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11. 发明申请

US20040031757A1 High performance continuous reaction/separation process using a continuous liquid-solid contactor 审中-公开
公开(公告)号：US20040031757A1
公开(公告)日：2004-02-19
申请号：US10213580
申请日：2002-08-06
发明人： Chen-Chou Chiang , David L. Fair
IPC分类号： C02F001/28
CPC分类号： B01D15/1857 , B01D15/1864 , B01D2215/023 , B01D2215/028 , C07C37/20 , C07C39/16
摘要： A process for reaction and separation which comprises inputting a process material into at least one column of a plurality of columns wherein each column has at least one inlet for accepting flow from another column or group of columns, an external feed stream, an external eluent stream or a combination thereof, and each column has at least one outlet for connecting to another column, a group of columns, an external product stream or a combination thereof. Each column is independently operable in an up-flow or down-flow mode and connected independently to one of the group comprising another column, an external feed stream, an external eluent stream, an external product stream and combinations thereof.

12. 发明申请

US20040019241A1 Process for the production of bisphenol-A 失效
标题翻译：生产双酚A的方法
公开(公告)号：US20040019241A1
公开(公告)日：2004-01-29
申请号：US10412180
申请日：2003-04-11
发明人： Chen-Chou Chiang , David L. Fair
IPC分类号： C07C039/16
CPC分类号： B01D15/1857 , B01D15/1864 , B01D2215/023 , B01D2215/028 , C07C37/20 , C07C39/16
摘要： The invention provides a process for the continuous production of bisphenol-A by continuously reacting phenol using an acid catalyst resin and continuously or essentially continuously removing water from the system. Continuous removal of water allows for increased catalytic activity of the resin and therefore improved productivity. Removal is facilitated by conducting the process in a carousel simulated moving bed device. Process efficiency is further enhanced by conducting the process in a device configured to have a combination of series, parallel or reverse flows which are optionally arranged so the process results in higher yield and lower impurities.
摘要翻译：本发明提供了一种通过使用酸催化剂树脂连续反应苯酚并连续或基本上连续地从体系中除去水来连续生产双酚A的方法。持续去除水允许增加树脂的催化活性，从而提高生产率。通过在旋转木马模拟移动床装置中进行该过程来促进移除。通过在配置为具有串联，并联或逆流的组合的装置中进行该方法进一步提高了工艺效率，该组合可选地布置，使得该方法产生较高的产率和较低的杂质。

13. 发明授权

US09914072B2 Process for operating a simulated moving bed reactor 有权
公开(公告)号：US09914072B2
公开(公告)日：2018-03-13
申请号：US15316542
申请日：2015-06-04
申请人： GEORGIA TECH RESEARCH CORPORATION
发明人： Yoshiaki Kawajiri , Andreas S. Bommarius , Jungmin Oh , Gaurav Agrawal , Balamurali Sreedhar
IPC分类号： B01D15/18 , C07C67/08 , C07C67/56
CPC分类号： B01D15/1857 , C07C67/08 , C07C67/56 , C07C69/14
摘要： The present disclosure provides for a process for supplying a first reactant and a second reactant (reactants) to a simulated moving bed reactor (SMBR) at each step of a sequential repeating injection cycle, where the SMBR includes zones each having an injection point and each containing a solid separation media; reacting the reactants in the SMBR during the sequential repeating injection cycle (cycle) to form a first product; separating the first product in the SMBR with the solid separation media; and changing an amount of one or both of the reactants injected at one or more of the injection points of the SMBR during a step of the cycle. Changing the amount of the reactants can be done at each step of the sequential repeating injection cycle. Changing the amount can include changing an inlet concentration of the reactants injected at one or more of the injection points during each step of the cycle.

14. 发明授权

US08216475B2 Process and device for separating fractions of a mixture 有权
$Process and device for separating fractions of a mixture$
标题翻译：用于分离混合物馏分的方法和装置
公开(公告)号：US08216475B2
公开(公告)日：2012-07-10
申请号：US12281170
申请日：2007-03-07
申请人： Eric Valery , Céline Morey
发明人： Eric Valery , Céline Morey
IPC分类号： B01D15/08
CPC分类号： B01D15/1828 , B01D15/1857
摘要： The invention concerns a method for separating fractions of a mixture using a chromatography device. The method includes the following steps: controlling in one node of the device, the history of a specific variable of the fractions of the mixture to be separated; detecting one characteristic point of the history, the characteristic point being between two successive steps of fraction collecting; comparing the position of the characteristic point relative to a target position; adjusting the amount of mobile phase modifying the position of the characteristic point to cause the position of the characteristic point to coincide with the target position. The invention also concerns a device for implementing the method. The method enables the operation of the device to be automatically set.
摘要翻译：本发明涉及使用色谱装置分离混合物的馏分的方法。该方法包括以下步骤：在设备的一个节点中控制要分离的混合物的分数的特定变量的历史; 检测历史的一个特征点，特征点在分级收集的两个连续步骤之间; 比较特征点相对于目标位置的位置; 调整移动相位的量，改变特征点的位置，使得特征点的位置与目标位置一致。本发明还涉及一种用于实现该方法的装置。该方法使得能够自动设置设备的操作。

