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11. 发明授权

US09573127B2 Process for producing shaped catalyst and process for producing diene or unsaturated aldehyde and/or unsaturated carboxylic acid using the shaped catalyst 有权
标题翻译：用于生产成形催化剂的方法和使用成型催化剂生产二烯或不饱和醛和/或不饱和羧酸的方法
公开(公告)号：US09573127B2
公开(公告)日：2017-02-21
申请号：US14396478
申请日：2013-04-19
申请人： NipponKayaku KabushikiKaisha
发明人： Ryota Hiraoka , Yumi Hino , Kimito Okumura , Motohiko Sugiyama , Hiroki Motomura
IPC分类号： B01J23/887 , B01J35/02 , B01J37/02 , C07C45/35 , C07C51/25 , C07C5/48 , B01J23/88 , B01J37/03 , B01J37/00
CPC分类号： B01J37/0223 , B01J23/88 , B01J23/8876 , B01J35/026 , B01J37/0045 , B01J37/038 , B01J2523/00 , C07C5/48 , C07C45/35 , C07C51/252 , C07C2523/04 , C07C2523/28 , C07C2523/745 , C07C2523/75 , C07C2523/755 , C07C2523/88 , C07C2523/883 , C07C2523/887 , Y02P20/52 , C07C11/167 , B01J2523/13 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/847 , B01J2523/15 , C07C57/04
摘要： There is provided a process for producing a shaped catalyst for a fixed bed oxidation reaction or a fixed bed oxidative dehydrogenation reaction, the catalyst having both of sufficient mechanical strength and catalyst performance, and the catalyst is produced by supporting a catalyst powder containing a complex metal oxide having molybdenum as an essential ingredient on an inert support by a tumbling granulation method at a relative centrifugal force of 1 to 35 G.
摘要翻译：提供了一种用于固定床氧化反应或固定床氧化脱氢反应的成型催化剂的制备方法，该催化剂具有足够的机械强度和催化剂性能，并且催化剂通过负载含有复合金属的催化剂粉末氧化物，以1〜35G的相对离心力，通过滚筒造粒法在惰性载体上具有钼作为必需成分。

12. 发明申请

US20160279618A1 METAL OXIDE CATALYST MATERIAL AND PROCESSES FOR MAKING AND USING SAME 有权
标题翻译：金属氧化物催化剂材料和制备和使用它们的方法
公开(公告)号：US20160279618A1
公开(公告)日：2016-09-29
申请号：US15061033
申请日：2016-03-04
申请人： CLARIANT CORPORATION
发明人： Claus G. Lugmair , Hailian Li
IPC分类号： B01J23/889 , C07C45/35 , B01J23/00 , C07C253/26 , B01J35/02 , B01J35/00
CPC分类号： B01J23/8898 , B01J23/002 , B01J23/8876 , B01J35/0013 , B01J35/023 , B01J37/0045 , B01J37/0081 , B01J37/03 , B01J37/08 , B01J2523/00 , C07C45/35 , C07C253/26 , Y02P20/52 , C07C255/08 , B01J2523/13 , B01J2523/15 , B01J2523/22 , B01J2523/3712 , B01J2523/41 , B01J2523/54 , B01J2523/67 , B01J2523/68 , B01J2523/72 , B01J2523/842 , B01J2523/845 , C07C253/28
摘要： The present disclosure relates to metal oxide catalyst materials useful, for example, in the ammoxidation of propylene or isobutylene, processes for making them, and processes for making acrylonitrile and methacrylonitrile using such catalyst materials. In certain aspects, a catalyst material is a fused composite of a metal oxide catalyst and nanoparticulate silica, the nanoparticulate silica comprising in the range of about 40 wt % to about 80 wt % of silica having a particle size in the range of 10 nm to 35 nm, and in the range of about 20 wt % to about 60 wt % of silica having a particle size in the range of 36 nm to 80 nm. The metal oxide catalyst can be, for example, a molybdenum-containing mixed metal oxide catalyst.
摘要翻译：本公开内容涉及可用于例如丙烯或异丁烯的氨氧化的金属氧化物催化剂材料，其制备方法，以及使用这种催化剂材料制备丙烯腈和甲基丙烯腈的方法。在某些方面，催化剂材料是金属氧化物催化剂和纳米颗粒二氧化硅的熔融复合物，所述纳米颗粒二氧化硅在约40重量％至约80重量％的范围内，所述二氧化硅的粒径在10nm至 35nm，在约20wt％至约60wt％范围内的二氧化硅粒径在36nm至80nm的范围内。金属氧化物催化剂可以是例如含钼混合金属氧化物催化剂。

