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11. 发明授权

US07651970B2 Regeneration of ionic liquid catalyst by hydrogenation using a metal or metal alloy catalyst 有权
标题翻译：使用金属或金属合金催化剂通过氢化再生离子液体催化剂
公开(公告)号：US07651970B2
公开(公告)日：2010-01-26
申请号：US11316107
申请日：2005-12-20
申请人： Saleh Elomari , Thomas V. Harris
发明人： Saleh Elomari , Thomas V. Harris
IPC分类号： B01J20/34 , B01J21/20 , B01J23/90 , B01J25/04 , B01J27/28 , B01J29/90 , B01J38/48 , B01J38/60 , B01J31/00 , B01J31/40 , B01J38/00
CPC分类号： B01J31/0288 , B01J27/125 , B01J27/32 , B01J31/0239 , B01J31/0284 , B01J31/40 , B01J38/10 , B01J2231/4205 , B01J2231/64 , C07C2/861 , Y02P20/584
摘要： A process for regenerating a used acidic ionic liquid catalyst which has, been deactivated comprising the steps of contacting the used chloroaluminate ionic liquid catalyst and hydrogen with a metal hydrogenation catalyst in a reaction zone under hydrogenation conditions for a time sufficient to increase the activity of the ionic liquid catalyst is described. In one embodiment, hydrogenation is conducted in the presence of a hydrocarbon solvent.
摘要翻译：一种使已使用的酸性离子液体催化剂再生的方法，其被去活化，包括以下步骤：在氢化条件下在反应区中使所用的氯铝酸盐离子液体催化剂和氢与金属氢化催化剂接触足够时间以提高活性离子液体催化剂。在一个实施方案中，在烃溶剂的存在下进行氢化。

12. 发明申请

US20090326240A1 Iron-Copper Co-Catalyzed Process for Carbon-Carbon or Carbon-Heteroatom Bonding 有权
标题翻译：用于碳 - 碳或碳 - 杂原子键合的铁 - 铜共催化方法
公开(公告)号：US20090326240A1
公开(公告)日：2009-12-31
申请号：US12308985
申请日：2007-07-04
申请人： Marc Taillefer , Ning Xia , Armelle Ouali
发明人： Marc Taillefer , Ning Xia , Armelle Ouali
IPC分类号： C07D249/04 , C07D231/12 , C07D233/56 , C07D207/00 , C07D249/08 , C07D209/04 , C07C211/43
CPC分类号： C07C41/16 , C07B37/04 , C07B41/04 , C07B43/04 , C07C2/861 , C07C67/343 , C07C249/02 , C07C2523/72 , C07C2531/22 , C07D207/267 , C07D207/323 , C07D209/08 , C07D231/12 , C07D233/54 , C07D233/58 , C07D249/06 , C07D249/08 , C07C15/54 , C07C69/612 , C07C251/24 , C07C43/275 , C07C43/29
摘要： The present invention relates to a process for creating a Carbon-Carbon bond (C—C) or a Carbon-Heteroatom bond (C—HE) by reacting a compound carrying a leaving group with a nucleophilic compound carrying a carbon atom or a heteroatom (HE) that can substitute for the leaving group, creating a C—C or C—HE bond, wherein the reaction takes place in the presence of an effective quantity of a catalytic system comprising iron and copper.
摘要翻译：本发明涉及通过使携带离去基团的化合物与携带碳原子或杂原子（HE）的亲核化合物反应来制备碳 - 碳键（CC）或碳 - 杂原子键（C-HE）的方法，可以代替离去基团，产生CC或C-HE键，其中反应在有效量的包含铁和铜的催化体系的存在下进行。

