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11. 发明授权

US07285692B2 Process for the preparation of 1,1,1,3,3-pentafluoropropane and 1,1,1,2,3-pentafluoropropane 有权
标题翻译：制备1,1,1,3,3-五氟丙烷和1,1,1,2,3-五氟丙烷的方法
公开(公告)号：US07285692B2
公开(公告)日：2007-10-23
申请号：US10572626
申请日：2004-10-13
申请人： Velliyur Nott Mallikarjuna Rao , Allen C. Sievert
发明人： Velliyur Nott Mallikarjuna Rao , Allen C. Sievert
IPC分类号： C07C17/10 , C07C17/00
CPC分类号： B01J23/002 , B01J23/26 , B01J27/12 , B01J35/0006 , B01J37/26 , B01J2523/00 , C07C17/21 , C07C17/23 , C07C19/08 , C07C19/10 , B01J2523/27 , B01J2523/67
摘要： A process is disclosed for the manufacture of CF3CH2CHF2 and CF3CHFCH2F. The process involves (a) reacting hydrogen fluoride, chlorine, and at least one halopropene of the formula CX3CCl═CClX (where each X is independently F or Cl) to produce a product including both CF3CCl2CClF2 and CF3CClFCCl2F; (b) reacting CF3CCl2CClF2 and CF3CClFCCl2F produced in (a) with hydrogen to produce a product including both CF3CH2CHF2, and CF3CHFCH2F; and (c) recovering CF3CH2CHF2 and CF3CHFCH2F from the product produced in (b). In (a), the CF3CCl2CClF2 and CF3CClFCCl2F are produced in the presence of a chlorofluorination catalyst including a ZnCr2O4/crystalline α-chromium oxide composition, a ZnCr2O4/crystalline α-chromium oxide composition which has been treated with a fluorinating agent, a zinc halide/α-chromium oxide composition and/or a zinc halide/α-chromuim oxide composition which has been treated with a fluorinating agent.
摘要翻译：公开了用于制造CF 3 CH 2 CHF 2 2和CF 3 CHFCh 2的方法 F。该方法包括（a）使氟化氢，氯和至少一种式CX 3 CCl-CClX（其中每个X独立地为F或Cl）的卤代丙烯反应，以产生包含CF _{3 CCl 2 CClF 2和CF 3 CClFCCl 2 F; （b）使CF 3 3 CCl 2 CClF 2和CF 3 CClFCCl 2 2和/ （a）中用氢气生产的产物，以产生包含CF 3 3 CH 2 CHF 2 2和CF 3 H 2的产物， 2> CHFCH 2＆lt; 2＆gt; 和（c）回收CF 3 CH 2 CHF 2和CF 3 CHFCH 2}

12. 发明授权

US07285690B2 Process for the preparation of 1,1,1,3,3-pentafluoropropane and 1,1,1,3,3,3-hexafluoropropane 有权
标题翻译：制备1,1,1,3,3-五氟丙烷和1,1,1,3,3,3-六氟丙烷的方法
公开(公告)号：US07285690B2
公开(公告)日：2007-10-23
申请号：US10572627
申请日：2004-10-13
申请人： Velliyur Nott Mallikarjuna Rao , Allen C. Sievert
发明人： Velliyur Nott Mallikarjuna Rao , Allen C. Sievert
IPC分类号： C07C17/00 , C07C17/10
CPC分类号： C07C17/23 , B01J23/002 , B01J23/26 , B01J27/12 , B01J37/26 , B01J2523/00 , C07C17/206 , C07C17/21 , C07C19/08 , C07C21/18 , C07C19/10 , B01J2523/27 , B01J2523/67
摘要： A process for the manufacture of CF3CH2CHF2 and CF3CH2CF3 is disclosed. The process involves (a) reacting HF and at least one halopropene of the formula CX3CCI=CCIX (where each X is independently F or CI) to produce a product including both CF3CCI=CF2 and CF3CHCICF3; (b) reacting CF3CCI=CF2 and CF3CHCICF3 produced in (a) with hydrogen to produce a product including both CF3CH2CHF2 and CF3CH2CF3; and (c) recovering CF3CH2CHF2 and CF3CH2CF3 from the product produced in (b). In (a), the CF3CCI=CF2 and CF3CHCICF3 are produced in the presence of a fluorination catalyst including a ZnCr2O4/crystalline α-chromium oxide composition, a ZnCr2O4/crystalline α-chromium oxide composition which has been treated with a fluorinating agent, a zinc halide/α-chromium oxide composition and/or a zinc halide/α-chromium oxide composition which has been treated with a fluorinating agent.
摘要翻译：用于制备CF 3 CH 2 CHF 2 CH 2和CF 3 CH 2的方法， SUB> CF 3 3 。该方法包括（a）使HF和式CX 3 CCl-CClX（其中每个X独立地为F或Cl）的至少一种卤代丙烯反应，以产生包含CF 3 CCl-CF 2和CF 3 CHClCF 3; （b）使（a）中制备的CF 3 N 3 CCl-CF 2 H 2和CF 3 COClCF 3 N与氢以产生包含CF 3 CH 2 CHF 2 CH 2和CF 3 CH 2 CH 2的化合物， CF 3 3; 和（c）回收CF 3 3 CH 2 CHF 2和CF 3 CH 2 2 / / SUB >（CF 3）3 。在（a）中，CF 3 3 CCl-CF 2 CO 3和CF 3 CHClCF 3 3在存在下产生包含ZnCr 2 O 4 /结晶α-氧化铬组合物的氟化催化剂，ZnCr 2 O 4 O 3 已经用氟化剂处理的结晶α-氧化铬组合物，已经用氟化剂处理的卤化锌/α-氧化铬组合物和/或卤化锌/α-氧化铬组合物。

