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21. 发明授权

US06858655B1 High-resilient polyurethane foams produced from polyether polyols 有权
标题翻译：由聚醚多元醇生产的高弹性聚氨酯泡沫
公开(公告)号：US06858655B1
公开(公告)日：2005-02-22
申请号：US10018332
申请日：2000-06-06
申请人： Jörg Hofmann , Pramod Gupta , Manfred Dietrich , Hansjürgen Rabe , Jürgen Grönen , Pieter Ooms
发明人： Jörg Hofmann , Pramod Gupta , Manfred Dietrich , Hansjürgen Rabe , Jürgen Grönen , Pieter Ooms
IPC分类号： C08G18/48 , C08G65/26 , C08G101/00 , C08G18/28
CPC分类号： C08G65/2663 , C08G18/4845 , C08G18/485 , C08G18/4866 , C08G2101/0008 , C08G2101/0083
摘要： Flexible polyurethane foams are produced from a polyisocyanate and a polyether polyol which has been alkoxylated in the presence of a double metal cyanide catalyst and that has at least one ethylene oxide-propylene oxide mixed block.
摘要翻译：柔性聚氨酯泡沫由多异氰酸酯和聚醚多元醇生产，所述多异氰酸酯和聚醚多元醇在双金属氰化物催化剂存在下被烷氧基化，并且具有至少一个环氧乙烷 - 环氧丙烷混合嵌段。

22. 发明授权

US06852663B2 Double-metal cyanide catalysts for preparing polyether polyols 失效
标题翻译：用于制备聚醚多元醇的双金属氰化物催化剂
公开(公告)号：US06852663B2
公开(公告)日：2005-02-08
申请号：US10138080
申请日：2002-05-03
申请人： Pieter Ooms , Jöerg Hofmann , Walter Schäfer
发明人： Pieter Ooms , Jöerg Hofmann , Walter Schäfer
IPC分类号： B01J27/26 , C08G65/26 , B01J31/00
CPC分类号： C08G65/2663 , B01J27/26
摘要： The invention is directed to a double-metal cyanide catalyst for the preparation of a polyether polyol by the polyaddition of an alkylene oxide on to a starter compound containing active hydrogen atoms, wherein the DMC catalyst comprises a) at least one double-metal cyanide compound; b) at least one organic complexing ligand which is not a polyether, polyester, polycarbonate, polyalkylene glycol sorbitan ester, polyalkylene glycol glycidyl ether, glycidyl ether, glycoside, carboxylic acid ester of polyhydric alcohol, cyclodextrin, phosphorus compound, α,β-unsaturated carboxylic acid ester or ionic surfactant compound; c) at least one polyether; and d) at least one polyester, polycarbonate, polyalkylene glycol sorbitan ester, polyalkylene glycol glycidyl ether, glycidyl ether, glycoside, carboxylic acid ester of polyhydric alcohol, cyclodextrin, phosphorus compound, α,β-unsaturated carboxylic acid ester or ionic surfactant compound. The catalyst of the present invention has increased activity in the preparation of a polyether polyol.
摘要翻译：本发明涉及用于通过将烯化氧加成到含有活性氢原子的起始化合物上制备聚醚多元醇的双金属氰化物催化剂，其中DMC催化剂包含a）至少一种双金属氰化物化合物 ; b）至少一种不是聚醚，聚酯，聚碳酸酯，聚亚烷基二醇脱水山梨糖醇酯，聚亚烷基二醇缩水甘油醚，缩水甘油醚，糖苷，多元醇的羧酸酯，环糊精，磷化合物，α，β-不饱和的有机络合配体羧酸酯或离子表面活性剂化合物; c）至少一种聚醚; 和d）至少一种聚酯，聚碳酸酯，聚亚烷基二醇脱水山梨糖醇酯，聚亚烷基二醇缩水甘油醚，缩水甘油醚，糖苷，多元醇的羧酸酯，环糊精，磷化合物，α，β-不饱和羧酸酯或离子表面活性剂化合物。本发明的催化剂在制备聚醚多元醇时具有增加的活性。

23. 发明授权

US08304509B2 Process for preparing diaryl carbonates from dialkyl carbonates 有权
标题翻译：由碳酸二烷基酯制备碳酸二芳基酯的方法
公开(公告)号：US08304509B2
公开(公告)日：2012-11-06
申请号：US13251381
申请日：2011-10-03
申请人： Christoph Gürtler , Thomas Ernst Müller , Pieter Ooms , Friedhelm Risse , Johann Rechner , Franco Doro , Angelina Prokofieva
发明人： Christoph Gürtler , Thomas Ernst Müller , Pieter Ooms , Friedhelm Risse , Johann Rechner , Franco Doro , Angelina Prokofieva
IPC分类号： C08G64/06 , C08G64/00
CPC分类号： C07C68/06 , C07C68/065 , C07D317/36 , C08G64/06 , C08G64/307 , C07C69/96
摘要： The present invention relates to a process for continuously preparing diaryl carbonates from dialkyl carbonates and at least one monohydroxyl compound in the presence of catalysts, and to the use thereof for preparation of polycarbonates. The alkylene glycol obtained in the preparation of the dialkyl carbonate used is recycled by oxidative carbonylation with carbon monoxide in the presence of a catalyst to give the cyclic alkylene carbonate which is in turn converted to the dialkyl carbonate. More particularly, the process utilizes the alkylene glycol obtained for the diphenyl carbonate preparation process (DPC process).
摘要翻译：本发明涉及一种在催化剂存在下从碳酸二烷基酯和至少一种单羟基化合物连续制备碳酸二芳酯的方法及其用于制备聚碳酸酯的方法。在制备碳酸二烷基酯中获得的亚烷基二醇在催化剂存在下通过氧化羰基化与一氧化碳再循环，得到环状亚烷基碳酸酯，然后将其转化为碳酸二烷基酯。更具体地，该方法利用获得的用于碳酸二苯酯制备方法的亚烷基二醇（DPC方法）。