13. 发明授权

US07504548B2 Method for formulation of synthetic gas oils or additives for gas oil 失效
标题翻译：合成瓦斯油或瓦斯油添加剂的配制方法
公开(公告)号：US07504548B2
公开(公告)日：2009-03-17
申请号：US10943896
申请日：2004-09-20
申请人： Patrick Briot , Sylvie Lacombe , Jean-François Joly , Eric Llido
发明人： Patrick Briot , Sylvie Lacombe , Jean-François Joly , Eric Llido
IPC分类号： C07C2/64 , C10G35/00
CPC分类号： C10L1/08 , C07C2/64 , C07C2/66 , C07C2/861 , C07C5/10 , C07C13/18 , C07C2521/04 , C07C2527/126 , C07C2529/18 , C07C2601/14 , C07C15/107
摘要： The invention relates to a method for formulation of a synthetic gas oil or an additive for gas oil in which an alkyl-aromatic compound or a mixture of alkyl-aromatic compounds is selected based on at least one parameter that is selected from the group that consists of the number of cycles of the aromatic core, the number of alkyl chains that are grafted to the aromatic cycle, the length of the alkyl chain or chains, the position of the aromatic cycle or cycles on the alkyl chain or chains of said alkyl-aromatic compound or compounds such that the cetane number of the synthetic gas oil or the additive for gas oil is greater than 30. The invention also relates to a process for the production of alkyl-aromatic compounds for use as a gas oil or additive.
摘要翻译：本发明涉及一种用于制备瓦斯油的合成瓦斯油或其添加剂的方法，其中烷基芳族化合物或烷基芳族化合物的混合物基于至少一个参数，该参数选自组成的芳族核心的循环次数，接枝到芳香环的烷基链的数量，烷基链或链的长度，芳族环或在所述烷基链或烷基链的烷基链上的循环的位置，芳族化合物或化合物，使得合成瓦斯油的十六烷值或瓦斯油的添加剂大于30.本发明还涉及用作瓦斯油或添加剂的烷基 - 芳族化合物的制备方法。

14. 发明申请

US20050255575A1 Methods of 1,3-enyne preparation using copper (I) catalysts 失效
标题翻译：使用铜（I）催化剂制备1,3-戊烯的方法
公开(公告)号：US20050255575A1
公开(公告)日：2005-11-17
申请号：US11115502
申请日：2005-04-27
申请人： Dhandapani Venkataraman , Craig Bates , Pranorm Saejueng
发明人： Dhandapani Venkataraman , Craig Bates , Pranorm Saejueng
IPC分类号： C07B37/04 , C07C2/86 , C07C67/343 , C07C205/56 , C07C319/20 , C07C323/62 , C07D213/55 , C07D333/16 , C07D333/24 , C12N9/00
CPC分类号： C07C205/56 , B01J31/1805 , B01J31/1815 , B01J31/183 , B01J31/2217 , B01J2231/4266 , B01J2531/16 , C07B37/04 , C07C2/861 , C07C67/343 , C07C201/12 , C07C253/30 , C07C319/20 , C07C2527/167 , C07C2531/24 , C07C2602/10 , C07D213/55 , C07D333/16 , C07D333/24 , C12N9/00 , C07C11/28 , C07C69/65 , C07C69/606 , C07C69/738 , C07C69/76 , C07C69/618 , C07C69/734 , C07C323/62 , C07C255/57
摘要： A copper(I) bi-dentate ligand complex-catalyzed procedure for synthesis of 1,3-enynes. The methods and/or systems of this invention afford a variety of enynes, tolerate a variety of sensitive functional groups, and can be employed without resort to expensive palladium reagents.
摘要翻译：铜（I）双齿配体配合物催化合成1,3-烯炔的方法。本发明的方法和/或系统提供各种烯炔，可耐受各种敏感的官能团，并且可以在不使用昂贵的钯试剂的情况下使用。