13. 发明申请

US20160059220A1 Catalyst For Producing Unsaturated Aldehyde And/or Unsaturated Carboxylic Acid, Method For Producing The Catalyst, And Method For Producing Unsaturated Aldehyde and/or Unsaturated Carboxylic Acid Using The Catalyst 有权
标题翻译：用于生产不饱和醛和/或不饱和羧酸的催化剂，用于生产催化剂的方法，以及使用催化剂生产不饱和醛和/或不饱和羧酸的方法
公开(公告)号：US20160059220A1
公开(公告)日：2016-03-03
申请号：US14785714
申请日：2014-04-15
申请人： NIPPONKAYAKU KABUSHIKIKAISHA
发明人： Toru Kawaguchi , Yoshiko Shoya , Asa Taniguchi , Masashi Hashiba , Hideo Yoshida
IPC分类号： B01J23/89 , C07C51/25 , C07C45/35 , B01J23/00 , B01J35/02
CPC分类号： B01J23/8993 , B01J21/08 , B01J23/002 , B01J23/8876 , B01J35/023 , B01J37/0018 , B01J37/0238 , B01J37/04 , B01J37/08 , B01J37/088 , B01J2523/00 , C07C45/35 , C07C51/215 , C07C51/252 , C07C57/04 , C07C47/22 , B01J2523/13 , B01J2523/54 , B01J2523/68 , B01J2523/842 , B01J2523/845 , B01J2523/847
摘要： An object of the invention is to provide a novel catalyst having high mechanical strength and capable of obtaining an unsaturated aldehyde or an unsaturated carboxylic acid in a high yield and a method for producing the same, and a method for producing an unsaturated aldehyde and/or an unsaturated carboxylic acid using the catalyst.By containing silane-treated glass fibers in a catalytic active component composed of molybdenum and bismuth as essential components, high mechanical strength is revealed, and it is possible to obtain an unsaturated aldehyde or an unsaturated carboxylic acid in a high yield.
摘要翻译：本发明的目的是提供一种具有高机械强度且能够以高收率获得不饱和醛或不饱和羧酸的新型催化剂及其制备方法，以及制备不饱和醛和/或使用该催化剂的不饱和羧酸。通过将由钼和铋组成的催化活性组分中的硅烷处理的玻璃纤维作为主要组分，显示出高的机械强度，并且可以高产率获得不饱和醛或不饱和羧酸。