24. 发明申请

US20120101293A1 PROCESS FOR CONTINUOUSLY PREPARING DIALKYL CARBONATE 审中-公开
标题翻译：连续制备碳酸氢钾的方法
公开(公告)号：US20120101293A1
公开(公告)日：2012-04-26
申请号：US13280438
申请日：2011-10-25
申请人： Pieter Ooms , Friedhelm Risse , Andre Düx , Carsten Buchaly , Thomas Pancur , Arthur Susanto , Georg Ronge , Johan Vanden Eynde , Wim Wuytack
发明人： Pieter Ooms , Friedhelm Risse , Andre Düx , Carsten Buchaly , Thomas Pancur , Arthur Susanto , Georg Ronge , Johan Vanden Eynde , Wim Wuytack
IPC分类号： C07C68/08
CPC分类号： C07C68/08 , Y02P20/127 , C07C69/96
摘要： The present invention relates to a continuous process for purifying a dialkyl carbonate/alkyl alcohol mixture in the preparation of dialkyl carbonate by catalysed transesterification of a cyclic alkylene carbonate (e.g. ethylene carbonate or propylene carbonate) with alkyl alcohols. For the increase in the product quality of the dialkyl carbonate, the selection of the operating parameters of the dialkyl carbonate purification column are crucial, in order to reduce the formation of unwanted by-products such as alkoxy alcohols and aliphatic carbonate ethers.
摘要翻译：本发明涉及通过环状碳酸亚烷基酯（例如碳酸亚乙酯或碳酸亚丙酯）与烷基醇的催化酯交换反应来制备碳酸二烷基酯中的碳酸二烷基酯/烷基醇混合物的连续方法。为了提高碳酸二烷基酯的产品质量，选择碳酸二烷基二烷基酯纯化塔的操作参数至关重要，以减少不需要的副产物如烷醇和脂族碳酸酯醚的形成。

25. 发明申请

US20090240021A1 PROCESS FOR THE PREPARATION OF POLYCARBONATES AND DIARYL CARBONATE 有权
标题翻译：制备聚碳酸酯和二氧化碳的方法
公开(公告)号：US20090240021A1
公开(公告)日：2009-09-24
申请号：US12370182
申请日：2009-02-12
申请人： Helmut-Werner Heuer , Pieter Ooms
发明人： Helmut-Werner Heuer , Pieter Ooms
IPC分类号： C08G64/30 , B01J19/18
CPC分类号： C08G64/24 , C07C68/02 , C07C69/96
摘要： The present invention relates to a process for the continuous preparation of polycarbonates or diaryl carbonates by the method of the phase boundary process, in which both the mixing of the organic and aqueous phase and the upstream oligomerization step or aryl chloroformate and/or diaryl carbonate preparation step are effected in a special pump.
摘要翻译：本发明涉及通过相界方法连续制备聚碳酸酯或二芳基碳酸酯的方法，其中有机相和水相的混合与上游低聚步骤或氯甲酸芳基酯和/或碳酸二芳基酯制备步骤在特殊的泵中进行。

26. 发明申请

US20090215977A1 PROCESS FOR THE PREPARATION OF POLYCARBONATE 有权
标题翻译：制备聚碳酸酯的方法
公开(公告)号：US20090215977A1
公开(公告)日：2009-08-27
申请号：US12390794
申请日：2009-02-23
申请人： Pieter Ooms , Andreas Bulan , Rainer Weber , Johann Rechner
发明人： Pieter Ooms , Andreas Bulan , Rainer Weber , Johann Rechner
IPC分类号： C08G64/24
CPC分类号： C08G64/24 , C01D3/06 , Y02P20/582
摘要： The invention relates to a combined process for the preparation of polycarbonate by the phase boundary process and downstream electrolysis of sodium chloride-containing process wastewater.
摘要翻译：本发明涉及通过相边界法制备聚碳酸酯的方法和含氯化钠的工艺废水的下游电解。

27. 发明授权

US06600064B2 Process for the preparation of hydroxybenzoic benzyl esters 失效
公开(公告)号：US06600064B2
公开(公告)日：2003-07-29
申请号：US10090392
申请日：2002-03-04
申请人： Pieter Ooms , Bernd-Ulrich Schenke
发明人： Pieter Ooms , Bernd-Ulrich Schenke
IPC分类号： C07C6976
CPC分类号： C07C67/24 , C07C69/84
摘要： The invention relates to a process for the preparation of hydroxybenzoic benzyl esters by reacting dibenzyl ethers with alkylcarbonyloxybenzoic or alkoxycarbonyloxybenzoic acids and optionally anhydrides thereof in the presence of one or more acids as catalyst.

