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21. 发明授权

US6096240A Composition for the removal of water from a surface 失效
标题翻译：用于从表面去除水的组合物
公开(公告)号：US6096240A
公开(公告)日：2000-08-01
申请号：US320651
申请日：1999-05-27
申请人： Ezio Strepparola , Simonetta Fontana , Rossella Silvani
发明人： Ezio Strepparola , Simonetta Fontana , Rossella Silvani
IPC分类号： B01D12/00 , C08G65/00 , C09D171/08 , C09K3/00
CPC分类号： C08G65/007 , B01D12/00
摘要： Method for the water removal from a surface, which comprises covering the surface with a composition having specific weight higher than that of the water, and subsequently removing water from the composition by skimming, such composition comprising a (per)fluoropolyether having molecular weight comprised between 300 and 1500 and a non ionic additive having a (perfluoropolyethereal structure similar to that of the solvent, linked to an hydrogenated part of hydrophilic type, the molecular weight of the (per)fluorinated part is comprised between 400 and 1200 and the ratio by weight between (per)fluorinated part and hydrogenated part is comprised between 1.5 and 3.5.
摘要翻译：从表面除去水的方法，其包括用具有比水重量更高的比重的组合物覆盖表面，以及随后通过撇取从组合物中除去水，该组合物包含（per）含氟聚醚，其分子量介于 300和1500的非离子添加剂和具有与溶剂相类似的全氟聚醚结构的非离子添加剂，与亲水型的氢化部分相连，（每个）氟化部分的分子量在400和1200之间，重量比（全）氟化部分和氢化部分之间的比例在1.5和3.5之间。

22. 发明授权

US5969192A Process for preparing hydrogen-terminated polyoxyperfluoroalkanes 失效
标题翻译：制备氢封端的聚氧氟烷烃的方法
公开(公告)号：US5969192A
公开(公告)日：1999-10-19
申请号：US769861
申请日：1996-12-19
申请人： Giuseppe Marchionni , Gianfranco Spataro , Ezio Strepparola
发明人： Giuseppe Marchionni , Gianfranco Spataro , Ezio Strepparola
IPC分类号： C08G65/00 , C08G65/324 , C07C43/11
CPC分类号： C08G65/007 , C08G65/324
摘要： A process for preparing hydrogen-terminated polyoxyperfluoroalkanes having molecular weight lower than 1800, by decarboxylation of the corresponding polyoxyperfluoroalkanes having one or two end groups selected form --OCF.sub.2 COOZ, --OCF.sub.2 CF.sub.2 COOZ and --OCF(CF.sub.3)COOZ, wherein Z is an alkaline metal or ammonium, carried out in the presence of water at temperatures from 140.degree.-170.degree. C. and under a pressure of at least 4 atmospheres.
摘要翻译：通过使具有一个或两个选自-OCF 2 COOZ，-OCF 2 CF 2 COOZ和-OCF（CF 3）COOZ的端基的相应的聚氧氟烷烃脱羧来制备分子量低于1800的氢封端的聚氧全氟烷烃的方法，其中Z是碱金属或铵在140-170℃的温度和至少4个大气压的压力下在水的存在下进行。

23. 发明授权

US5917008A Polytetrafluoroethylene dispersions in an organic solvent and dispersing agents employed therein 失效
标题翻译：聚四氟乙烯分散在有机溶剂中并在其中使用分散剂
公开(公告)号：US5917008A
公开(公告)日：1999-06-29
申请号：US100037
申请日：1998-06-19
申请人： Laura Montagna , Ezio Strepparola
发明人： Laura Montagna , Ezio Strepparola
IPC分类号： C03C25/24 , C07C69/708 , C07C235/06 , C07C235/08 , C08G65/00 , C08G65/22 , C08J3/11 , C08K5/00 , C08K5/17 , C08K5/20 , C08L27/12 , C08L27/18 , C08L67/00 , C08L71/00 , C08L71/02 , C08L77/00 , C09D127/12 , C10M107/38 , C08G73/24
CPC分类号： C08J3/11 , C07C235/06 , C07C235/08 , C07C69/708 , C08G65/007 , C10M107/38 , C08J2327/18 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66 , C10N2250/121
摘要： Polytetrafluoroethylene (PTFE) dispersions in an organic solvent, comprising:(A) from 2 to 40% by weight of PTFE in powder form;(B) from 50 to 95% by weight of an organic solvent;(C) from 0.5 to 10% by weight of a dispersing agent of formula:(R.sub.H -L).sub.y -(R.sub.F -L).sub.x R.sub.H (I)whereinx is an integer from 1 to 3;y is 0 or 1, with the proviso that x=1 when y=1;R.sub.H is a x-functional radical having an alkylic or polyoxyalkylenic structure;R.sub.F is (per)fluoropolyoxyalkylenic radical;L is a divalent organic group.Such dispersions are utilized for the surface treatment of metals, glass fibers, and the like, and in particular as mould release agents.
摘要翻译：聚四氟乙烯（PTFE）分散在有机溶剂中，包括：（A）粉末形式的2至40重量％的PTFE; （B）50〜95重量％的有机溶剂; （C）0.5至10重量％的分子式为：（RH-L）y-（RF-L）xRH（I）其中x为1至3的整数; y为0或1，条件是当y = 1时x = 1; RH是具有烷基或聚氧亚烷基结构的x-官能团; RF是（全）氟聚氧亚烷基; L是二价有机基团。这种分散体用于金属，玻璃纤维等的表面处理，特别是脱模剂。

