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21. 发明授权

US5051504A Doubled triphenylmethane dyes having bis acylpiperazine linkage 失效
标题翻译：具有双酰基哌嗪键的双重三苯甲烷染料
公开(公告)号：US5051504A
公开(公告)日：1991-09-24
申请号：US521382
申请日：1990-05-10
申请人： Erwin Hahn , Walter Breitschaft , Udo Mayer , Gunter-Rudolf Schroeder
发明人： Erwin Hahn , Walter Breitschaft , Udo Mayer , Gunter-Rudolf Schroeder
IPC分类号： C07D295/18 , C07D295/185 , C09B11/00 , C09B11/10 , C09B11/12 , C09B11/16 , C09B11/18 , D06P1/42 , D21H21/28
CPC分类号： C07D295/185 , C09B11/12 , C09B11/16 , C09B11/18
摘要： Triphenylmethane dyes of the formula ##STR1## where each R.sup.1 is independently of the others hydrogen or substituted or unsubstituted C.sub.1 -C.sub.6 -alkyl, or two R.sup.1 radicals together with the nitrogen atom joining them form a heterocyclic radical,R.sup.2 and R.sup.5 is independently of the others hydrogen or C.sub.1 -C.sub.4 -alkyl,R.sup.3 and R.sup.4 is independently of the others hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy or halogen,An.sup..crclbar. is one equivalent of an anion, andn is 1 or 2,preparable from piperazine derivatives as intermediates, are useful for coloring paper.
摘要翻译：其中每个R 1独立于其它的氢或取代或未取代的C 1 -C 6 - 烷基或两个R 1基团与连接它们的氮原子一起形成杂环基，R 2和 R5独立于氢或C1-C4-烷基，R3和R4独立于氢，C1-C4-烷基，C1-C4-烷氧基或卤素，An（ - ）是1当量的阴离子，和 n为1或2，可用作中间体的哌嗪衍生物，可用于着色纸。

22. 发明授权

US4908041A Navy and black dye mixtures: thiophene azo disperse dye and red, yellow or orange disperse dye 失效
标题翻译：海军和黑色染料混合物：噻吩偶氮分散染料和红色，黄色或橙色分散染料
公开(公告)号：US4908041A
公开(公告)日：1990-03-13
申请号：US256997
申请日：1988-10-13
申请人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Helmut Degen , Reinhold Krallmann , Gerhard Wagenblast
发明人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Helmut Degen , Reinhold Krallmann , Gerhard Wagenblast
IPC分类号： C09B29/00 , C09B67/22
CPC分类号： C09B67/0041 , C09B29/0059 , Y10S8/922
摘要： Navy and black dye mixtures contain one or more thiophene-azo dyes of the formula ##STR1## where R.sup.1, R.sup.2, R.sup.3, R.sup.4, R.sup.5, X and Y each have defined meanings, and one or more dyes F whose absorption maximum is at a wavelength of from 390 to 520 nm, the proportion of thiophene-azo dyes being from 60 to 99% by weight, based on the total weight of thiophene-azo dyes and dyes F in the mixture.
摘要翻译：海军和黑色染料混合物含有一种或多种式（IMAGE）的噻吩 - 偶氮染料，其中R1，R2，R3，R4，R5，X和Y各自具有定义的含义，以及一种或多种吸收最大值为波长为390-520nm，噻吩 - 偶氮染料的比例为60-99重量％，基于噻吩 - 偶氮染料和染料F在混合物中的总重量。

