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11. 发明授权

US07767858B2 Diimines and secondary diamines 失效
标题翻译：二亚胺和仲胺
公开(公告)号：US07767858B2
公开(公告)日：2010-08-03
申请号：US11855839
申请日：2007-09-14
申请人： Paul L. Wiggins , Judit Orgad , John Y. Lee , Mahmood Sabahi
发明人： Paul L. Wiggins , Judit Orgad , John Y. Lee , Mahmood Sabahi
IPC分类号： C07C209/26
CPC分类号： C07C211/12 , C07C211/51 , C08G18/10 , C08G18/3234 , C08G18/324 , C08G18/325 , C08G18/5024 , C08G18/6685 , C08G18/7671 , Y02P20/582
摘要： This invention provides aromatic diimines which have imino hydrocarbylidene groups with at least two carbon atoms, and aromatic secondary diamines which have amino hydrocarbyl groups with at least two carbon atoms. Both the aromatic diimines and the aromatic secondary diamines either are in the form of one phenyl ring, or are in the form of two phenyl rings connected by an alkylene bridge; each position ortho to an imino group or an amino group bears a hydrocarbyl group. When in the form of one phenyl ring, there are two imino groups on the ring or two amino groups on the ring; the imino groups or amino groups are meta or para relative to each other. When in the form of two phenyl rings connected by an alkylene bridge, there is either one imino group or one amino group on each phenyl ring. Also provided are processes for forming diimines and secondary diamines.
摘要翻译：本发明提供具有至少两个碳原子的亚氨基亚烃基的芳族二亚胺和具有至少两个碳原子的氨基烃基的芳族仲二胺。芳族二亚胺和芳族仲胺都是一个苯环的形式，或者是由亚烷基桥连接的两个苯环的形式; 亚氨基或氨基的邻位各为一个烃基。当以一个苯环的形式，环上有两个亚氨基或环上两个氨基; 亚氨基或氨基相对于彼此是间位或对位的。当以亚烷基桥连接的两个苯环的形式，每个苯环上有一个亚氨基或一个氨基。还提供了形成二亚胺和仲二胺的方法。

12. 发明申请

US20080262187A1 Blends of Diamines Having Reduced Color 审中-公开
标题翻译：减少颜色的二胺的共混物
公开(公告)号：US20080262187A1
公开(公告)日：2008-10-23
申请号：US12096128
申请日：2006-12-21
申请人： John Y. Lee , David W. Owens , Paul L. Wiggins , Richard D. Glass , Michael J. Wilhelm , Robert Phillip Slicker
发明人： John Y. Lee , David W. Owens , Paul L. Wiggins , Richard D. Glass , Michael J. Wilhelm , Robert Phillip Slicker
IPC分类号： C08G71/02 , C07C211/54 , C08G71/04 , C07C211/50
CPC分类号： C08G18/325 , C07C211/50 , C08G18/3237 , C08G18/5024 , C08G18/6685
摘要： This invention provides a blend which comprises (i) at least one aromatic primary diamine, with which has been blended a color-minimizing amount of at least one N,N-dmydrocarbylhydroxylamine, wherein the aromatic primary diamine is in the form of one benzene ring having two primary amino groups on the ling, which amino groups are meta or para relative to each other, and in which each position ortho to a primary amino group bears an alkyl group, and (ii) at least one aromatic secondary diamine having a Gardner color number no more than about 7, wherein said aromatic secondary diamine either is in the form of one benzene ring having two secondary amino groups on the ring, or is in the form of two benzene rings connected by an alkylene bridge and having one secondary amino group on each ring. Optionally, at least one N,N-dihydrocarbylhydroxylamine has been blended with the aromatic secondary diamine.
摘要翻译：本发明提供了一种共混物，其包含（i）至少一种芳族伯二胺，与其配合着色最小化量的至少一种N，N-二烃基羟胺，其中芳族伯胺为一个苯环形式在氨基上具有两个伯氨基，这些氨基相对于彼此是间位或对位的，并且其中与伯氨基邻位的每个位置都具有烷基，和（ii）至少一种具有加德纳的芳族仲胺颜色数不超过约7，其中所述芳族仲胺是环上具有两个仲氨基的一个苯环的形式，或者是由亚烷基桥连接并具有一个仲氨基的两个苯环的形式组在每个戒指任选地，将至少一种N，N-二烃基羟胺与芳族仲胺共混。