14. 发明申请

US20160052853A1 PLATE-TYPE REACTOR WITH IN-SITU INJECTION 有权
标题翻译：具有现场注射的板式反应器
公开(公告)号：US20160052853A1
公开(公告)日：2016-02-25
申请号：US14931445
申请日：2015-11-03
申请人： ARKEMA FRANCE
发明人： Jean-Luc DUBOIS
IPC分类号： C07C45/51 , C07C45/29 , C07C45/35 , C07D307/89 , C07D307/60 , C07C51/347 , C07C41/01
CPC分类号： C07C45/512 , B01J19/249 , B01J2219/2453 , B01J2219/2455 , B01J2219/2459 , B01J2219/246 , B01J2219/2462 , B01J2219/247 , B01J2219/2481 , C07C41/01 , C07C45/29 , C07C45/35 , C07C51/347 , C07D307/60 , C07D307/89 , F28D9/0043 , F28D2021/0022 , F28F9/027
摘要： A chemical reactor including: a plurality of heat exchange plates which between them define reaction compartments, in which reactor each heat exchange plate includes two walls between them defining at least one heat exchange space, the respective walls being fixed together by joining regions, and the reactor also comprises at least one injection device for injecting substance into the reaction compartments, said substance-injection device passing through the heat-exchange plates in respective joining regions thereof. Also, a chemical reaction process that can be carried out in this reactor.
摘要翻译：一种化学反应器，包括：多个热交换板，它们之间限定反应隔室，其中反应器每个热交换板包括它们之间的两个壁，其间限定至少一个热交换空间，各个壁通过连接区域固定在一起，反应器还包括至少一个用于将物质注入到反应室中的注射装置，所述物质注射装置在其各自的接合区域中通过热交换板。另外，可以在该反应器中进行的化学反应过程。

15. 发明申请

US20160051967A1 METHOD FOR PRODUCING A CATALYST FOR THE PARTIAL OXIDATION/AMMOXIDATION OF OLEFINS 审中-公开
标题翻译：生产烯烃部分氧化/脱氧催化剂的方法
公开(公告)号：US20160051967A1
公开(公告)日：2016-02-25
申请号：US14782878
申请日：2014-04-11
申请人： CLARIANT CORPORATION
发明人： Valery Sokolovskii , David Michael Lowe , Deepti Machiraju , Hongyi C. Hou , Gerhard Mestl , Claus G. Lugmair , Aaron B. Miller , Anthony F. Volpe, JR.
IPC分类号： B01J23/888 , B01J37/02 , C07C253/26 , B01J35/10 , C07C45/35 , B01J23/00 , B01J37/08
CPC分类号： B01J23/8885 , B01J21/08 , B01J23/002 , B01J23/8872 , B01J35/1009 , B01J35/1014 , B01J35/1019 , B01J37/0201 , B01J37/0215 , B01J37/08 , B01J2523/00 , C07C45/35 , C07C253/26 , Y02P20/52 , B01J2523/13 , B01J2523/22 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , B01J2523/847 , C07C255/08 , C07C47/22
摘要： The present invention relates to a method for producing a supported catalyst, a catalyst which is obtainable using the method, and use thereof for the partial oxidation or ammoxidation of olefins, in particular for the oxidation of propene to acrolein, of isobutene to methacrolein, and/or the ammoxidation of propene to acrylonitrile. The method according to the invention includes the following steps: a) providing a solution in which precursor compounds of the catalytically active component are essentially completely dissolved in a suitable solvent; b) bringing the solution obtained in step a) into contact with a (chemically) inert, porous support having a specific surface of 1 to 500 m2/g; c) heat treatment of the material obtained in step b), in which the precursor compounds of the catalytically active component are converted to their oxides.
摘要翻译：本发明涉及负载型催化剂的制造方法，使用该方法得到的催化剂及其用于将烯烃部分氧化或氨氧化成烯烃，特别是将丙烯氧化为丙烯醛的异丁烯与甲基丙烯醛的用途，以及 /或丙烯对丙烯腈的氨氧化。根据本发明的方法包括以下步骤：a）提供其中催化活性组分的前体化合物基本上完全溶解在合适溶剂中的溶液; b）将步骤a）中获得的溶液与具有1至500m 2 / g比表面积的（化学）惰性多孔载体接触; c）对步骤b）中获得的材料进行热处理，其中将催化活性组分的前体化合物转化为其氧化物。

