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11. 发明授权

US5175336A Fluoromethylated polycyanobenzenes, their alkali metal cyanide adducts, processes for their preparation and use of the fluoromethylated polycyanobenzenes 失效
标题翻译：氟代金刚烷基多胺，其碱金属氰化物助剂，其制备和使用氟代聚亚烷基苯甲酸的方法
公开(公告)号：US5175336A
公开(公告)日：1992-12-29
申请号：US701540
申请日：1991-05-16
申请人： Gunther Beck , Wolfgang von der Emden , Helmut Heitzer , Friedrich W. Krock , Ernst Kysela , Albrecht Marhold
发明人： Gunther Beck , Wolfgang von der Emden , Helmut Heitzer , Friedrich W. Krock , Ernst Kysela , Albrecht Marhold
IPC分类号： C07C253/14 , C07C253/30 , C07C255/51 , G01N21/64 , G01N31/22
CPC分类号： C07C255/51 , G01N2021/7786
摘要： The invention relates to new fluoromethylated polycyanobenzenes of the formula ##STR1## in which X represents hydrogen, fluorine or chlorine,m is 1 or 2 andn is (6-m),to a process for their preparation and to the salt-like alkali metal cyanide adducts of the fluoromethylated polycyanobenzenes formed as intermediates in this preparation process and to the use of the fluoromethylated polycyanobenzenes for the detection of anions.
摘要翻译：本发明涉及式（I）的新的氟甲基化聚氰化苯，其中X代表氢，氟或氯，m为1或2，n为（6-m），其制备方法和盐在该制备方法中作为中间体形成的氟甲基化聚氰基苯类似的碱金属氰化物加合物，以及氟甲基化聚氰基苯用于检测阴离子的用途。

12. 发明授权

US4732711A Herbicidal novel 1-(2-trifluoromethoxy-phenylsulphonyl)-3-heteroaryl-(thio)ureas 失效
标题翻译：除草新型1-（2-三氟甲氧基 - 苯基磺酰基）-3-杂芳基 - （硫代）脲
公开(公告)号：US4732711A
公开(公告)日：1988-03-22
申请号：US868962
申请日：1986-05-30
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
IPC分类号： A01N47/36 , C07C311/65 , C07C331/32 , C07D239/42 , C07D239/46 , C07D251/16 , C07D251/18 , C07D251/22 , C07D251/46 , C07D253/06 , C07D257/08 , C07D521/00 , C07C154/00 , C07D251/02
CPC分类号： C07D521/00 , A01N47/36 , C07C311/65 , C07C331/32
摘要： 1-(2-Trifluoromethoxy-phenylsulphonyl)-3-heteroaryl-(thio)urea herbicides of the formula ##STR1## in which Q represents oxygen or sulphur,R.sup.1 represents hydrogen, C.sub.1 -C.sub.4 -alkyl or benzyl,R.sup.2 represents hydrogen, halogen, hydroxyl, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -halogenoalkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -halogenoalkoxy, C.sub.1 -C.sub.4 -alkylthio, C.sub.1 -C.sub.4 -halogenoalkylthio, amino, C.sub.1 -C.sub.4 -alkylamino or di-(C.sub.1 -C.sub.4 -alkyl)-amino,X represents nitrogen or a --CH-- grouping,Y represents nitrogen or a --CR.sup.3 -- grouping,whereinR.sup.3 represents hydrogen, halogen, C.sub.1 -C.sub.4 -alkyl, (C.sub.1 -C.sub.2 -alkyl)-carbonyl or (C.sub.1 -C.sub.2 -alkoxy)-carbonyl, andZ represents nitrogen or a --CR.sup.4 -- grouping,whereinR.sup.4 represents hydrogen, halogen, hydroxyl, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, C.sub.1 -C.sub.4 -alkylthio, C.sub.1 -C.sub.4 -alkylamino or di-(C.sub.1 -C.sub.4 -alkyl)-amino.
摘要翻译：其中Q代表氧或硫，R1代表氢，C1-C4-烷基或苄基，R2代表氢，卤素的1-（2-三氟甲氧基 - 苯基磺酰基）-3-杂芳基 - （硫代）脲除草剂，羟基，C 1 -C 4烷基，C 1 -C 4卤代烷基，C 1 -C 4 - 烷氧基，C 1 -C 4卤代烷氧基，C 1 -C 4 - 烷硫基，C 1 -C 4卤代烷硫基，氨基，C 1 -C 4烷基氨基或二 C 1 -C 4烷基） - 氨基，X表示氮或-CH-基团，Y表示氮或-CR 3 - 基团，其中R 3表示氢，卤素，C 1 -C 4 - 烷基，（C 1 -C 2-烷基）羰基或（C1-C2-烷氧基） - 羰基，Z表示氮或-CR4-基团，其中R4表示氢，卤素，羟基，C1-C4-烷基，C1-C4-烷氧基，C1-C4-烷硫基， C 1 -C 4 - 烷基氨基或二 - （C 1 -C 4 - 烷基） - 氨基。