13. 发明申请

US20080194788A1 Diimines and Secondary Diamines 有权
标题翻译：二亚胺和二胺
公开(公告)号：US20080194788A1
公开(公告)日：2008-08-14
申请号：US11909824
申请日：2005-12-30
申请人： John Y. Lee , Paul L. Wiggins , Judit Orgad , Mahmood Sabahi , Vernon O. Brandt , David W. Owens
发明人： John Y. Lee , Paul L. Wiggins , Judit Orgad , Mahmood Sabahi , Vernon O. Brandt , David W. Owens
IPC分类号： C08G18/00 , C07C211/49 , C07C249/02
CPC分类号： C07C211/12 , C07C211/51 , C08G18/10 , C08G18/3234 , C08G18/324 , C08G18/325 , C08G18/5024 , C08G18/6685 , C08G18/7671 , Y02P20/582
摘要： This invention provides aromatic diimines where the diimines have imino groups with at least two carbon atoms, and either are in the form of one benzene ring having two imino groups on the ring, which imino groups are meta or para relative to each other, and in which each position ortho to an imino group bears a hydrocarbyl group, or are in the form of two benzene rings connected by an alkylene bridge and having one imino group on each ring, and in which each position ortho to an imino group bears a hydrocarbyl group. This invention also provides aromatic secondary diamines where the diamines have amino hydrocarbyl groups with at least two carbon atoms, and either are in the form of one benzene ring having two amino groups on the ring, which amino groups are meta or para relative to each other, and in which each position ortho to an amino group bears a hydrocarbyl group, or are in the form of two benzene rings connected by an alkylene bridge and having one amino group on each ring, and in which each position ortho to an amino group bears a hydrocarbyl group. Also provided are processes for forming diimines and secondary diamines from primary diamines, including the aromatic diimines and aromatic secondary diamines of the invention.
摘要翻译：本发明提供芳族二亚胺，其中二亚胺具有至少两个碳原子的亚氨基，并且是环上具有两个亚氨基的一个苯环的形式，该亚氨基相对于彼此是间位或对位的，并且在其中每个位于亚氨基的邻位具有烃基，或者是由亚烷基桥连接并在每个环上具有一个亚氨基的两个苯环的形式，并且其中亚氨基的邻位各有一个烃基。本发明还提供芳族仲二胺，其中二胺具有至少两个碳原子的氨基烃基，并且是环上具有两个氨基的一个苯环的形式，该氨基相对于彼此是间位或对位的并且其中氨基的每个位置具有烃基，或者为两个苯环的形式，其通过亚烷基桥连接并且在每个环上具有一个氨基，并且其中氨基的邻位各自承载烃基。还提供了由伯二胺形成二亚胺和仲二胺的方法，包括本发明的芳族二亚胺和芳族仲二胺。

14. 发明授权

US5874619A Reducing the coloration of aromatic diamines 失效
标题翻译：减少芳族二胺的着色
公开(公告)号：US5874619A
公开(公告)日：1999-02-23
申请号：US56600
申请日：1998-04-07
申请人： Paul L. Wiggins , Gregory H. Lambeth , William R. Brown
发明人： Paul L. Wiggins , Gregory H. Lambeth , William R. Brown
IPC分类号： C07B61/00 , C07C209/68 , C07C209/90 , C07C211/50 , C07C211/51 , C07C209/38
CPC分类号： C07C209/90
摘要： Existing coloration of a liquid ring-polyalkyl-substituted aromatic primary diamine is reduced by blending into such diamine a color-reducing amount of at least one dihydrocarbylhydroxylamine. Preferably, the resultant product is stored in a closed container under an inert atmosphere.
摘要翻译：通过混合到这种二胺中减少颜料的至少一种二烃基羟胺来降低液体环 - 多烷基取代的芳族伯二胺的现有着色。优选地，将所得产物在惰性气氛下储存在密闭容器中。

15. 发明授权

US5705039A Process for purifying a 2,6-dialkylphenol 失效
标题翻译：纯化2,6-二烷基苯酚的方法
公开(公告)号：US5705039A
公开(公告)日：1998-01-06
申请号：US542612
申请日：1995-10-13
申请人： Sam F. Clarke , Venkataraman Ramachandran , J. Steve Staton , Paul L. Wiggins
发明人： Sam F. Clarke , Venkataraman Ramachandran , J. Steve Staton , Paul L. Wiggins
IPC分类号： B01D3/14 , C07C37/74 , B01D3/00 , C07C37/68
CPC分类号： B01D3/146 , C07C37/685 , C07C37/74 , Y10S203/07 , Y10S203/09
摘要： Impure 2,6-diisopropylphenol (DIP) is purified by use of a distillation process in which a single distillation column is used. The process comprises: (a) subjecting the impure DIP to a first continuous distillation in the column in an inert environment to distill off lower boiling components and produce first column bottoms enriched in DIP; (b) collecting, cooling and storing the first column bottoms while continuously maintaining them in an inert environment; (c) discontinuing the first continuous distillation; (d) subjecting the first column bottoms to a second continuous distillation in an inert environment in the same column to produce a second overhead distillate composed of purified DIP. The process avoids the formation in the distilling mixtures of dose boiling impurities due to seepage of air through standard pipe flanges and fittings and consequent oxidation reactions which occur under the conditions needed for batch distillations conducted in typical industrial distillation facilities. These impurities include 2,6-diisopropylbenzoquinone, 2-isopropyl-6-isopropenylphenol, 2,6-diisopropenylphenol and 2,2-dimethyl-4-isopropyl-1,3-benzodioxole. The capital investment needed for a conventional continuous distillation facility is also avoided.
摘要翻译：不纯的2,6-二异丙基苯酚（DIP）通过使用其中使用单个蒸馏塔的蒸馏方法纯化。该方法包括：（a）使惰性DIP在惰性环境中在柱中进行第一次连续蒸馏以蒸馏掉低沸点组分并产生富含DIP的第一塔底物; （b）收集，冷却和储存第一塔底，同时将其保持在惰性环境中; （c）停止第一次连续蒸馏; （d）在同一塔的惰性环境中对第一塔底部进行第二次连续蒸馏以产生由纯化的DIP组成的第二塔顶馏出物。该过程避免了在典型工业蒸馏设备中进行的批次蒸馏所需的条件下，由于通过标准管道法兰和配件的空气渗漏导致的沸腾杂质的蒸馏混合物中的形成以及随之而来的氧化反应。这些杂质包括2,6-二异丙基苯醌，2-异丙基-6-异丙烯基苯酚，2,6-二异丙烯基苯酚和2,2-二甲基-4-异丙基-1,3-苯并间二氧杂环戊烯。也避免了常规连续蒸馏设备所需的投资。