16. 发明授权

US09108904B2 Process for converting a hydrocarbon to an oxygenate or a nitrile 有权
标题翻译：将烃转化为含氧化合物或腈的方法
公开(公告)号：US09108904B2
公开(公告)日：2015-08-18
申请号：US11836811
申请日：2007-08-10
申请人： John H. Brophy , Frederick A. Pesa , Anna Lee Tonkovich , Jeffrey S. McDaniel , Kai Tod Paul Jarosch
发明人： John H. Brophy , Frederick A. Pesa , Anna Lee Tonkovich , Jeffrey S. McDaniel , Kai Tod Paul Jarosch
IPC分类号： B01J19/00 , C07C253/26 , C07B41/00 , C07B43/08 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C51/25 , C07C51/265 , C07C67/05 , C07C253/24
CPC分类号： C07C253/26 , B01J19/0093 , B01J2219/00783 , B01J2219/00804 , B01J2219/00835 , B01J2219/0086 , B01J2219/00873 , C07B41/00 , C07B43/08 , C07C45/33 , C07C45/34 , C07C45/35 , C07C45/36 , C07C51/252 , C07C51/265 , C07C67/05 , C07C253/24 , C07C47/22 , C07C57/04 , C07C63/16 , C07C69/01 , C07C255/08 , C07C69/15 , C07C69/155
摘要： This invention relates to a process for converting a hydrocarbon reactant to a product comprising an oxygenate or a nitrile, the process comprising: (A) flowing a reactant composition comprising the hydrocarbon reactant, and oxygen or a source of oxygen, and optionally ammonia, through a microchannel reactor in contact with a catalyst to convert the hydrocarbon reactant to the product, the hydrocarbon reactant undergoing an exothermic reaction in the microchannel reactor; (B) transferring heat from the microchannel reactor to a heat exchanger during step (A); and (C) quenching the product from step (A).
摘要翻译：本发明涉及一种将烃反应物转化为含有氧化合物或腈的产物的方法，该方法包括：（A）使包含烃反应物的反应物组合物和氧气或氧源和任选的氨通过与催化剂接触以将烃反应物转化成产物的微通道反应器，在微通道反应器中经历放热反应的烃反应物; （B）在步骤（A）期间将热量从微通道反应器传递到热交换器; 和（C）淬灭步骤（A）的产物。

17. 发明申请

US20150133686A1 MECHANICALLY STABLE HOLLOW CYLINDRICAL SHAPED CATALYST BODIES FOR GAS PHASE OXIDATION OF AN ALKENE TO AN UNSATURATED ALDEHYDE AND/OR AN UNSATURATED CARBOXYLIC ACID 有权
标题翻译：机械稳定的中空圆柱形催化剂体，用于气相氧化为不饱和醛和/或不饱和羧酸的碱
公开(公告)号：US20150133686A1
公开(公告)日：2015-05-14
申请号：US14535743
申请日：2014-11-07
申请人： BASF SE
发明人： Josef Macht , Christian Walsdorff , Cornelia Katharina Dobner , Stefan Lipp , Cathrin Alexandra Welker-Nieuwoudt , Ulrich Hammon , Holger Borchert
IPC分类号： B01J23/888 , C07C45/35 , C07C51/25 , B01J35/04
CPC分类号： B01J23/8885 , B01J23/002 , B01J23/8876 , B01J35/0006 , B01J35/0026 , B01J35/023 , B01J35/026 , B01J35/04 , B01J37/0009 , B01J37/0045 , B01J37/04 , B01J37/08 , B01J2523/00 , C01G49/0036 , C01G51/00 , C01G53/00 , C01P2002/72 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C04B35/495 , C04B35/6261 , C04B35/62655 , C04B35/62675 , C04B35/62685 , C04B35/64 , C04B2235/3201 , C04B2235/3256 , C04B2235/326 , C04B2235/3275 , C04B2235/3298 , C04B2235/44 , C04B2235/443 , C04B2235/5409 , C04B2235/5427 , C04B2235/5436 , C04B2235/5445 , C04B2235/604 , C04B2235/608 , C04B2235/656 , C04B2235/72 , C04B2235/95 , C07C45/35 , C07C51/252 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , C07C47/22 , C07C57/04
摘要： A hollow cylindrical shaped catalyst body for gas phase oxidation of an alkene to an α,β-unsaturated aldehyde and/or an α,β-unsaturated carboxylic acid comprises a compacted multimetal oxide having an external diameter ED, an internal diameter ID and a height H, wherein ED is in the range from 3.5 to 4.5 mm; the ratio q=ID/ED is in the range from 0.4 to 0.55; and the ratio p=H/ED is in the range from 0.5 to 1. The shaped catalyst body is mechanically stable and catalyzes the partial oxidation of an alkene to the products of value with high selectivity. It provides a sufficiently high catalyst mass density of the catalyst bed and good long-term stability with acceptable pressure drop.
摘要翻译：用于将烯烃气相氧化成α，β-不饱和醛和/或α，β-不饱和羧酸的中空圆柱形催化剂体包括具有外径ED，内径ID的压实多金属氧化物，和高度H，其中ED在3.5至4.5mm的范围内; 比值q = ID / ED在0.4至0.55的范围内; 并且比例p = H / ED在0.5至1的范围内。成形的催化剂体是机械稳定的并且以高选择性催化烯烃部分氧化成价值的产物。它提供催化剂床的足够高的催化剂质量密度，并具有良好的长期稳定性和可接受的压降。