28. 发明授权

US06414192B1 Process for preparing 4-aminodiphenylamine 失效
标题翻译：制备4-氨基二苯胺的方法
公开(公告)号：US06414192B1
公开(公告)日：2002-07-02
申请号：US10007014
申请日：2001-11-06
申请人： Michael Schelhaas , Carl Casser , Dietmar Bielefeldt , Pieter Ooms , Joachim Haider , Manfred Jautelat , Christian Laue , Henry Giera
发明人： Michael Schelhaas , Carl Casser , Dietmar Bielefeldt , Pieter Ooms , Joachim Haider , Manfred Jautelat , Christian Laue , Henry Giera
IPC分类号： C07C20900
CPC分类号： C07C209/38 , C07C211/55
摘要： The invention provides a process for preparing 4-aminodiphenylamine, an important starting product for synthesizing antioxidants and stabilizers in the rubber and polymer industry, by hydrogenating nitrosobenzene with hydrogen in the presence of a proton acid as catalyst and in the presence of a hydrogenating catalyst, optionally in the presence of an inert organic solvent and thermally decomposing the 4-ADPA ammonium salt produced in this way, wherein 4-ADPA is obtained. 4-aminodiphenylamine is produced in good yields and high purity by the process according to the present invention. Furthermore, no effluent is produced, which makes the process particularly economic and ecological.
摘要翻译：本发明提供一种制备4-氨基二苯胺的方法，该方法是在质子酸作为催化剂存在下，在氢化催化剂存在下，通过在氢气存在下，用氢气将亚硝基苯氢化，在橡胶和聚合物工业中合成抗氧化剂和稳定剂的重要起始产物，任选地在惰性有机溶剂的存在下，并以这种方式产生的4-ADPA铵盐热分解，得到4-ADPA。4-氨基二苯胺通过本发明的方法以良好的产率和高纯度生产。此外，没有产生流出物，这使得该过程特别经济和生态。

29. 发明授权

US5932768A Process for the preparation of 4-aminodiphenylamine 失效
标题翻译： 4-氨基二苯胺的制备方法
公开(公告)号：US5932768A
公开(公告)日：1999-08-03
申请号：US126344
申请日：1998-07-30
申请人： Pieter Ooms , Ulrich Notheis , Christian Laue
发明人： Pieter Ooms , Ulrich Notheis , Christian Laue
IPC分类号： B01J21/16 , B01J23/42 , B01J23/44 , B01J23/46 , B01J29/44 , B01J29/62 , C07B61/00 , C07C209/36 , C07C209/38 , C07C211/54 , C07C211/55 , C07C209/30
CPC分类号： C07C209/38 , C07C209/36
摘要： 4-aminodiphenylamines are prepared by hydrogenating nitrosobenzene or mixtures of nitrosobenzene and nitrobenzene with hydrogen in the presence of bases containing hydroxide, oxide and/or alkoxide groups and heterogeneous catalysts in inert aprotic solvents at temperatures of from 0 to 200.degree. C. and at pressures of from 0.1 to 150 bar.
摘要翻译：在惰性非质子传递溶剂中，在0至200℃的温度和压力下，在含有氢氧化物，氧化物和/或醇盐基团的碱和非均相催化剂的存在下，将亚硝基苯或亚硝基苯和硝基苯的混合物与氢气氢化制备4-氨基二苯胺，为0.1至150巴。

30. 发明授权

US5679825A Process for the production of aryl carbonates 失效
标题翻译：制备芳基碳酸酯的方法
公开(公告)号：US5679825A
公开(公告)日：1997-10-21
申请号：US583882
申请日：1996-01-11
申请人： Pieter Ooms , Hans-Josef Buysch
发明人： Pieter Ooms , Hans-Josef Buysch
IPC分类号： B01J21/06 , B01J23/28 , B01J23/30 , B01J27/22 , B01J27/24 , C07B61/00 , C07C68/02 , C07C68/06 , C07C69/96
CPC分类号： C07C68/02
摘要： Carbonates with aromatic ester groups may be produced by reacting aromatic monohydroxy compounds with phosgene or with chlorocarbonates of aromatic monohydroxy compounds, wherein a temperature in the range from 50.degree. to 450.degree. C. and a pressure in the range from 0.05 to 20 bar are used in the presence of hard materials with metal-like properties (ceramic precursors) as heterogeneous catalysts.
摘要翻译：具有芳族酯基的碳酸酯可以通过使芳族单羟基化合物与光气或芳族单羟基化合物的氯碳酸酯反应来制备，其中使用温度在50℃至450℃的温度和0.05至20巴的压力范围内在具有金属状特性的硬质材料（陶瓷前体）作为非均相催化剂的存在下。

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