24. 发明授权

US5714637A Functionalized fluoropolyethers 失效
标题翻译：官能化含氟聚醚
公开(公告)号：US5714637A
公开(公告)日：1998-02-03
申请号：US458330
申请日：1995-06-02
申请人： Giuseppe Marchionni , Piero Gavezotti , Ezio Strepparola
发明人： Giuseppe Marchionni , Piero Gavezotti , Ezio Strepparola
IPC分类号： C07D209/48 , C07C43/11 , C07C43/12 , C07C43/13 , C07C43/315 , C07C49/84 , C07C59/315 , C07C69/708 , C07C217/26 , C07C233/18 , C07C235/06 , C07C235/10 , C07C235/12 , C07C255/13 , C07C257/14 , C07D235/12 , C07D251/24 , C07D263/56 , C07D277/64 , C07D303/20 , C07D317/54 , C07F7/18 , C08G65/00 , C08G65/22 , C08G65/32 , C08G65/328 , C08G65/329 , C08G65/48 , C08K5/06 , C07C45/00
CPC分类号： C08G65/329 , C08G65/007 , C08G65/226 , C08G65/32
摘要： Fluoropolyethers having functional groups, consisting of randomly distributed sequences of perfluoropolyoxyalkylene units selected from: ##STR1## and included in one of the following formulas: ##STR2## T'--O--(CF.sub.2 CF.sub.2 O).sub.p (CF.sub.2 O).sub.s --CRR'--Y(II) ##STR3## where X is F or CF.sub.3 T, T', T"=a perfluoroalkyl group containing from 1 to 3 carbon atoms and one or two atoms of Cl, Br or I; R, R'=halogen atoms; Y=a functional group; o, q=numbers, zero included, such that o+q=1-20; n=a number ranging from 1 to 15; m/n=a number ranging from 0.01 to 0.5; p=a number ranging from 1 to 20; s/p=a number ranging from 0.5 to 2; and z/o+p=a number ranging from 0.01 to 0.05.
摘要翻译：具有官能团的含氟聚醚，其由选自以下的全氟聚氧化烯单元的随机分布的序列组成：并且包括在下列其中之一中：（I）T'-O-（CF 2 CF 2 O）p（CF 2 O）（II）其中X为F或CF 3 T，T'，T“=含有1至3个碳原子和1或2个Cl，Br或I原子的全氟烷基 ; R，R'=卤素原子; Y =官能团; o，q =数字，包括零，使得o + q = 1-20; n = 1到15之间的数字; m / n = 0.01〜0.5的数; p = 1到20之间的数字; s / p =从0.5到2的数字; z + o + p = 0.01〜0.05的数。

25. 发明授权

US5623037A Coatings based on perfluoropolyethers containing acrylic groups 失效
标题翻译：基于含有丙烯酸基团的全氟聚醚的涂料
公开(公告)号：US5623037A
公开(公告)日：1997-04-22
申请号：US234912
申请日：1994-04-28
申请人： Giovanni Simeone , Claudio Tonelli , Ezio Strepparola , Fabrizio Mutta
发明人： Giovanni Simeone , Claudio Tonelli , Ezio Strepparola , Fabrizio Mutta
IPC分类号： C08F299/02 , C07C69/653 , C08F20/24 , C08F290/00 , C08G65/32 , C09D4/00 , C09D133/04 , C09D133/14 , C09D133/16 , C09D171/00 , C08F16/24
CPC分类号： C08F20/24 , C07C69/653 , C09D133/16
摘要： Coatings based on perfluoropolyethers terminated with acrylic groups and containing ethoxylic groups as a connecting bridge between the fluorinated part and the (meth)acrylic group.
摘要翻译：基于全氟聚醚的涂料，其以丙烯酸基封端并含有乙氧基作为氟化部分和（甲基）丙烯酸基团之间的连接桥。