15. 发明授权

US07749390B2 Semi-continuous chromatographic method and corresponding device for the separation of binary and multi-component mixtures 失效
标题翻译：半连续色谱法和相应的二元和多组分混合物分离装置
公开(公告)号：US07749390B2
公开(公告)日：2010-07-06
申请号：US11916057
申请日：2006-06-03
申请人： Abdelaziz Toumi
发明人： Abdelaziz Toumi
IPC分类号： B01D15/08
CPC分类号： G01N30/44 , B01D15/1828 , B01D15/1842 , B01D15/1857 , G01N30/463
摘要： The invention relates to a semi-continuous chromatographic method for the separation of binary and multi-component mixtures and corresponding devices.
摘要翻译：本发明涉及用于分离二元和多组分混合物和相应装置的半连续色谱方法。

16. 发明授权

US07108789B2 High performance continuous reaction/separation process using a continuous liquid-solid contactor 有权
标题翻译：使用连续液固接触器的高性能连续反应/分离过程
公开(公告)号：US07108789B2
公开(公告)日：2006-09-19
申请号：US10412502
申请日：2003-04-11
申请人： Chen-Chou Chiang , David L. Fair
发明人： Chen-Chou Chiang , David L. Fair
IPC分类号： B01D15/04 , C02F1/44
CPC分类号： C07C37/20 , B01D15/1857 , B01D15/1864 , B01D2215/023 , B01D2215/028 , C07C39/16
摘要： A process for reaction and separation which comprises inputting a process material into at least one column of a plurality of columns wherein each column has at least one inlet for accepting flow from another column or group of columns, an external feed stream, an external eluent stream or a combination thereof, and each column has at least one outlet for connecting to another column, a group of columns, an external product stream or a combination thereof. Each column is independently operable in an up-flow or down-flow mode and connected independently to one of the group comprising another column, an external feed stream, an external eluent stream, an external product stream and combinations thereof.
摘要翻译：一种用于反应和分离的方法，其包括将工艺材料输入到多个塔的至少一个塔中，其中每个塔具有至少一个入口，用于接受来自另一个塔或一组塔的流，外部进料流，外部洗脱液流或其组合，并且每个柱具有至少一个用于连接到另一个柱，一组柱，外部产物流或其组合的出口。每列可独立地在上流或下流模式下操作，并且独立地与包括另一柱，外部进料流，外部洗脱液流，外部产物流及其组合的组之一独立连接。

17. 发明授权

US6063284A Single column closed-loop recycling with periodic intra-profile injection 失效
标题翻译：单柱闭环回收利用周期性轮廓内注射
公开(公告)号：US6063284A
公开(公告)日：2000-05-16
申请号：US857039
申请日：1997-05-15
申请人： Charles M. Grill
发明人： Charles M. Grill
IPC分类号： B01D15/08 , B01D15/18 , G01N30/44
CPC分类号： B01D15/1814 , B01D15/1857 , G01N30/44
摘要： A preparative chromatographic cyclical process utilizing a single column comprising, at steady state: (a) establishing and maintaining a circulating chromatographic profile through said column and through one solvent pump; (b) discontinuously and periodically injecting a sample comprising at least two components, into the interior of said maintained circulating profile; and (c) collecting, discontinuously and periodically, at least two enriched fractions from said circulating profile.
摘要翻译：使用单柱的制备型色谱循环方法，其包括在稳定状态：（a）通过所述柱和通过一种溶剂泵建立和维持循环色谱图; （b）不连续地和周期地将包含至少两个组分的样品注入所述维持的循环轮廓的内部; 和（c）从所述循环曲线收集，不连续和周期性地至少两个富集部分。