18. 发明授权

US08962881B2 Oxidized organic compound manufacturing method 有权
标题翻译：氧化有机化合物的制造方法
公开(公告)号：US08962881B2
公开(公告)日：2015-02-24
申请号：US13203311
申请日：2009-03-09
申请人： Michio Tanimoto , Nobuyuki Hakozaki
发明人： Michio Tanimoto , Nobuyuki Hakozaki
IPC分类号： C07C45/35 , C07C47/22 , C07C51/235 , C07C51/25 , C07C57/05 , C07C57/055
CPC分类号： C07C51/235
摘要： The disclosed invention is a method for manufacturing an oxidized organic compound which includes a step of forming an oxidized organic compound, in use of a fixed-bed reactor having a reaction tube packed with an oxide catalyst, by supplying at least one type of organic compound as a reaction feedstock gas and using a molecular oxygen-containing gas to carry out a catalytic gas-phase oxidation reaction; and a step of stopping the catalytic gas-phase oxidation reaction. In the manufacturing method, when stopping the catalytic gas-phase oxidation reaction, the supply of the reaction feedstock gas is stopped, after which an inert gas is supplied to the reactor, then a molecular oxygen-containing gas is supplied, subsequent to which the supply of the molecular oxygen-containing gas to the reactor is stopped.
摘要翻译：所公开的发明是一种氧化有机化合物的制造方法，其包括形成氧化有机化合物的步骤，在使用具有填充有氧化物催化剂的反应管的固定床反应器的情况下，通过供给至少一种类型的有机化合物作为反应原料气体并使用含分子氧的气体进行催化气相氧化反应; 以及停止催化气相氧化反应的步骤。在制造方法中，停止催化气相氧化反应时，停止供给反应原料气体，之后向反应器供给惰性气体，然后供给含分子氧气体，接着，停止向反应器供应含分子氧的气体。

