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11. 发明授权

US6136970A Asymmetric dioxazine compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：不对称二恶嗪化合物及其染色或印花方法
公开(公告)号：US6136970A
公开(公告)日：2000-10-24
申请号：US967617
申请日：1992-10-29
申请人： Kazufumi Yokogawa , Takahiko Fujisaki , Miyao Takahashi , Shigeru Kawabata , Naoki Harada , Kingo Akahori , Yutaka Kayane , Takashi Omura
发明人： Kazufumi Yokogawa , Takahiko Fujisaki , Miyao Takahashi , Shigeru Kawabata , Naoki Harada , Kingo Akahori , Yutaka Kayane , Takashi Omura
IPC分类号： C07D265/34 , C09B19/00 , C09B62/002 , C09B62/02 , C09B62/44 , C09B62/503 , C07D498/04
CPC分类号： C09B62/5033 , C09B62/0025 , C09B62/021 , C09B62/4405
摘要： An asymmetric dioxazine compound represented by the following formula (I) in the free acid form: ##STR1## wherein A.sub.1 and A.sub.2 independently of one another are each sulfo, halo, alkyl or alkoxy, X.sub.1 and X.sub.2 independently of one another are each hydrogen, halo, alkyl, alkoxy or phenoxy, R.sub.1 is hydrogen or unsubstituted or substituted alkyl, R.sub.2 and R.sub.3 independently of one another are each hydrogen, alkyl, alkoxy, halo or unsubstituted or substituted amino, Z is a fiber-reactive group, m and n independently of one another are each 0 or 1, provided that m.noteq.n, and L is 1 or 2. This compound is suitable for dyeing and printing cellulose fiber, natural and synthetic polyamide fibers, polyurethane fiber, leather and the like and mixed yarns thereof, to obtain dyed or printed products of a color fast to light, wetness and chlorine with superior build-up and level dyeing properties.
摘要翻译：由游离酸形式的下式（I）表示的不对称二嗪类化合物：其中A1和A2彼此独立地各自为磺基，卤素，烷基或烷氧基，X 1和X 2彼此独立地为氢，卤素，烷基，烷氧基或苯氧基，R 1是氢或未取代或取代的烷基，R 2和R 3彼此独立地各自为氢，烷基，烷氧基，卤素或未取代或取代的氨基，Z为纤维反应性基团，m和n独立地为一个另外每个都为0或1，条件是m注意n和L为1或2.该化合物适用于将纤维素纤维，天然和合成聚酰胺纤维，聚氨酯纤维，皮革等及其混合纱线染色和印刷到获得染色或印刷的产品，颜色快速到轻，湿和氯，具有优异的积聚和水平的染色性能。

12. 发明授权

US5438137A Fiber reactive asymmetric dioxazine compounds and their use as fiber reactive dyes 失效
标题翻译：纤维反应性不对称二嗪化合物及其作为纤维活性染料的用途
公开(公告)号：US5438137A
公开(公告)日：1995-08-01
申请号：US128725
申请日：1993-09-30
申请人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura , Naoki Harada
发明人： Tetsuya Miyamoto , Miyao Takahashi , Takahiko Fujisaki , Shinei Ikeou , Takashi Omura , Naoki Harada
IPC分类号： C09B62/44 , C09B62/503 , C07D498/04
CPC分类号： C09B62/5033 , C09B62/4405
摘要： An asymmetric dioxazine compound of the following formula in the free acid form, ##STR1## wherein R is hydrogen, halogen, sulfo or alkoxy, R.sub.1, R.sub.2 and R.sub.3 are each hydrogen or alkyl, X.sub.1 and X.sub.2 are each hydrogen, halogen, alkyl, alkoxy or phenoxy, Y is alkylene, phenylene or naphthylene, Z is --SO.sub.2 CH.dbd.CH.sub.2, --SO.sub.2 CH.sub.2 CH.sub.2 OSO.sub.3 H or the like, V is hydrogen, alkyl, acyl or substituted triazinyl, and Q is halogen, alkoxy, amino or a group similar to that of ##STR2## provided that R is hydrogen, and Q is amino or a group similar to that of ##STR3## when V is substituted triazinyl, which is useful for dyeing or printing fiber materials to give dyed or printed products of a brilliant blue color superior in fastness properties, particularly those such as chlorine fastness with superior build-up property.
摘要翻译：游离酸形式的下式的不对称二恶嗪化合物，其中R是氢，卤素，磺基或烷氧基，R 1，R 2和R 3各自为氢或烷基，X 1和X 2各自为氢，卤素，烷基，烷氧基或苯氧基，Y是亚烷基，亚苯基或亚萘基，Z是-SO2CH = CH2，-SO2CH2CH2OSO3H等，V是氢，烷基，酰基或取代的三嗪基，Q是卤素，烷氧基，氨基或类似的基团条件是R为氢，Q为氨基或V为与IMA相似的基团，当V为取代的三嗪基时，可用于染色或印刷纤维材料以得到亮蓝色的染色或印刷产品耐牢度特性优异，特别是具有优异聚集性能的耐氯牢度。