13. 发明授权

US07354529B2 1,1,1,2,2,3,3,4,4-nonafluro-4-methoxybutane refrigerant compositions comprising hydrofluorocarbon, and uses thereof 失效
标题翻译：包含氢氟烃的1,1,1,2,2,3,3,4,4-非芴-4-甲氧基丁烷制冷剂组合物及其用途
公开(公告)号：US07354529B2
公开(公告)日：2008-04-08
申请号：US11703878
申请日：2007-02-08
申请人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
发明人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/112 , C09K2205/22 , C09K2205/32
摘要： Disclosed herein are refrigerant or heat transfer fluid compositions further comprising fluoroether, 1,1,1,2,2,3,3,4,4-nonafluoro-4-methoxybutane, and hydrofluorocarbon, which are useful in refrigeration or air conditioning apparatus or as heat transfer fluids. The compositions of the present invention are also useful in centrifugal compressor apparatus that employ two-stage compressors or single slab/single pass heat exchangers.
摘要翻译：本文公开的还包含氟代醚，1,1,1,2,2,3,3,4,4-九氟-4-甲氧基丁烷和氢氟烃的制冷剂或传热流体组合物，其可用于制冷或空调设备或作为传热流体。本发明的组合物也可用于使用两级压缩机或单片/单程热交换器的离心式压缩机装置中。

14. 发明授权

US07201855B2 1,1,1,3,3-pentafluorobutane refrigerant compositions comprising fluoroether and uses thereof 失效
标题翻译：包含氟醚的1,1,1,3,3-五氟丁烷制冷剂组合物及其用途
公开(公告)号：US07201855B2
公开(公告)日：2007-04-10
申请号：US11342444
申请日：2006-01-30
申请人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
发明人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/112 , C09K2205/22
摘要： Disclosed herein are 1,1,1,3,3-pentafluorobutane refrigerant or heat transfer fluid compositions further comprising fluoroether, which are useful in refrigerain or air conditioning apparatus or as heat transfer fluids. The compositions of the present invention are also useful in centrifugal compressor apparatus that employ two-stage compressors or single slab single pass heat exchangers.
摘要翻译：本文公开了还包含氟代醚的1,1,1,3,3-五氟丁烷制冷剂或传热流体组合物，其可用于制冷剂或空调设备或作为传热流体。本发明的组合物也可用于使用两级压缩机或单板式单通道热交换器的离心式压缩机装置中。