13. 发明授权

US4990661A Process for the preparation of benzoic acid derivatives 失效
标题翻译：苯甲酸衍生物的制备方法
公开(公告)号：US4990661A
公开(公告)日：1991-02-05
申请号：US330396
申请日：1989-03-29
申请人： Uwe Petersen , Michael Schriewer , Ernst Kysela , Klaus Grohe
发明人： Uwe Petersen , Michael Schriewer , Ernst Kysela , Klaus Grohe
IPC分类号： C07C63/72 , C07C51/363 , C07C51/60 , C07C63/00 , C07C63/70 , C07C67/00 , C07C227/00 , C07C229/60
CPC分类号： C07C51/363 , C07C51/60
摘要： A process for the preparation of a compound of the formula ##STR1## in which X.sup.1 and X.sup.2 each independently is chlorine or fluorine, andY is chlorine, bromine, fluorine or iodine, comprising subjecting a compound of the formula ##STR2## to a Sandmeyer or Balz-Schiemann reaction thereby to produce a carboxylic acid of the formula ##STR3## and converting the carboxylic acid (Ia) into an acyl chloride of the formula ##STR4## The compound (II) is new. The products are known intermediates for anti-bacterials.

14. 发明授权

US4990637A 1-benzylsulphonyl-3-heteroaryl-(thio)urea herbicides 失效
标题翻译： 1-苄基磺酰基-3-杂芳基 - （硫代）脲除草剂
公开(公告)号：US4990637A
公开(公告)日：1991-02-05
申请号：US472520
申请日：1990-01-30
申请人： Christa Fest , Klaus-Helmut Muller , Theodor Pfister , Hans-Jochem Riebel , Ernst Kysela , Hans-Joachim Santel , Robert R. Schmidt , Robert H. Strang
发明人： Christa Fest , Klaus-Helmut Muller , Theodor Pfister , Hans-Jochem Riebel , Ernst Kysela , Hans-Joachim Santel , Robert R. Schmidt , Robert H. Strang
IPC分类号： C07D251/16 , A01N47/36 , C07C41/00 , C07C43/225 , C07C67/00 , C07C301/00 , C07C303/02 , C07C303/38 , C07C311/65 , C07C325/00 , C07C331/16 , C07D239/42 , C07D239/47 , C07D239/48 , C07D239/52 , C07D251/18 , C07D251/22 , C07D251/42 , C07D251/46 , C07D251/52 , C07D253/06 , C07D521/00
CPC分类号： C07D521/00 , A01N47/36 , C07C43/225
摘要： Herbicidally active novel substituted 1-benzylsulphonyl-3-heteroaryl(thio)-ureas of the formula ##STR1## in whichQ.sub.1 represents oxygen or sulphur,R.sup.1 represents hydrogen, or represents optionally substituted radicals from the series comprising alkyl, alkenyl, alkynyl and aralkyl,R.sup.2 represents hydrogen, halogen, hydroxyl, alkyl, halogenoalkyl, alkoxy, halogenoalkoxy, alkylthio, halogenoalkylthio, amino, alkylamino or dialkylamino,R.sup.3 represents hydrogen or alkyl,R.sup.4 represents halogenoalkyl,X represents nitrogen or a --CH grouping,Y represents nitrogen or a --CR.sup.5 grouping,R.sup.5 represents hydrogen, halogen, cyano, alkyl, formyl, alkyl-carbonyl or alkoxy-carbonyl,Z represents nitrogen or a --CR.sup.6 grouping, andR.sup.6 represents hydrogen, halogen, hydroxyl, alkyl, halogenoalkyl, alkoxy, halogenoalkoxy, alkylthio, alkylamino or dialkylamino,and salts thereof with metals and basic organic nitrogen compounds. The benzylsulphonyl moieties are also new.