13. 发明授权

US5324329A Reactive dye composition and dyeing or printing process using the same 失效
标题翻译：活性染料组合物和染色或印刷方法使用相同
公开(公告)号：US5324329A
公开(公告)日：1994-06-28
申请号：US76962
申请日：1993-06-16
申请人： Takeshi Washimi , Naoki Harada , Shuhei Hashizume , Takashi Omura
发明人： Takeshi Washimi , Naoki Harada , Shuhei Hashizume , Takashi Omura
IPC分类号： C09B67/24 , C09B62/44 , C09B67/22 , D06P1/384 , D06P3/66 , C09B62/00
CPC分类号： C09B67/0052 , C09B62/4413 , Y10S8/918
摘要： A reactive dye composition containing at least one dye of the formula (I) in the free acid form: ##STR1## wherein m is zero or 1; R.sub.1 is hydrogen, lower alkyl or lower alkoxy; R.sub.2 and R.sub.3 are independently hydrogen or substituted or unsubstituted lower alkyl; A is substituted or unsubstituted phenylene or naphthylene; X.sub.1 is halogen, --N(R.sub.4)R.sub.5 or --OR.sub.6 in which R.sub.4, R.sub.5 and R.sub.6 are independently hydrogen or substituted or unsubstituted alkyl, phenyl or naphthyl; and Y.sub.1 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.1 in which Z.sub.1 is a group splittable by the action of an alkali, and at least one dye of the formula (II) in the free acid form: ##STR2## wherein n is zero, 1 or 2; one of W.sub.1 and W.sub.2 is hydrogen and the other is sulfo; R.sub.7 is hydrogen or substituted or unsubstituted lower alkyl; B is substituted or unsubstituted phenylene or naphthylene; X.sub.2 is --N(R.sub.8)R.sub.9, --OR.sub.10 in which R.sub.8, R.sub.9 and R.sub.10 are independently hydrogen or substituted or unsubstituted alkyl, phenyl, naphthyl, pyridinio, morpholino or piperidino; and Y.sub.2 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.2 in which Z.sub.2 is a group splittable by the action of an alkali, dyes or prints cellulose fiber materials or fiber materials containing a cellulose fiber to give a vivid, deep and highly fast red color.
摘要翻译：含有游离酸形式的至少一种式（I）染料的活性染料组合物：其中m为0或1; R1是氢，低级烷基或低级烷氧基; R2和R3独立地为氢或取代或未取代的低级烷基; A是取代或未取代的亚苯基或亚萘基; X 1是卤素，-N（R 4）R 5或-OR 6，其中R 4，R 5和R 6独立地是氢或取代或未取代的烷基，苯基或萘基; Y1是基团-SO2CH = CH2或基团-SO2CH2CH2Z1，其中Z1是可以通过碱作用而分裂的基团，以及至少一种游离酸形式的式（II）染料：II ）其中n为0,1或2; W1和W2之一是氢，另一个是磺基; R7是氢或取代或未取代的低级烷基; B是取代或未取代的亚苯基或亚萘基; X 2是-N（R 8）R 9，-OR 10，其中R 8，R 9和R 10独立地是氢或取代或未取代的烷基，苯基，萘基，吡啶基，吗啉代或哌啶子基; 并且Y2是基团-SO 2 CH = CH 2或基团-SO 2 CH 2 CH 2 Z 2，其中Z 2是可以通过碱的作用而分裂的基团，染料或印刷含纤维素纤维的纤维素纤维材料或纤维材料，以产生生动，深度和高度快速红色。