15. 发明申请

US20050227863A1 Process for aryl-aryl carbon to carbon bond formation by arylation of aryl halide or an aromatic compound 审中-公开
标题翻译：通过芳基卤化物或芳族化合物的芳基化形成芳基 - 芳基碳与碳键的方法
公开(公告)号：US20050227863A1
公开(公告)日：2005-10-13
申请号：US10814860
申请日：2004-03-31
申请人： Vasant Choudhary , Rani Jha
发明人： Vasant Choudhary , Rani Jha
IPC分类号： B01J21/16 , B01J23/26 , B01J23/83 , B01J27/06 , B01J27/132 , B01J27/187 , B01J29/03 , B01J29/035 , B01J29/70 , B01J29/83 , B01J37/22 , B01J37/24 , C07C2/86
CPC分类号： B01J37/24 , B01J21/16 , B01J23/26 , B01J23/83 , B01J27/132 , B01J29/0308 , B01J29/035 , B01J29/7007 , B01J29/83 , B01J37/22 , C07C2/861 , C07C2523/745 , Y02P20/588 , C07C15/16
摘要： A solid catalyst, consisting of partially halogenated metal oxide or mixed metal oxide or zeolite or zeolite-like solid, represented by a general formula: X(a)/PbMOc(OH)d wherein, X is halogen element selected from F, Cl, Br and I; P is phosphorous element; M is at least one metallic element selected from alkaline earth metals, rare earth metals, group IIIa metals, non-noble transition metals, Sn, Sb, Bi, Si, thorium and uranium; O is oxygen; H is hydrogen; a is the concentration of halogen element X present in the catalyst in the range from 0.01 wt % to 50 wt %; b is the mole ratio of P to M in the range from zero to 1.0; c and d are the number of oxygen and OH groups, respectively, required to satisfy the valence requirement of the metallic and non-metallic elements (M and P); and the ratio of d to c in the range from zero to about 1.0, with or without any catalyst support, useful for the Friedel-Crafts reactions and also its method of preparation are disclosed.
摘要翻译：由以下通式表示的部分卤化金属氧化物或混合金属氧化物或沸石或类似沸石的固体组成的固体催化剂：<？in-line-formula description =“In-Line Formulas”end =“lead”？> α（in）-in-line-formula description =“In-line Formulas”end =“尾”→其中，X是选自F，Cl，Br和I的卤素元素; P是磷元素; M是选自碱土金属，稀土金属，IIIa族金属，非贵金属过渡金属，Sn，Sb，Bi，Si，钍和铀中的至少一种金属元素; O是氧; H是氢; a是催化剂中存在的卤素元素X的浓度在0.01重量％至50重量％的范围内; b是P与M的摩尔比在0至1.0的范围内; c和d分别是满足金属和非金属元素（M和P）的化合价要求所需的氧和OH基数; 并且公开了对于Friedel-Crafts反应可用的有或没有任何催化剂载体的d至c在0至约1.0的范围内的比率，以及其制备方法。

16. 发明申请

US20050178650A1 Method for producing organic alkyne compounds 审中-公开
标题翻译：有机炔化合物的制备方法
公开(公告)号：US20050178650A1
公开(公告)日：2005-08-18
申请号：US10511761
申请日：2003-04-25
申请人： Robert Parker , Robert Reinhard
发明人： Robert Parker , Robert Reinhard
IPC分类号： C07C51/353 , C07B61/00 , C07C2/86 , C07C63/66 , C07D285/12 , C07D285/14 , C07D41/02 , C07D43/02
CPC分类号： C07C2/861
摘要： The invention relates to a method for producing organic alkyne compounds of formula (I), X—C═C—Y According to said method, organic halogen compounds of formula (Ia), X-Hal, are reacted with organic terminal alkyne compounds of formula (Ib), H—C═C—Y, X and Y representing the same or different organic radicals and Hal representing chlorine or bromine, in inert solvents under the action of microwave radiation, in the presence of at least one metallic compound and at least one base.
摘要翻译：本发明涉及一种制备式（I）的有机炔化合物的方法，XCCY根据所述方法，式（Ia）的有机卤素化合物，X-Hal与式（Ib）的有机末端炔化合物，HCCY 在微波辐射的作用下，在至少一种金属化合物和至少一种碱的存在下，在惰性溶剂中代表相同或不同的有机基团和Hal代表氯或溴。

17. 发明申请

US20050065388A1 Method for formulation of synthetic gas oils or additives for gas oil 失效
标题翻译：合成瓦斯油或瓦斯油添加剂的配制方法
公开(公告)号：US20050065388A1
公开(公告)日：2005-03-24
申请号：US10943896
申请日：2004-09-20
申请人： Patrick Briot , Sylvie Lacombe , Jean-Francois Joly , Eric Llido
发明人： Patrick Briot , Sylvie Lacombe , Jean-Francois Joly , Eric Llido
IPC分类号： C07C2/64 , C07C2/66 , C07C2/86 , C07C5/10 , C07C13/18 , C10L1/08
CPC分类号： C10L1/08 , C07C2/64 , C07C2/66 , C07C2/861 , C07C5/10 , C07C13/18 , C07C2521/04 , C07C2527/126 , C07C2529/18 , C07C2601/14 , C07C15/107
摘要： The invention relates to a method for formulation of a synthetic gas oil or an additive for gas oil in which an alkyl-aromatic compound or a mixture of alkyl-aromatic compounds is selected based on at least one parameter that is selected from the group that consists of the number of cycles of the aromatic core, the number of alkyl chains that are grafted to the aromatic cycle, the length of the alkyl chain or chains, the position of the aromatic cycle or cycles on the alkyl chain or chains of said alkyl-aromatic compound or compounds such that the cetane number of the synthetic gas oil or the additive for gas oil is greater than 30. The invention also relates to a process for the production of alkyl-aromatic compounds for use as a gas oil or additive.
摘要翻译：本发明涉及一种用于制备瓦斯油的合成瓦斯油或其添加剂的方法，其中烷基芳族化合物或烷基芳族化合物的混合物基于至少一个参数，该参数选自组成的芳族核心的循环次数，接枝到芳香环的烷基链的数量，烷基链或链的长度，芳族环或在所述烷基链或烷基链的烷基链上的循环的位置，芳族化合物或化合物，使得合成瓦斯油的十六烷值或瓦斯油的添加剂大于30.本发明还涉及用作瓦斯油或添加剂的烷基 - 芳族化合物的制备方法。