23. 发明授权

US4751288A Azo dyes containing 2-amino-3-cyano-5-formylthiophene derivatives as diazo components and substituted aniline compounds as coupling components 失效
标题翻译：含有2-氨基-3-氰基-5-甲酰基噻吩衍生物作为重氮组分的偶氮染料和取代的苯胺化合物作为偶联组分
公开(公告)号：US4751288A
公开(公告)日：1988-06-14
申请号：US843397
申请日：1986-03-24
申请人： Udo Bergmann , Erwin Hahn , Guenter Hansen , Helmut Reichelt
发明人： Udo Bergmann , Erwin Hahn , Guenter Hansen , Helmut Reichelt
IPC分类号： C09B29/09 , C09B29/00 , C09B29/033 , C09B29/08 , D06P1/18 , D06P3/54
CPC分类号： C09B29/0809 , C09B29/0059 , C09B29/0808 , Y10S534/02
摘要： The compounds of the formula I ##STR1## where R is unsubstituted or substituted phenyl or naphthyl, R.sup.1 and R.sup.2 are each unsubstituted or substituted alkyl, alkenyl or cycloalkyl, and one of the radicals may furthermore be hydrogen, R.sup.3 is hydrogen, methyl, methoxy, ethoxy or chlorine, and R.sup.4 is acylamino, are particularly useful for dyeing polyesters.
摘要翻译：其中R是未取代或取代的苯基或萘基，R 1和R 2各自为未取代或取代的烷基，链烯基或环烷基，并且其中一个基团可以是氢，R 3是氢，甲基，甲氧基，乙氧基或氯，R4为酰氨基，特别适用于染色聚酯。

24. 发明授权

US4213900A Spray-drying method for the preparation of water-dispersible pulverulent disperse dye formulations 失效
标题翻译：用于制备水分散性粉末分散染料配方的喷雾干燥方法
公开(公告)号：US4213900A
公开(公告)日：1980-07-22
申请号：US925527
申请日：1978-07-17
申请人： Ewald Daubach , Dieter Horn , Erwin Hahn , Herbert Uhrig
发明人： Ewald Daubach , Dieter Horn , Erwin Hahn , Herbert Uhrig
IPC分类号： C09B67/20 , C09B67/06 , C09B67/38 , D06P1/16 , C09B5/24 , C09B6/00 , C09B46/00
CPC分类号： C09B67/0003 , C09B67/008 , D06P1/16 , Y10S534/01
摘要： Easily water-dispersible pulverulent formulations of disperse dyes are prepared by spray-drying a dye solution which comprises(a) one or more disperse dyes,(b) one or more water-soluble anionic dispersants,(c) from 0 to 20% by weight, based on (a+b+c+d), of other surfactants and(d) from 0 to 20% by weight, based on (a+b+c+d) of agents which serve as protective colloids (the proportion of (c+d) being at most 20% by weight).Suitable solvents (e) are formic acid, formamide, N-methylformamide, butyrolactone, ethylene glycol and propylene glycol, which may in addition contain up to 100% by weight, based on (e), of N,N-dimethylformamide or acetic acid or mixtures of these. The formulations obtained by the above process contain the dye in very fine dispersion.
摘要翻译：通过喷雾干燥染料溶液来制备分散染料的易水分散性粉剂，其包含（a）一种或多种分散染料，（b）一种或多种水溶性阴离子分散剂，（c）0-20％基于（a + b + c + d）的其他表面活性剂和（d）0至20重量％，基于（a + b + c + d）作为保护胶体的试剂（比例（c + d）为20重量％以下）。合适的溶剂（e）是甲酸，甲酰胺，N-甲基甲酰胺，丁内酯，乙二醇和丙二醇，其还可以含有至多100重量％（e）的N，N-二甲基甲酰胺或乙酸或这些的混合物。通过上述方法获得的制剂含有非常细的分散体中的染料。