14. 发明授权

US4910298A Monoazo compound having triazinyl bridging group and two vinylsulfone type fiber reactive groups imparting yellowish color 失效
标题翻译：具有三嗪基桥连基团的单偶氮化合物和赋予淡黄色的两个乙烯基砜类纤维反应性基团
公开(公告)号：US4910298A
公开(公告)日：1990-03-20
申请号：US116147
申请日：1987-11-03
申请人： Kazufumi Yokogawa , Sadanobu Kikkawa , Naoki Harada , Takashi Omura
发明人： Kazufumi Yokogawa , Sadanobu Kikkawa , Naoki Harada , Takashi Omura
IPC分类号： C09B62/51 , D06P1/38 , D06P1/384
CPC分类号： C09B62/51
摘要： A monoazo compound of the following formula, ##STR1## wherein D is sulfonaphthyl, sulfophenyl or carboxyphenyl, any one of A.sub.1 and A.sub.2 is sulfo and the other is hydrogen, methoxy or ethoxy, R.sub.1 and R.sub.2 are independently hydrogen or alkyl, B.sub.1 and B.sub.2 are independently phenylene or naphthylene, and Y.sub.1 and Y.sub.2 are independently vinyl, .beta.-sulfatoethyl or the like, which is useful for dyeing or printing fiber materials to give dyed or printed products of a deep color excellent in fastness properties.

15. 发明授权

US4530996A Bisazo blue-black dye having vinylsulfone type fiber-reactive group 失效
标题翻译：具有乙烯基砜型纤维反应性基团的双偶氮蓝黑色染料
公开(公告)号：US4530996A
公开(公告)日：1985-07-23
申请号：US384889
申请日：1982-06-04
申请人： Takashi Omura , Naoki Harada , Yasuo Tezuka
发明人： Takashi Omura , Naoki Harada , Yasuo Tezuka
IPC分类号： C09B62/513 , C09B62/503 , D06P1/38 , D06P3/66
CPC分类号： C09B62/513
摘要： A compound represented by a free acid of the formula: ##STR1## wherein D is ##STR2## (R.sub.1 and R.sub.2 independently represent hydrogen, methyl or methoxy) or ##STR3## (n is 0 or 1, the mark * signifies the position of linkage to --N.dbd.N-- and the mark # signifies the position of linkage to Q mentioned below); Q is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 R (R is a group capable of being split off by the action of alkali); one of X.sub.1 and X.sub.2 is hydrogen and the other is a sulfonic acid group; and m is 0 or 1, which is useful for dyeing cellulose fibers a blue-black color with good dyeability and excellent fastnesses, particularly chlorine fastness.
摘要翻译：由下式的游离酸表示的化合物：其中D为（R 1和R 2独立地表示氢，甲基或甲氧基）或（n为0或1，标记*表示连接到-N = N-，标记＃表示与下述Q的连接位置）; Q是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 R（R是能够被碱的作用分解的基团）; X1和X2之一是氢，另一个是磺酸基; m为0或1，可用于染色纤维素纤维，染色性能好，耐牢牢度优异的蓝黑色。

16. 发明授权

US4505714A Phthalocyanine fiber reactive compound 失效
标题翻译：酞菁纤维反应性化合物
公开(公告)号：US4505714A
公开(公告)日：1985-03-19
申请号：US579546
申请日：1984-02-13
申请人： Takashi Omura , Mikoto Takahashi , Naoki Harada , Akira Takeshita
发明人： Takashi Omura , Mikoto Takahashi , Naoki Harada , Akira Takeshita
IPC分类号： C09B47/26 , C09B62/44 , C09B62/517 , D06P1/38 , D06P3/66 , C09B62/51
CPC分类号： C09B62/4418 , Y10S8/917 , Y10S8/918 , Y10S8/924 , Y10S8/926
摘要： A phthalocyanine compound which is represented by a free acid of the following formula, ##STR1## wherein Pc is a metal-free or metal-containing phthalocyanine residue, W is a group of ##STR2## in which R' and R" are independently a hydrogen atom or a methyl or ethyl group, and n is an integer of from 2 to 6, R is an unsubstituted or substituted lower alkyl group, A is an unsubstituted or substituted phenylene or naphthylene group, Y is a group of --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z in which Z is a group capable of being split by the action of an alkali, a is a positive number of from 1 to 3, and b and c are independently a positive number of from 0 to 3, provided that a, b and c statisfy 0
摘要翻译：由下式的游离酸表示的酞菁化合物，其中Pc是不含金属或含金属的酞菁残基，W是其中R'和R“独立地为”IMAGE“的基团氢原子或甲基或乙基，n为2〜6的整数，R为未取代或取代的低级烷基，A为未取代或取代的亚苯基或亚萘基，Y为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Z，其中Z是能够被碱作用的基团，a是1至3的正数，b和c独立地为0至3的正数，条件是a ，b和c统计0 ，可用于染色或印刷纤维材料，特别是纤维素纤维材料，以得到具有优异的各种坚牢度的辉煌绿松石蓝色的染色或印刷产品，特别是耐光牢度和耐湿牢度。