18. 发明授权

US06852896B2 Concerted process for the production of an alkenyl substituted aromatic compound 有权
标题翻译：用于生产烯基取代的芳族化合物的协调方法
公开(公告)号：US06852896B2
公开(公告)日：2005-02-08
申请号：US10268803
申请日：2002-10-11
申请人： John E. Stauffer
发明人： John E. Stauffer
IPC分类号： C07C2/86 , C07C17/156 , C07C1/20
CPC分类号： C07C17/156 , C07C2/861 , Y02P20/125 , C07C15/02
摘要： An integrated process of preparing a C2-5 alkenyl-substituted aromatic compound using a C6-12 aromatic compound and a C2-5 alkane as raw materials. The process involves two reaction steps operating in tandem, the first reaction step reacts the C6-12 aromatic compound with hydrogen chloride and molecular oxygen in the presence of a catalyst to yield water and mono-, di-, tri-, and higher chlorinated aromatic adducts. The chlorinated compounds from the first reaction step are reacted with ethane in the second reaction step to produce alkane-substituted aromatic compounds which spontaneously dehydrogenate to an alkenyl-substituted aromatic compound and hydrogen chloride. After separating the alkenyl-substituted aromatic product from the hydrogen chloride, the hydrogen chloride is recycled to the first reaction step so that there is no net production or consumption of hydrogen chloride.
摘要翻译：使用C6-12芳香族化合物和C2-5烷烃作为原料制备C2-5烯基取代的芳族化合物的综合方法。该方法包括串联操作的两个反应步骤，第一反应步骤在催化剂存在下使C6-12芳族化合物与氯化氢和分子氧反应，得到水和一，二，三和高级氯代芳族化合物加合物在第二反应步骤中将来自第一反应步骤的氯化化合物与乙烷反应，以生成烷基取代的芳族化合物，其自发脱氢至烯基取代的芳族化合物和氯化氢。在将烯基取代的芳族化合物与氯化氢分离后，将氯化氢循环至第一反应步骤，使得不产生或消耗氯化氢。