15. 发明授权

US5523501A Catalytic hydrogenolysis 失效
标题翻译：催化氢解
公开(公告)号：US5523501A
公开(公告)日：1996-06-04
申请号：US362331
申请日：1994-12-22
申请人： Carl S. Kellner , V. N. Mallikarjuna Rao , Allen C. Sievert
发明人： Carl S. Kellner , V. N. Mallikarjuna Rao , Allen C. Sievert
IPC分类号： B01J23/44 , C07B61/00 , C07C17/23 , C07C17/278 , C07C19/08 , C07C17/10
CPC分类号： C07C17/23 , C07C17/278
摘要： A process is disclosed for the catalytic hydrogenolysis of at least one starting material selected from saturated acyclic halofluorocarbons and hydrohalofluorocarbons containing three or four carbon atoms, and from one to five non-fluorine halogens (each non-fluorine halogen being independently chlorine or bromine) wherein all non-fluorine halogen substituents are contained on end carbons. The process involves reacting the starting material with hydrogen at an elevated temperature of about 300.degree. C. or less in the presence of a catalyst containing a catalytically effective amount of palladium supported on carbon to produce a hydrogenolysis product wherein over 80 mole percent of the hydrogenolysis product is a saturated compound having the same distribution of fluorine substituents as the starting material. The carbon support has an ash content of less than about 0.5% by weight.
摘要翻译：公开了用于催化氢解至少一种选自饱和的无环卤代烃和含有三或四个碳原子的氢卤氟烃的起始材料和一至五个非氟卤素（每个非氟卤素独立地是氯或溴）的催化氢解，其中所有非氟卤素取代基都包含在末端碳上。该方法包括在含有催化有效量的负载在碳上的钯的催化剂存在下，在约300℃或更低的升高温度下使起始材料与氢反应以产生氢解产物，其中超过80摩尔％的氢解产物是具有与起始原料相同的氟取代基分布的饱和化合物。碳载体的灰分含量小于约0.5重量％。

16. 发明授权

US07641809B2 Tracer-containing compositions 失效
标题翻译：含示踪剂的组合物
公开(公告)号：US07641809B2
公开(公告)日：2010-01-05
申请号：US11062044
申请日：2005-02-18
申请人： Thomas J. Leck , Stuart C. Bricker , Allen C. Sievert
发明人： Thomas J. Leck , Stuart C. Bricker , Allen C. Sievert
IPC分类号： G01M3/20
CPC分类号： C09K5/045 , C09K5/041 , Y10T436/13
摘要： The present invention relates to the field of compression refrigeration and air conditioning. Specifically, the present invention relates to a tracer-containing compositions comprising refrigeration/heating fluid and tracer compound(s). Additionally, the present invention relates to a method for detecting tracer compounds to identify gases after leaving the custody of the original manufacturer or prior source, and the verification of authenticity. The aforementioned method provides for the detection of tracer compounds, which in turn, may alert the refrigeration industry to when dilution, adulteration, contamination or other unauthorized practices have occurred with refrigeration products.
摘要翻译：本发明涉及压缩制冷和空调领域。具体地，本发明涉及包含制冷/加热流体和示踪剂化合物的含示踪剂组合物。此外，本发明涉及一种用于检测示踪剂化合物在离开原始制造商或先前来源的保管之后识别气体的方法以及真实性的验证。上述方法提供了示踪剂化合物的检测，其又可以警告制冷行业在制冷产品中发生稀释，掺假，污染或其他未经授权的做法时。

17. 发明授权

US5274190A Process for the manufacture of linear hydrofluorocarbons containing end group hydrogen substituents 失效
标题翻译：含有端基氢取代基的直链氢氟烃的制备方法
公开(公告)号：US5274190A
公开(公告)日：1993-12-28
申请号：US66448
申请日：1993-05-24
申请人： Mario J. Nappa , Allen C. Sievert
发明人： Mario J. Nappa , Allen C. Sievert
IPC分类号： C07C17/093 , C07C19/08 , C07C29/32 , C07C49/08 , C07C51/58 , C07C303/24 , C07C305/26 , C07C21/18
CPC分类号： C07C303/24 , C07C17/093 , C07C19/08 , C07C29/32 , C07C49/08 , C07C51/58
摘要： Linear hydrofluorocarbons of the formula XCF.sub.2 (CF.sub.2).sub.n CH.sub.2 F where X is H or F, and n is 1 to 7 when X is H and 0 to 7 when X is F, are produced by a vapor phase catalytic reaction of HF with corresponding compounds of the formula XCF.sub.2 (CF.sub.2).sub.n CH.sub.2 OY where Y is --(CO)Cl or --SO.sub.2 Cl.
摘要翻译：式XCF2（CF2）nCH2F的线性氢氟烃，其中X为H或F，当X为H时，n为1至7，X为F时为n至0，通过HF与相应的化合物式XCF2（CF2）nCH2OY，其中Y是 - （CO）Cl或-SO2Cl。