25. 发明授权

US5421990A Production of shining shaped articles coated with zinc or a zinc alloy 失效
标题翻译：生产镀锌或锌合金的发光成型制品
公开(公告)号：US5421990A
公开(公告)日：1995-06-06
申请号：US140178
申请日：1993-11-09
申请人： Erwin Hahn , Bernhard Dung , Bernd Burkhart , Chung-Ji Tschang
发明人： Erwin Hahn , Bernhard Dung , Bernd Burkhart , Chung-Ji Tschang
IPC分类号： C25D3/22 , C25D3/56
CPC分类号： C25D3/22
摘要： The production of shining shaped articles coated with zinc or a zinc alloy by electrodeposition of zinc or a zinc alloy from acidic aqueous electrolytic baths which contain as essential components one or more zinc salts and, where appropriate, salts of the other alloy metals, one or more conducting salts, one or more surfactants and one or more brighteners, entails employing as brighteners compounds of the formula I ##STR1## where R.sup.1 is C.sub.1 -C.sub.8 -alkoxy, phenoxy, benzyloxy, amino, C.sub.1 -C.sub.6 -alkylamino or di(C.sub.1 -C.sub.6)alkylamino,R.sup.2 is C.sub.1 -C.sub.4 -alkyl, phenyl, benzyl or the meanings of R.sup.1, andAr is phenyl or naphthyl which can additionally be substituted by one to three C.sub.1 -C.sub.4 -alkyl groups or C.sub.1 -C.sub.4 -alkoxy groups.
摘要翻译： PCT No.PCT / EP92 / 00983第 371日期：1993年11月9日 102（e）日期1993年11月9日PCT提交1992年5月6日PCT公布。公开号WO92 / 22683 日期为1992年12月23日。通过从酸性水溶液电解浴中电镀锌或锌合金制成涂有锌或锌合金的闪亮成形制品，其中含有一种或多种锌盐和适当的盐，其他合金金属，一种或多种导电盐，一种或多种表面活性剂和一种或多种增白剂，需要使用式I的增白剂化合物，其中R 1是C 1 -C 8 - 烷氧基，苯氧基，苄氧基，氨基，C 1 C 1-6 - 烷基氨基或二（C 1 -C 6）烷基氨基，R 2是C 1 -C 4烷基，苯基，苄基或R 1的含义，Ar是苯基或萘基，其可另外被一至三个C 1 -C 4烷基基团或C 1 -C 4 - 烷氧基。

26. 发明授权

US5410053A Rhodamine derivatives 失效
标题翻译：罗丹明衍生物
公开(公告)号：US5410053A
公开(公告)日：1995-04-25
申请号：US213596
申请日：1994-03-16
申请人： Erwin Hahn , Claudia Kraeh , Udo Mayer , Bernhard Albert , Walter Denzinger
发明人： Erwin Hahn , Claudia Kraeh , Udo Mayer , Bernhard Albert , Walter Denzinger
IPC分类号： C09B11/28 , C08K5/18 , C09B11/24 , C09D11/00 , D06P3/76 , G03G9/09 , C07D221/18 , C07D311/88 , D06P3/52 , D06P3/70
CPC分类号： C09D11/50 , C08K5/18 , C09B11/24 , D06P3/76 , G03G9/0914
摘要： There are described rhodamine derivatives of the formula ##STR1## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are each hydrogen or substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl, or R.sup.2 is paired off with R.sup.5 or R.sup.4 with R.sup.6 to form 1,3-propylene, which can be substituted,R.sup.5, R.sup.6, R.sup.7 and R.sup.8 are each hydrogen or methyl,R.sup.9 is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl or a radical of the formula (C.sub.2 H.sub.4 O--).sub.n H, where n is 2 or 3, andAn.sup..crclbar. is the equivalent of an anion derived from an addition or condensation polymer that contains acid groups, novel cyclic rhodamine dyes, and the use of the novel rhodamine derivatives and cyclic rhodamine dyes for dyeing polyacrylonitrile fibers, for incorporation into polymers or for preparing inks.
摘要翻译：描述了具有式“IMAGE”的罗丹明衍生物，其中R 1，R 2，R 3和R 4各自为氢或取代或未取代的C 1 -C 4 - 烷基，或R 2与R 5或R 4与R 6配对形成1,3-丙烯其可以被取代，R5，R6，R7和R8各自为氢或甲基，R9为氢，取代或未取代的C1-C4-烷基或式（C2H4O-）nH基，其中n为2或3，以及 An（ - ）相当于衍生自含有酸基的加成或缩合聚合物的阴离子，新型环状罗丹明染料，以及使用新型罗丹明衍生物和环状罗丹明染料染色聚丙烯腈纤维，用于掺入聚合物或用于准备油墨。