19. 发明授权

US06548722B1 Process for the preparation of substituted aromatic compound employing friedel-crafts reaction using a reusable basic anionic clay catalyst 失效
标题翻译：使用可重复使用的碱性阴离子粘土催化剂使用Friedel-Crafts反应制备取代的芳族化合物的方法
公开(公告)号：US06548722B1
公开(公告)日：2003-04-15
申请号：US09685682
申请日：2000-10-10
申请人： Vasant Ramchandra Choudhary , Suman Kumar Jana
发明人： Vasant Ramchandra Choudhary , Suman Kumar Jana
IPC分类号： C07C30900
CPC分类号： C07C41/30 , C07C2/861 , C07C2/864 , C07C45/46 , C07C201/12 , C07C2521/10 , C07C2523/08 , C07C2527/236 , C07C2603/24 , C07C15/16 , C07C49/784 , C07C49/83 , C07C49/84 , C07C49/786 , C07C205/06 , C07C15/12 , C07C15/28 , C07C43/205
摘要： A process for Friedel-Crafts type liquid-phase alkylation or acylation of an aromatic compound using a hydrotalcite-type basic anionic clay catalyst represented by a formula: [(M2−)1−x(M3+)x(OH)2]x+[Ay−]x/yqH2O where M2+ is a divalent cation selected from Mg2+, Zn2+, Ni2+, Co2+, Mn2+, Cu2+ or a mixture thereof; M3+ is a trivalent cation selected from Ga3+, In3+ Al3+, Fe3+ Cr3+ or a mixture thereof; x is a mole fraction of trivalent cations in the range of about 0.05 to about 0.5; 0 is oxygen; H is hydrogen; Ay− is an anion; y minus is an anionic negative charge having a value of 1 minus or 2 minus; and q is a number of water molecules, as the water of hydration; and involving following steps: i. pretreating said catalyst by contacting it with a halogen containing compound in the presence or absence of a non-aqueous solvent and optionally washing the pretreated catalyst with non-aqueous solvent or liquid aromatic compound to be alkylated or acylated; and then ii. contacting a liquid reaction mixture comprising said aromatic compound and said alkylating or acylating agent in the presence or absence of a non-aqueous solvent with the catalyst obtained from step (i) in a stirred batch reactor fitted with a reflux condenser under vigorous stirring, in the presence or absence of an inert gas bubbling through the reaction mixture, at effective reaction conditions; iii. cooling the reaction mixture to a temperature about 30° C., removing said catalyst from the reaction mixture by filtration and then separating the reaction products from the reaction mixture, and optionally washing the used catalyst by non-aqueous solvent, and if desired, iv. reusing the used catalyst directly with or without drying for the subsequent reaction batch avoiding step (i), is disclosed.
摘要翻译：使用由下式表示的水滑石型碱性阴离子粘土催化剂，使用Friedel-Crafts型液相烷基化或芳族化合物酰化的方法：其中M2 +是选自Mg2 +，Zn2 +，Ni2 +，Co2 +，Mn2 +，Cu2 +或其混合物; M3 +是选自Ga3 +，In3 + Al3 +，Fe3 + Cr3 +或其混合物的三价阳离子; x是三价阳离子在约0.05至约0.5范围内的摩尔分数; 0是氧; H是氢; Ay-是阴离子; y minus是具有值1或2减去的阴离子负电荷; 和q是水分子的数量，作为水合水; 并涉及以下步骤：i。在存在或不存在非水溶剂的情况下，通过使其与含卤素的化合物接触来预处理所述催化剂，并任选地用待进行烷基化或酰化的非水溶剂或液体芳族化合物洗涤预处理的催化剂; 然后。在非水溶剂存在或不存在下，将含有所述芳族化合物和所述烷基化或酰化剂的液体反应混合物与步骤（i）获得的催化剂在剧烈搅拌下在装有回流冷凝器的搅拌间歇式反应器中接触，在有效的反应条件下存在或不存在通过反应混合物鼓泡的惰性气体; iii。将反应混合物冷却至约30℃的温度，通过过滤从反应混合物中除去所述催化剂，然后将反应产物与反应混合物分离，并任选地通过非水溶剂洗涤所用催化剂，如果需要，将iv 。公开了直接使用或不用干燥后续反应批次的用过的催化剂，以避免步骤（i）。

20. 发明申请

US20020187891A1 Zeolite catalyst and use for hydrocarbon conversion 失效
公开(公告)号：US20020187891A1
公开(公告)日：2002-12-12
申请号：US10126597
申请日：2002-04-19
发明人： Johannes Petrus Verduijn , Jannetje Maatje van de Berge , Gary D. Mohr
IPC分类号： B01J029/06
CPC分类号： C10G11/05 , B01J29/005 , B01J29/06 , B01J29/061 , B01J29/084 , B01J29/40 , B01J29/50 , B01J29/60 , B01J29/70 , B01J29/80 , B01J29/83 , B01J29/84 , B01J29/85 , B01J29/87 , B01J2229/42 , B01J2229/62 , C07C1/20 , C07C2/861 , C07C2/864 , C07C2/865 , C07C2/868 , C07C4/06 , C07C5/2708 , C07C5/2737 , C07C5/41 , C07C6/123 , C07C6/126 , C07C2529/035 , C07C2529/08 , C07C2529/18 , C07C2529/40 , C07C2529/50 , C07C2529/65 , C07C2529/70 , C07C2529/80 , C10G29/205 , C10G35/065 , C10G35/095 , C10G45/64 , Y02P20/52 , C07C15/00 , C07C15/08
摘要： There is provided a zeolite bound zeolite catalyst which can be tailored to optimize its performance and a process for converting hydrocarbons utilizing the zeolite bound zeolite catalyst. The zeolite bound zeolite catalyst comprises a first zeolite and a binder comprising a second zeolite. The structure type of the second zeolite is different from the structure type of the first zeolite. The zeolite bound zeolite finds particular application in hydrocarbon conversion process, e.g., catalytic cracking, alkylation, disproportional of toluene, isomerization, and transalkylation reactions.

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