26. 发明授权

US5294248A Polishes for metal surfaces containing cationic emulsifiers, and cationic emulsifiers contained therein 失效
标题翻译：含有阳离子乳化剂的金属表面的抛光剂和其中包含的阳离子乳化剂
公开(公告)号：US5294248A
公开(公告)日：1994-03-15
申请号：US20144
申请日：1993-02-19
申请人： Alba Chittofrati , Viviana Boselli , Giovanni Gavazzi , Ezio Strepparola , Renato Spiti , Silvia Tresoldi
发明人： Alba Chittofrati , Viviana Boselli , Giovanni Gavazzi , Ezio Strepparola , Renato Spiti , Silvia Tresoldi
IPC分类号： B01F17/46 , C08G65/00 , C08G65/32 , C08L71/02 , C09G1/10 , C09G1/04 , C09G1/12
CPC分类号： C09G1/10 , C08G65/007
摘要： Polishes for metal surfaces, based on dispersions of waxes, fluorinated polymers and perfluoropolyoxyalkylene oils acquire high gloss characteristics combined with improved water-repellency and resistance to soiling of 0.1-5% by weight of at least a cationic emulsifier comprised in the general formulaR--L--Q.sup.+ X.sup.-.sub.t (I)where:R=a chain of perfluoropolyoxyalkylene units;L=a divalent organic group;Q=a polar group;X=a halogen, or a group of formulaCH.sub.3 -Phenylene-SO.sub.3.sup.-R"SO.sub.3 --R"=F-(CF.sub.2).sub.m -;t=1 or 2;m=1-4.The polished containing the emulsifiers of formula (I) as well as the compounds comprised in said formula are claimed as new products.
摘要翻译：基于蜡，氟化聚合物和全氟聚氧化烯油的分散体，用于金属表面的抛光获得高光泽特性，结合改善的防水性和耐污染性至少为通式RL-中包含的至少一种阳离子乳化剂0.1-5重量％ Q + Xt（I）其中：R =全氟聚氧化烯单元链; L =二价有机基团; Q =极性基团; X =卤素或式为CH 3 - 亚苯基-SO 3 -R“SO 3 -R”= F-（CF 2）m - 的基团; t = 1或2; m = 1-4。含有式（I）的乳化剂的抛光剂以及所述式中包含的化合物被称为新产品。

27. 发明授权

US06509509B2 Process for the preparation of perfluoropolyoxyalkylenes with hydroxyl end groups 失效
标题翻译：用羟基端基制备全氟聚氧化烯的方法
公开(公告)号：US06509509B2
公开(公告)日：2003-01-21
申请号：US09750101
申请日：2000-12-29
申请人： Claudio Tonelli , Antonio Russo , Ezio Strepparola
发明人： Claudio Tonelli , Antonio Russo , Ezio Strepparola
IPC分类号： C07C4311
CPC分类号： C08G65/324 , C08G65/007
摘要： A process for preparing perfluoropolyoxyalkylenes with hydroxyl end groups having structure: T1—CFW1—O—Rf—CFW2—T2 (I) wherein: T1, T2, are selected from —CH2OH, —F, —CF3, —CF2CF3 with the proviso that at least one of T1 and T2 is —CH2OH; W1 and W2 are selected from F, CF3; Rf is a perfluoropolyoxyalkylene chain having a number average molecular weight 500-10,000 comprising one or more units of the type —CF2CF2O—, —CF2O—, —C3F6O—, —CF2(CF2)zCF2O— (z=1,2); —CR4R5CF2CF2O— with R4 and R5 selected from H, Cl, perfluoroalkyl group; said process comprising the following steps: a) adding an ester precursor having structure (I) and T1, T2 end groups selected from —F, —CF3, —CF2CF3, —COOR (R=linear or branched alkyl group having a number of C atoms from 1 to 5), with the proviso that at least one of T1 and T2 is —COOR, in a reaction mixture formed by: an inert or protic reaction solvent; a reducing agent selected from metal hydrides; an unreactive organic base with respect to the ester; b) hydrolysis of the product obtained in step a) for obtaining the compounds of structure (I) with at least a —CH2OH end group.
摘要翻译：制备具有以下结构的羟基端基的全氟聚氧化烯的方法：其中：T1，T2选自-CH2OH，-F，-CF3，-CF2CF3，条件是T1和T2中的至少一个为-CH2OH; W1和W2 选自F，CF 3; Rf是数均分子量为500-10,000的全氟聚氧亚烷基链，其包含一种或多种-CF 2 CF 2 O-，-CF 2 O-，-C 3 F 6 O-，-CF 2（CF 2）z CF 2 O-（z = 1,2）; -CR4R5CF2CF2O-，其中R4和R5选自H，Cl，全氟烷基; 所述方法包括以下步骤：a）加入具有结构（I）和T1的酯前体，T2端基选自-F，-CF 3，-CF 2 CF 3，-COOR（R =直链或支链烷基，其数目为C 原子从1至5），条件是至少一个T1和T2是-COOR，在由惰性或质子反应溶剂形成的反应混合物中;还原剂选自金属氢化物;非反应性有机碱，相对于酯化; b）在步骤a）中获得的产物的水解，得到至少具有-CH 2 OH端基的结构（I）化合物。