18. 发明授权

US5630943A Discontinuous countercurrent chromatographic process and apparatus 失效
标题翻译：不连续的逆流色谱法和仪器
公开(公告)号：US5630943A
公开(公告)日：1997-05-20
申请号：US566425
申请日：1995-11-30
申请人： Charles M. Grill
发明人： Charles M. Grill
IPC分类号： G01N30/46 , B01D15/08 , B01D15/18 , G01N30/44
CPC分类号： B01D15/1814 , B01D15/1864 , G01N30/44 , B01D15/1857
摘要： A preparative chromatographic cyclical process comprising, at steady state: establishing a figure-of-eight circulating chromatographic profile between two chromatographic columns with the provision that said chromatographic profile never passes through a pump; discontinuously and periodically injecting a sample comprising at least two components, into said circulating profile; and collecting, discontinuously and periodically, at least two enriched fractions from said circulating profile, the apparatus for conducting this process comprising only two chromatographic columns, at least one solvent pump, an injection pump, two 4-way valves, and conduit communicating said columns and the two 4-way valves in the form of a figure-of-eight pattern without traversing a pump, and conduit communicating said at least one solvent pump and at least one of said columns.
摘要翻译：一种制备型色谱循环方法，其包括在稳定状态：在两个色谱柱之间建立八位循环色谱图，其规定所述色谱图从未通过泵; 不连续地和周期性地将包含至少两个组分的样品注入所述循环轮廓; 以及从所述循环曲线收集，不连续和周期性地至少两个富集部分，用于进行该方法的装置仅包括两个色谱柱，至少一个溶剂泵，注射泵，两个四通阀和将所述柱和两个八通阀形式的图形，而不穿过泵，以及连通所述至少一个溶剂泵和至少一个所述柱的导管。

19. 发明授权

US09732025B2 Process for equilibrium-limited reactions 有权
公开(公告)号：US09732025B2
公开(公告)日：2017-08-15
申请号：US14888535
申请日：2014-05-02
申请人： Dow Global Technologies LLC , Georgia Tech Research Corporation
发明人： Yoshiaki Kawajiri , Andreas Sebastian Bommarius , Timothy C. Frank , Megan E. Donaldson , Jungmin Oh , Gaurav Agrawal
IPC分类号： C07C67/02 , C07C51/48 , B01D15/36 , C07C67/08 , B01D15/38 , C07C67/56 , B01D15/18
CPC分类号： C07C51/48 , B01D15/1857 , B01D15/362 , B01D15/3857 , C07C67/08 , C07C67/56 , Y02P20/127 , C07C69/14
摘要： A process for conducting equilibrium-limited chemical reactions that produce water as a reaction product. Specifically, a process that uses a reactive chromatography unit (RCU) to improve the efficiency of equilibrium-limited reactions, such as a process for reacting glycol ether (GE) and carboxylic acid (CA) to form water and glycol ether ester (GEE). The process includes supplying GE and CA to the RCU, where one of either the CA or the GE is in a stoichiometric deficit relative to the other reactant. The reactant in the stoichiometric deficit reacts in the presence of the catalyst in the RCU to form a mixture of GEE and water. A raffinate is separated from the mixture using the separation media of the RCU contains at least the GEE. An extract separated from the mixture using the separation media of the RCU contains at least the water.

20. 发明申请

US20170216740A1 PROCESS FOR OPERATING A SIMULATED MOVING BED REACTOR 有权
公开(公告)号：US20170216740A1
公开(公告)日：2017-08-03
申请号：US15316542
申请日：2015-06-04
申请人： GEORGIA TECH RESEARCH CORPORATION
发明人： Yoshiaki Kawajiri , Andreas S. Bommarius , Jungmin Oh , Gaurav Agrawal , Balamurali Sreedhar
IPC分类号： B01D15/18 , C07C67/56 , C07C67/08
CPC分类号： B01D15/1857 , C07C67/08 , C07C67/56 , C07C69/14
摘要： The present disclosure provides for a process for supplying a first reactant and a second reactant (reactants) to a simulated moving bed reactor (SMBR) at each step of a sequential repeating injection cycle, where the SMBR includes zones each having an injection point and each containing a solid separation media; reacting the reactants in the SMBR during the sequential repeating injection cycle (cycle) to form a first product; separating the first product in the SMBR with the solid separation media; and changing an amount of one or both of the reactants injected at one or more of the injection points of the SMBR during a step of the cycle. Changing the amount of the reactants can be done at each step of the sequential repeating injection cycle. Changing the amount can include changing an inlet concentration of the reactants injected at one or more of the injection points during each step of the cycle.

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