16. 发明授权

US4757119A Epoxy resin compositions containing poly-(hydrocarbylthio)aromatic diamines 失效
标题翻译：含有聚（烃硫基）芳族二胺的环氧树脂组合物
公开(公告)号：US4757119A
公开(公告)日：1988-07-12
申请号：US45521
申请日：1987-05-04
申请人： Paul L. Wiggins , Gordon G. Knapp
发明人： Paul L. Wiggins , Gordon G. Knapp
IPC分类号： C08G59/40 , C08G59/50
CPC分类号： C08G59/504
摘要： Novel compositions suitable for use in preparing prepregs comprise an epoxy resin and a poly(hydrocarbylthio)aromatic diamine curing agent, preferably a substituted di(alkylthio)-diaminobenzene wherein the alkylthio groups contain 1-10 carbons.

17. 发明申请

US20120252971A1 Coating Composition 有权
标题翻译：涂料组成
公开(公告)号：US20120252971A1
公开(公告)日：2012-10-04
申请号：US13515582
申请日：2010-12-16
申请人： Peter J. Schreiber , Samuel L. Lane , Paul L. Wiggins
发明人： Peter J. Schreiber , Samuel L. Lane , Paul L. Wiggins
IPC分类号： C09D175/04 , C08L75/04 , C08K5/12 , C08G18/32
CPC分类号： C09D175/02 , C08G18/10 , C08G18/3243
摘要： The present invention relates to a coating composition. More particularly the present invention relates to a coating composition comprising an amine curative composition comprising a bis-aromatic secondary diamine, a bis-aromatic primary diamine and optionally a mono-aromatic primary diamine.
摘要翻译：本发明涉及涂料组合物。更具体地说，本发明涉及包含胺固化剂组合物的涂料组合物，其包含双芳族仲胺，双芳族伯二胺和任选的单芳族伯二胺。

18. 发明授权

US08536297B2 Coating composition 有权
标题翻译：涂料组成
公开(公告)号：US08536297B2
公开(公告)日：2013-09-17
申请号：US13515582
申请日：2010-12-16
申请人： Peter J. Schreiber , Samuel L. Lane , Paul L. Wiggins
发明人： Peter J. Schreiber , Samuel L. Lane , Paul L. Wiggins
IPC分类号： C08G18/32
CPC分类号： C09D175/02 , C08G18/10 , C08G18/3243
摘要： The present invention relates to a coating composition. More particularly the present invention relates to a coating composition comprising an amine curative composition comprising a bis-aromatic secondary diamine, a bis-aromatic primary diamine and optionally a mono-aromatic primary diamine.
摘要翻译：本发明涉及涂料组合物。更具体地说，本发明涉及包含胺固化剂组合物的涂料组合物，其包含双芳族仲胺，双芳族伯二胺和任选的单芳族伯二胺。

19. 发明授权

US4775736A Epoxy curing agent composition 失效
标题翻译：环氧固化剂组合物
公开(公告)号：US4775736A
公开(公告)日：1988-10-04
申请号：US89524
申请日：1987-08-26
申请人： Paul L. Wiggins
发明人： Paul L. Wiggins
IPC分类号： C08G59/50 , C08G59/72 , C08G59/68 , C08G65/10
CPC分类号： C08G59/5033 , C08G59/72
摘要： Epoxy resins having acceptable pot lives, degrees of reactivity, and physical properties are obtained by the use of curing agent compositions which comprise about 99.6-90% by weight of a hindered aromatic diamine, such as diethyltoluenediamine, and about 0.4-10% by weight of an accelerator complex of boron trifluoride and a cycloaliphatic diamine, such as isophoronediamine.
摘要翻译：具有可接受的适用寿命，反应活性和物理性能的环氧树脂通过使用包含约99.6-90％重量的受阻芳族二胺如二乙基甲苯二胺和约0.4-10％重量的固化剂组合物获得的三氟化硼和脂环族二胺的加速剂络合物，例如异佛尔酮二胺。

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