27. 发明授权

US5393828A Chemical degradation of cured amino resins 失效
标题翻译：固化的氨基树脂的化学降解
公开(公告)号：US5393828A
公开(公告)日：1995-02-28
申请号：US163715
申请日：1993-12-09
申请人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
发明人： Juergen Weiser , Wolfgang Reuther , Erwin Hahn
IPC分类号： C08J11/28 , C08G63/91
CPC分类号： C08J11/28 , C08J2361/20 , Y02W30/706
摘要： A process for chemically degrading cured amino resins comprises reacting cured amino resins, which may contain fillers, with a primary and/or secondary amine at from 40.degree. to 250.degree. C.
摘要翻译：化学降解固化的氨基树脂的方法包括将可含有填料的固化的氨基树脂与40℃至250℃的伯胺和/或仲胺反应。

28. 发明授权

US5332830A Preparation of N-hydroxyazoles 失效
标题翻译： N-羟基唑的制备
公开(公告)号：US5332830A
公开(公告)日：1994-07-26
申请号：US37910
申请日：1993-03-26
申请人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
发明人： Klaus H. von Locquenghien , Wolfgang Hoelderich , Ulf Baus , Wolfgang Reuther , Erwin Hahn
IPC分类号： C07D231/12 , C07D233/54 , C07D249/08 , C07D521/00 , C07D233/56
CPC分类号： C07D231/12 , C07D233/56 , C07D249/08
摘要： N-Hydroxyazoles of the general formula I ##STR1## where A is ##STR2## and R.sup.1, R.sup.2 and R.sup.3 are each hydrogen, C.sub.1 -C.sub.4 -alkyl or halogen, are prepared by a process in which an azole of the general formula II ##STR3## where A, R.sup.1, R.sup.2 and R.sup.3 have the abovementioned meanings, is reacted with hydrogen peroxide or an alkyl peroxide in the presence of a zeolite catalyst at from -20.degree. to 150.degree. C. and from 0.1 to 150 bar.
摘要翻译：通式Ⅰ的N-羟基唑（I）其中A是，并且R 1，R 2和R 3各自是氢，C 1 -C 4 - 烷基或卤素，其通过以下方法制备：其中唑其中A，R 1，R 2和R 3具有上述含义的通式II的化合物在沸石催化剂存在下，在-20℃至150℃下与过氧化氢或烷基过氧化物反应。和0.1至150巴。

29. 发明授权

US5306815A Azo dyes with a coupling component of the quinoline series 失效
标题翻译：具有喹啉系偶合成分的偶氮染料
公开(公告)号：US5306815A
公开(公告)日：1994-04-26
申请号：US947533
申请日：1992-09-21
申请人： Erwin Hahn , Clemens Grund , Andreas Geisberger , Helmut Reichelt , Andreas Guldner , Mathias Wiesenfeldt , Karl-Heinz Etzbach , Ruediger Sens , Helmut Hagen
发明人： Erwin Hahn , Clemens Grund , Andreas Geisberger , Helmut Reichelt , Andreas Guldner , Mathias Wiesenfeldt , Karl-Heinz Etzbach , Ruediger Sens , Helmut Hagen
IPC分类号： C09B29/033 , C09B29/00 , C09B29/042 , C09B29/045 , C09B29/44 , D06P1/18
CPC分类号： C09B29/0059 , C09B29/0074 , C09B29/3643
摘要： Azo dyes useful for dyeing or printing textile fibers or fabrics and for thermal transfer have the formula ##STR1## where R.sup.1 and R.sup.2 are each substituted or unsubstituted C.sub.1 -C.sub.10 -alkyl or substituted or unsubstituted C.sub.3 -C.sub.4 -alkenyl or R.sup.1 may also be hydrogen,R.sup.3 is hydrogen or C.sub.1 -C.sub.6 -alkyl,R.sup.4 and R.sup.5 are each hydrogen, C.sub.1 -C.sub.6 -alkyl, halogen, C.sub.1 -C.sub.6 -alkoxy, amino or mono- or di(C.sub.1 -C.sub.4 -alkyl)amino, andD is a radical of the thiophene, thiazole, isothiazole, benzothiophene, thienothiophene or thienothiazole series.
摘要翻译：可用于染色或印刷纺织纤维或织物和热转印的偶氮染料具有式（*化学结构*），其中R 1和R 2各自为取代或未取代的C 1 -C 10 - 烷基或取代或未取代的C 3 -C 4 - 烯基或R 1可以也可以是氢，R 3是氢或C 1 -C 6烷基，R 4和R 5各自是氢，C 1 -C 6烷基，卤素，C 1 -C 6烷氧基，氨基或单或二（C 1 -C 4烷基）氨基， D是噻吩，噻唑，异噻唑，苯并噻吩，噻吩并噻吩或噻吩并噻唑系的基团。

