（A），将混合物进行离心脱泡，将混合物小心地注入聚乙烯框架中以不混合气泡，将混合物在23℃下老化1小时，进一步在70℃ ℃下冲洗20小时，根据JIS K6251冲压得到的3mm厚的固化片，得到3号哑铃，在23℃，50％RH下进行拉伸试验（拉伸速度：200mm / min）。

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