17. 发明授权

US5266696A 1-aminoanthraquinone dye compound having fiber reactive group through sulfur or oxygen atom at 4-position and imparting red color 失效
标题翻译：具有纤维反应性基团的1-氨基蒽醌染料化合物，通过硫或氧原子在4位上赋予红色
公开(公告)号：US5266696A
公开(公告)日：1993-11-30
申请号：US836825
申请日：1992-02-19
申请人： Kingo Akahori , Naoki Harada , Yutaka Kayane , Takashi Omura
发明人： Kingo Akahori , Naoki Harada , Yutaka Kayane , Takashi Omura
IPC分类号： C09B62/024 , C09B62/44 , C09B62/505 , C07D251/70 , C09B62/06 , D06P1/382 , D06P1/384
CPC分类号： C09B62/024 , C09B62/4409 , C09B62/505
摘要： Anthraquinone compounds of the formula, ##STR1## wherein R is hydrogen, alkyl or the like, R.sub.1 and R.sub.2 are each hydrogen, halogen or sulfo, l is 1 or 2, X is sulfo or the like or --V--A--(W).sub.m --Z, and Y is --V.sub.1 --A.sub.1 --U, wherein V and V.sub.1 are each --O-- or --S--, A and A.sub.1 are each a divalent group such as ##STR2## W is --NH-- or the like, Z is hydrogen or a fiber reactive group, and U is hydrogen, a fiber reactive group or a fiber reactive group-containing group, provided that at least one of Z and U is or has a fiber reactive group, which is useful for dyeing or printing fiber materials such as cotton to give a dyed or printed product having excellent fastness properties, particularly those such as light fastness and perspiration-light fastness.
摘要翻译：下式的蒽醌化合物，其中R是氢，烷基等，R 1和R 2各自为氢，卤素或磺基，l为1或2，X为磺基等或-VA-（W）mZ ，Y为-V1-A1-U，其中V和V1各自为-O-或-S-，A和A1各自为二价基团，例如W为-NH-等，Z为氢或纤维反应性基团，U为氢，纤维反应性基团或含纤维反应性基团，条件是Z和U中的至少一个为或具有纤维反应性基团，其可用于染色或印刷纤维材料例如棉，以得到具有优异坚牢性的染色或印刷产品，特别是耐光牢度和耐汗牢度等。

18. 发明授权

US4880434A Method of obtaining dyed and finished cellulose fiber materials using reactive metallized formazan dye with no color change 失效
标题翻译：使用无颜色变化的反应性金属化甲an染料获得染色和成品纤维素纤维材料的方法
公开(公告)号：US4880434A
公开(公告)日：1989-11-14
申请号：US217631
申请日：1988-07-12
申请人： Naoki Harada , Tetsuya Miyamoto , Kunihiko Imada , Takashi Omura
发明人： Naoki Harada , Tetsuya Miyamoto , Kunihiko Imada , Takashi Omura
IPC分类号： C09B62/503 , D06P3/66 , D06P5/08
CPC分类号： D06P3/66 , C09B62/5036 , D06P5/08 , Y10S8/918
摘要： Dyed and finished products of cellulose fiber materials superior in fastness properties are obtained without change in color shade by finishing dyed products with a fixing agent or/and a finishing agent capable of bonding with cellulose through a bridge formation, the dyed products being obtained by dyeing cellulose fiber materials with a dye represented by the following formula in the free acid form, ##STR1## wherein A is phenylene or naphthylene, B is alkyl, alkenyl, phenyl, naphthyl or heterocyclic group, Me is metal ion, X is --O-- or ##STR2## Y is alkoxy, phenoxy or amino, Z is sulfo or the like water-solubility-imparting group, m and n are each 0 or an integer of 1 to 3, provided that the sum is 1 to 3, D is phenylene or naphthylene, Q is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 L in which L is splittable group by the action of an alkali and R is hydrogen or alkyl.
摘要翻译：通过用能够通过桥接形成与纤维素结合的固色剂或/和整理剂对染色产物进行染色，可以获得色牢度优异的纤维素纤维材料的染色和成品而不变色，染色产品通过染色具有游离酸形式的下式表示的染料的纤维素纤维材料，其中A是亚苯基或亚萘基，B是烷基，烯基，苯基，萘基或杂环基，Me是金属离子，X是 -O-或Y是烷氧基，苯氧基或氨基，Z是磺基等水溶性赋予基团，m和n各自为0或1〜3的整数，条件是总和为1〜3 ，D是亚苯基或亚萘基，Q是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 L，其中L是可分裂的基团，R是氢或烷基。