30. 发明授权

US5286401A Use of heterocyclic compounds as bleach activators or optical brighteners in washing and cleaning agents 失效
标题翻译：在洗涤剂和清洁剂中使用杂环化合物作为漂白活化剂或荧光增白剂
公开(公告)号：US5286401A
公开(公告)日：1994-02-15
申请号：US836279
申请日：1992-03-03
申请人： Bernhard Dung , Wolfgang Trieselt , Erwin Hahn , Johannes Perner , Alfred Oftring
发明人： Bernhard Dung , Wolfgang Trieselt , Erwin Hahn , Johannes Perner , Alfred Oftring
IPC分类号： C11D3/28 , C07D265/22 , C11D3/39 , C11D3/42 , C11D3/395 , D06L3/02 , D06L3/12
CPC分类号： C07D265/22 , C11D3/392 , C11D3/42
摘要： Heterocyclic compounds which are useful as bleach activators or optical brighteners in washing and cleaning agents have the formula ##STR1## where the variables have the following meanings: X is O, S or the group N--R.sup.3, where R.sup.3 is hydrogen, C.sub.1 -C.sub.25 -alkyll C.sub.1 -C.sub.25 -acyl or an aryl group of up to12 carbon atoms,Y is CH or N,R.sup.1 for X=S or N--R.sup.3 is hydrogen, a C.sub.1 -C.sub.25 -alkyl or C.sub.2 -C.sub.25 -alkenyl group or a phenyl radical which may be additionally substituted by one or two C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, hydroxyl, carboxyl, sulfo, amino, C.sub.1 -C.sub.4 -acylamino, nitro or cyano groups or chlorine or bromine atoms, which substituents, if there are two of them, may be identical or different,R.sup.1 for X=O is phenyl, o-, m- or p-tolyl, p-chlorophenyl, m-nitrophenyl, m-methoxyphenyl or m-methylsulfonylphenyl,R.sup.2 for X=S or N--R.sup.3 is hydrogen, a C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, hydroxyl, carboxyl, sulfo, amino or C.sub.1 -C.sub.4 -acylamino group or a chlorine or bromine atom, andR.sup.2 for X=O is hydrogen.
摘要翻译：式（I）的杂环化合物，其中X代表O，S或NR 3基团，其中R 3代表氢，C 1 -C 25烷基，C 1 -C 25酰基或芳基，最多12个碳原子，Y代表CH或N，R 1代表X = S或NR 3，氢，C 1 -C 25烷基或C 2 -C 25烯基或苯基残基，其可以另外被一个或多个两个C 1 -C 4烷基，C 1 -C 4烷氧基，羟基，羧基，磺基，氨基，C 1 -C 4酰基氨基，硝基或氰基或氯或溴原子，其中两个取代基可以相同或不同，R 1，代表X = O，苯基，邻 - ，对 - 或对甲苯基，对氯苯基，间硝基苯基，间甲氧基苯基或间甲基磺酰基苯基，R 2代表X = S或NR 3，氢，C 1 -C 4烷基，C 1 -C 4烷氧基，羟基，羧基，磺基，氨基或C 1 -C 4酰氨基或氯或溴原子，R 2代表X = O或氢，可用作漂白活化剂或洗涤剂和清洁剂中的光学增亮剂。

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