19. 发明申请

US20140296558A1 PROCESS FOR PRODUCING GEOMETRIC SHAPED CATALYST BODIES 审中-公开
标题翻译：生产几何形状催化剂体的方法
公开(公告)号：US20140296558A1
公开(公告)日：2014-10-02
申请号：US14305548
申请日：2014-06-16
申请人： BASF SE
发明人： Andreas RAICHLE , Catharina Horstmann , Frank Rosowski , Klaus Joachim Mueller-Engel , Holger Borchert , Gerhard Cox , Ulrich Cremer
IPC分类号： C07C253/26 , C07C45/35 , B01J23/888
CPC分类号： C07C45/28 , B01J23/002 , B01J23/8885 , B01J35/0006 , B01J35/023 , B01J37/0036 , B01J37/0221 , B01J37/04 , B01J2523/00 , C07C45/35 , C07C45/37 , C07C51/252 , C07C253/26 , Y02P20/52 , C07C47/22 , C07C57/04 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845 , C07C255/08
摘要： A process for producing geometric shaped catalyst bodies K whose active material is a multielement oxide of stoichiometry [Bi1WbOx]a[Mo12Z1cZ2dFeeZ3fZ4gZ5hOy]1, in which a finely divided oxide Bi1WbOx with the particle size d50A1 and, formed from element sources, a finely divided intimate mixture of stoichiometry Mo12Z1cZ2dFeeZ3fZ4gZ5h with the particle size d90A2 are mixed in a ratio of a:1, this mixture is used to form shaped bodies and these are treated thermally, where (d50A1)0.7·(d90A2)1.5·(a)−1≧820. A shaped catalyst body obtained by the process. A catalyst obtained by grinding the shaped catalyst body. A process for heterogeneously catalyzing the partial gas phase oxidation of an alkane, alkanol, alkanal and/or an alkenal of 3 to 6 carbon atoms using the catalyst.
摘要翻译：一种生产几何形状的催化剂体K的方法，其活性材料是化学计量[Bi1WbOx] a [Mo12Z1cZ2dFeeZ3fZ4gZ5hOy] 1的多元素氧化物，其中粒径为d50A1的细分的氧化物Bi1WbOx由元素源形成，化学计量比的混合物Mo12Z1cZ2dFeeZ3fZ4gZ5h与粒径d90A2的混合比例为：1，该混合物用于形成成型体，热处理，其中（d50A1）0.7·（d90A2）1.5·（a）-1≧ 820。通过该方法获得的成型催化剂体。通过研磨成形催化剂体获得的催化剂。使用该催化剂非均相催化烷烃，链烷醇，链烷烃和/或具有3至6个碳原子的烯烃的部分气相氧化的方法。

20. 发明申请

US20140046093A1 PROCESS FOR CHARGING A LONGITUDINAL SECTION OF A CATALYST TUBE 审中-公开
标题翻译：用于对催化管长期充电的方法
公开(公告)号：US20140046093A1
公开(公告)日：2014-02-13
申请号：US14060406
申请日：2013-10-22
申请人： BASF SE
发明人： Martin DIETERLE , Klaus Joachim MUELLER-ENGEL
IPC分类号： B01J8/06 , C07C51/25 , C07C45/35
CPC分类号： B01J8/06 , B01J8/0015 , B01J8/067 , B01J19/30 , B01J23/002 , B01J23/28 , B01J23/50 , B01J23/8876 , B01J23/8885 , B01J27/198 , B01J35/0006 , B01J35/023 , B01J35/08 , B01J37/0009 , B01J2208/00752 , B01J2208/00805 , B01J2219/30207 , B01J2219/30215 , B01J2219/30416 , B01J2219/30475 , B01J2523/00 , C07C45/35 , C07C51/252 , C07C51/265 , C07C47/22 , C07C57/04 , C07C63/16 , B01J2523/13 , B01J2523/41 , B01J2523/54 , B01J2523/68 , B01J2523/69 , B01J2523/842 , B01J2523/845
摘要： A process for charging a longitudinal section of a catalyst tube with a homogeneous fixed catalyst bed section whose active composition is at least one multielement oxide or comprises elemental silver on an oxidic support body and whose geometric shaped catalyst bodies and shaped inert bodies have a specific inhomogeneity of their longest dimensions.
摘要翻译：一种催化剂管的纵截面的方法，其具有均匀的固定催化剂床部分，其活性组成为至少一种多元素氧化物或在氧化载体上包含元素银，并且其几何形状的催化剂体和成形惰性体具有特定的不均匀性的最长尺寸。

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