18. 发明授权

US5274189A Process for the manufacture of linear hydrofluorocarbons containing end group hydrogen substituents 失效
标题翻译：含有端基氢取代基的直链氢氟烃的制备方法
公开(公告)号：US5274189A
公开(公告)日：1993-12-28
申请号：US66367
申请日：1993-05-24
申请人： Mario J. Nappa , Allen C. Sievert
发明人： Mario J. Nappa , Allen C. Sievert
IPC分类号： C07B61/00 , C07C17/093 , C07C17/16 , C07C17/35 , C07C19/08 , C07C19/02
CPC分类号： C07C17/16 , C07C17/093 , C07C17/35
摘要： This invention relates to a process for producing linear hydrofluorocarbons of the formula XCF.sub.2 (CF.sub.2).sub.n CH.sub.2 F, where X is H or F, and n is 1 to 7 when X is H, and n is 0 to 7 when X is F, by a vapor phase catalytic reaction of HF and phosgene or sulfuryl chloride with corresponding compounds of the formula XCF.sub.2 (CF.sub.2).sub.n CH.sub.2 OZ where Z is H or --C(O)OCH.sub.2 (CF.sub.2).sub.n CF.sub.2 X.
摘要翻译：本发明涉及一种制备式XCF2（CF2）nCH2F的线性氢氟烃的方法，其中X为H或F，当X为H时n为1至7，当X为F时n为0至7， HF和光气或磺酰氯与相应的式XCF2（CF2）nCH2OZ化合物的气相催化反应，其中Z是H或-C（O）OCH 2（CF 2）n CF 2 X。

19. 发明授权

US5157171A Process for chlorofluoropropanes 失效
标题翻译：氯氟丙烷工艺
公开(公告)号：US5157171A
公开(公告)日：1992-10-20
申请号：US681564
申请日：1991-04-05
申请人： Allen C. Sievert , Carl G. Krespan , Frank J. Weigert
发明人： Allen C. Sievert , Carl G. Krespan , Frank J. Weigert
IPC分类号： B01J27/125 , C07C17/278 , C07C17/358 , C07C17/395 , C07C19/10
CPC分类号： C07C19/10 , B01J27/125 , C07C17/278 , C07C17/358 , C07C17/395
摘要： A process for the preparation of chlorofluoropropanes of the formula C.sub.3 HCl.sub.2 F.sub.5 by contacting monofluorodichloromethane with tetrafluoroethylene in the presence of a modified aluminum chloride catalyst at a temperature of 0.degree. to 150.degree. C. The novel compound CF.sub.3 CCl.sub.2 CHF.sub.2 is also disclosed.
摘要翻译：在改性氯化铝催化剂存在下，在0℃至150℃的温度下，使单氟二氯甲烷与四氟乙烯接触，制备式C 3 H 2 Cl 2 F 5的氯氟丙烷的方法。还公开了新的化合物CF 3 CCl 2 CHF 2。

20. 发明申请

US20080191162A1 1,1,1,3,3-PENTAFLUOROBUTANE REFRIGERANT OR HEAT TRANSFER FLUID COMPOSITIONS COMPRISING HYDROFLUOROCARBON AND USES THEREOF 审中-公开
标题翻译： 1,1,1,3,3-PENTAFLUOROBUTANE制冷剂或包含氢氟碳化合物的热交换流体组合物及其用途
公开(公告)号：US20080191162A1
公开(公告)日：2008-08-14
申请号：US12050711
申请日：2008-03-18
申请人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
发明人： Barbara Haviland Minor , Mario J. Nappa , Allen C. Sievert
IPC分类号： C09K5/04
CPC分类号： C09K5/045 , C09K2205/112 , C09K2205/22
摘要： Disclosed herein are 1,1,1,3,3-pentafluorobutane refrigerant or heat transfer fluid compositions further comprising hydrofluorocarbon, N-(difluoromethyl)-N,N-dimethylamine, 1,1,1,2,2-pentafluoro-2-[(pentafluoroethyl)thio]ethane or mixtures thereof, which are useful in refrigerain or air conditioning apparatus or as heat transfer fluids. The compositions of the present invention are also useful in centrifugal compressor apparatus that employ two-stage compressors or single slab.single pass heat exchangers.
摘要翻译：本文公开了1,1,1,3,3-五氟丁烷制冷剂或传热流体组合物，其还包含氢氟烃，N-（二氟甲基）-N，N-二甲胺，1,1,1,2,2-五氟-2- 乙醚或其混合物，其可用于制冷剂或空调设备或作为传热流体。本发明的组合物也可用于使用两级压缩机或单片式单通道热交换器的离心式压缩机设备中。

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