28. 发明授权

US06448319B1 Curable fluoroelastomer compositions 有权
标题翻译：可固化的含氟弹性体组合物
公开(公告)号：US06448319B1
公开(公告)日：2002-09-10
申请号：US09481698
申请日：2000-01-12
申请人： Ezio Strepparola , Franco Barbieri
发明人： Ezio Strepparola , Franco Barbieri
IPC分类号： C08K506
CPC分类号： C08K5/06 , C08L27/16 , C08L59/00 , C08L2666/14
摘要： Use in curable fluoroelastomer compositions of additives having polyacetal structure of general formula: HOCH2—[Rf—CH2O(CH2O)cCH2]t—Rf—CH2OH (I) wherein: c=1-10, preferably 1-3; t=0.5-20. Rf=poly-fluorooxyalkylenic chain, having number average molecular weight ({overscore (M)}n) in the range 500-2,500, preferably 1,000-2,000; the number average molecular weight of the formula (I) additive is in the range 3,000-15,000, preferably 3,000-10,000.
摘要翻译：在具有以下通式的聚缩醛结构的添加剂的可固化含氟弹性体组合物中使用：其中：c = 1-10，优选1-3; t = 0.5-20.Rf =数均分子量（{overscore（M）} n）在500-2,500，优选1,000-2,000范围内的聚氟氧烷基链;式（I）的数均分子量添加剂在3,000-15,000，优选3,000-10,000的范围内。

29. 发明授权

US6005054A Curable composition of fluoroelastomers 失效
标题翻译：含氟弹性体的固化组合物
公开(公告)号：US6005054A
公开(公告)日：1999-12-21
申请号：US848660
申请日：1997-04-29
申请人： Franco Barbieri , Ezio Strepparola , Mauro Luca Villa , Raffaele Ferro
发明人： Franco Barbieri , Ezio Strepparola , Mauro Luca Villa , Raffaele Ferro
IPC分类号： C08K5/06 , C08L27/12 , C08L27/16 , C08L71/00
CPC分类号： C08L27/12 , C08L27/16 , C08L71/00
摘要： Use of additives of the classes of mono- and/or di-hydroxypolyfluoroethers comprising the fluoropolyoxyalkylenic repeating units chosen from the following ones: (C.sub.3 F.sub.6 O); (CFXO) wherein X=F, CF.sub.3 ; (CH.sub.2 CF.sub.2 CF.sub.2 O); (CF.sub.2 (CF.sub.2).sub.z CF.sub.2 O) wherein z is an integer equal to 1 or 2; (C.sub.2 F.sub.4 O), in curable compositions of fluoroelastomers to improve the coefficient of friction without lowering the adhesion with bonding agents to metal reinforcements.
摘要翻译：使用包含选自以下的氟代聚氧亚烷基重复单元的单 - 和/或二 - 羟基多氟醚类的添加剂：（C 3 F 6 O）; （CFXO）其中X = F，CF 3; （CH 2 CF 2 CF 2 O）（CF 2（CF 2）z CF 2 O）其中z是等于1或2的整数; （C2F4O），用于改善摩擦系数而不降低与粘合剂对金属增强材料的粘合性的含氟弹性体的可固化组合物。

30. 发明授权

US5395657A Process for imparting oil- and water-repellency to the surface of porous ceramic materials 失效
标题翻译：赋予多孔陶瓷材料表面防油拒水性的方法
公开(公告)号：US5395657A
公开(公告)日：1995-03-07
申请号：US168712
申请日：1993-12-16
申请人： Ezio Strepparola , Viviana Boselli , Mauro Scapin
发明人： Ezio Strepparola , Viviana Boselli , Mauro Scapin
IPC分类号： C04B38/00 , C04B41/46 , C04B41/83 , C07F9/09 , C08F8/40 , C08G65/00 , C08G65/327 , C09K3/18 , B05D3/02
CPC分类号： C08G65/327 , C04B41/466 , C07F9/091 , C08G65/007 , Y10T428/31544 , Y10T428/4935
摘要： Oil- and water-repellency is imparted to the surface of a porous ceramic material, in particular of "cotto", by applying a phosphoric monoester having formula: ##STR1## where: L is a divalent organic group; m=1; Y is --F or --CF.sub.3 ;Z.sup.+ is a cation; R.sub.f is a polyperfluoroalkylene oxide chain.
摘要翻译：通过施加具有下式的磷酸单酯，其中：L是二价有机基团，赋予多孔陶瓷材料，特别是“cotto”表面的拒水拒油性。 m = 1; Y为-F或-CF 3; Z +是阳离子; Rf是聚全氟氧化烯链。

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