19. 发明授权

US4841048A Dioxazine compound having vinylsulfone type fiber reactive group 失效
标题翻译：具有乙烯基砜型纤维反应性基团的二恶嗪化合物
公开(公告)号：US4841048A
公开(公告)日：1989-06-20
申请号：US125745
申请日：1987-11-19
申请人： Hirokazu Sawamoto , Takashi Omura , Naoki Harada
发明人： Hirokazu Sawamoto , Takashi Omura , Naoki Harada
IPC分类号： C09B19/00 , C07D498/04 , C09B62/44 , C09B62/503 , D06P1/384 , D06P3/66
CPC分类号： C09B62/4405
摘要： A dioxazine compound of the formula, ##STR1## wherein A is a divalent group of the formula, ##STR2## in which * and ** denote linkages to the adjacent nitrogen and oxygen atoms, respectively, or the divalent group-containing 3- to 5-condensed aromatic ring residue, R is a substituent such as amino, cyano, nitro, halogeno and the like, V is --SO.sub.2 NR.sub.5 - or the like in which R.sub.5 is hydrogen or the like, X is aliphatic, alicyclic, araliphatic or aromatic divalent group, Y is phenylene or naphthylene, Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.1 in which Z.sub.1 is a splittable group, Q is halogeno, amino or the like, R.sub.1 and R.sub.2 are each hydrogen or alkyl, and O
摘要翻译：下式的二嗪嗪化合物，其中A是下式的二价基团，其中*和**分别表示与相邻的氮原子和氧原子的连接，或含二价基团的 3-至5-稠合芳环残基，R为氨基，氰基，硝基，卤代等取代基，V为-SO 2 NR 5 - 等，其中R 5为氢等，X为脂族，脂环族，芳烷基或芳族二价基团，Y为亚苯基或亚萘基，Z为-SO2CH = CH2或-SO2CH2CH2Z1，其中Z1为可裂解基团，Q为卤素，氨基等，R1和R2各自为氢或烷基， l + m + n = 6，条件是O

20. 发明授权

US4464297A Fiber reactive bisazo dye having both a vinylsulfone type reactive group and an ortho-nitrophenyl group 失效
标题翻译：具有乙烯基砜型反应性基团和邻位硝基苯基的纤维反应性双偶氮染料
公开(公告)号：US4464297A
公开(公告)日：1984-08-07
申请号：US398223
申请日：1982-07-14
申请人： Takashi Omura , Naoki Harada , Yasuo Tezuka
发明人： Takashi Omura , Naoki Harada , Yasuo Tezuka
IPC分类号： C09B62/513 , C09B62/533 , D06P1/384 , D06P3/66
CPC分类号： C09B62/513
摘要： A bisazo reactive compound represented by a free acid of the formula, ##STR1## wherein X is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 R (R is a group capable of being split off with an alkali); Y is phenylene group or naphthylene group, said phenylene group being unsubstituted or substituted by 1-3 identical or different substituent(s) selected from C.sub.1-C.sub.4 alkyl groups, C.sub.1 -C.sub.4 alkoxy groups, chlorine atom and bromine atom, and said naphthylene group being unsubstituted or substituted by 1-3 sulfonic acid group(s); and Z is hydrogen atom, halogen atom, nitro group, cyano group, C.sub.1 -C.sub.4 alkyl group or C.sub.1 -C.sub.4 alkoxy group. The compound is useful for dyeing cellulose, polyamide or polyurethane fibers in a blue-black color having excellent fastnesses, particularly chlorine fastness, and excellent built-up property.
摘要翻译：由下式的游离酸表示的双偶氮反应性化合物，其中X为-CH = CH 2或-CH 2 CH 2 R（R为可与碱分离的基团）。 Y是亚苯基或亚萘基，所述亚苯基是未取代的或被1-3个相同或不同的选自C 1 -C 4烷基，C 1 -C 4烷氧基，氯原子和溴原子的取代基取代，所述亚萘基未被取代或被1-3个磺酸基团取代; Z为氢原子，卤原子，硝基，氰基，C1-C4烷基或C1-C4烷氧基。该化合物可用于染色具有优异坚牢度，特别是耐氯牢度的蓝黑色的纤维素，聚酰胺或聚氨酯纤维，并且具有优异的组合性。

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