15. 发明授权

US4780126A 3-substituted 1-(2-halogenoalkoxy-benzenesulphonyl)-3-heteroaryl-(thio)ureas 失效
标题翻译： 3-取代的1-（2-卤代烷氧基 - 苯磺酰基）-3-杂芳基 - （硫代）脲
公开(公告)号：US4780126A
公开(公告)日：1988-10-25
申请号：US060187
申请日：1987-06-09
申请人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
发明人： Hans-Joachim Diehr , Christa Fest , Rolf Kirsten , Joachim Kluth , Klaus-Helmut Muller , Theodor Pfister , Uwe Priesnitz , Hans-Jochem Riebel , Wolfgang Roy , Hans-Joachim Santel , Robert R. Schmidt , Ludwig Eue , Ernst Kysela
IPC分类号： A01N47/36 , C07C311/65 , C07C331/32 , C07D521/00 , C07D251/42 , A01N43/66 , C07D251/46
CPC分类号： C07D521/00 , A01N47/36 , C07C311/65 , C07C331/32
摘要： 3-Substituted 1-(2-halogenoalkoxy-benzenesulphonyl)-3-heteroaryl-(thio)urea herbicides of the formula ##STR1## in which (A)R is CF.sub.3,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3, OC.sub.2 H.sub.5, SCH.sub.3, NH--CH.sub.3 or NH--C.sub.2 H.sub.5,X is N,Y is N andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(B)R is CF.sub.3,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3 or OC.sub.2 H.sub.5,X is N,Y is C--H andZ is C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(C)R is CH.sub.2 --CH.sub.2 Cl,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3, OC.sub.2 H.sub.5, SCH.sub.3, NH--CH.sub.3 or NH--C.sub.2 H.sub.5,X is N,Y is N andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(D)R is CH.sub.2 --CH.sub.2 Cl,Q is O,R.sup.1 is CH.sub.3, C.sub.2 H.sub.5, C.sub.3 H.sub.7 -n, C.sub.3 H.sub.7 -i, CH.sub.2 --CH.dbd.CH.sub.2, CH.sub.2 --C.tbd.CH or CH.sub.2 --C.sub.6 H.sub.5,R.sup.2 is CH.sub.3, OCH.sub.3 or OC.sub.2 H.sub.5,X is N,Y is C--H andZ is C--CH.sub.3, C--C.sub.2 H.sub.5, C--OCH.sub.3 or C--OC.sub.2 H.sub.5 ; or(E)R is CHF.sub.2,Q is O,R.sup.1 is CH.sub.3,R.sup.2 is CH.sub.3,X is N,Y is N andZ is C--CH.sub.3,or a salt thereof with a metal or basic organic nitrogen compound.
摘要翻译：（A）R为CF 3，Q为O，R 1为CH 3，C 2 H 5，C 3 H 7 -n的3-取代的1-（2-卤代烷氧基 - 苯磺酰基）-3-杂芳基 - （硫代）脲除草剂，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3，OC 2 H 5，SCH 3，NH-CH 3或NH-C 2 H 5，X是N，Y是N，Z是C -CH 3，C-C 2 H 5，C-OCH 3或C-OC 2 H 5; 或（B）R是CF 3，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7-i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3或OC 2 H 5， X是N，Y是CH，Z是C-C 2 H 5，C-OCH 3或C-OC 2 H 5; 或（C）R是CH 2 -CH 2 Cl，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3， OC2H5，SCH3，NH-CH3或NH-C2H5，X是N，Y是N，Z是C-CH3，C-C2H5，C-OCH3或C-OC2H5; 或（D）R是CH 2 -CH 2 Cl，Q是O，R 1是CH 3，C 2 H 5，C 3 H 7-n，C 3 H 7 -i，CH 2 -CH = CH 2，CH 2 -C 3 CH 2或CH 2 -C 6 H 5，R 2是CH 3，OCH 3或 OC2H5，X是N，Y是CH，Z是C-CH3，C-C2H5，C-OCH3或C-OC2H5; 或（E）R是CHF 2，Q是O，R 1是CH 3，R 2是CH 3，X是N，Y是N，Z是C-CH 3，或其与金属或碱性有机氮化合物的盐。

16. 发明授权

US4329458A Process for the preparation of 2,4,6-trifluoro-1,3,5-triazine 失效
标题翻译：制备2,4,6-三氟-1,3,5-三嗪的方法
公开(公告)号：US4329458A
公开(公告)日：1982-05-11
申请号：US238328
申请日：1981-02-26
申请人： Erich Klauke , Ernst Kysela , Arnd Stuwe , Alfons Dorlars
发明人： Erich Klauke , Ernst Kysela , Arnd Stuwe , Alfons Dorlars
IPC分类号： C07B61/00 , C07D251/28
CPC分类号： C07D251/28
摘要： The present invention relates to a process for the preparation of 2,4,6-trifluoro-1,3,5-triazine (TFT) from 2,4,6-trichloro-1,3,5-triazine (TCT) or from mixed chlorinated/fluorinated 1,3,5-triazines by fluorination with sodium fluoride in dipolar aprotic solvents.The process is characterized in that TCT or mixed chlorinated/fluorinated 1,3,5-triazines or mixtures thereof are metered into a suspension of sodium fluoride in a dipolar, aprotic solvent, which is warmed to a temperature of between 120.degree. C. and 220.degree. C. and optionally contains a further solvent.
摘要翻译：本发明涉及从2,4,6-三氯-1,3,5-三嗪（TCT）制备2,4,6-三氟-1,3,5-三嗪（TFT）或从混合氯化/氟化1,3,5-三嗪通过氟化氟化物在偶极非质子溶剂中氟化。该方法的特征在于将TCT或混合氯化/氟化1,3,5-三嗪或其混合物计量加入到氟化钠在偶极非质子溶剂中的悬浮液中，将其温热至120℃至 220℃，任选地含有另外的溶剂。

17. 发明授权

US4956370A Antimycotically active substituted 2-aminothiazoles 失效
标题翻译：抗真菌活性取代的2-氨基噻唑
公开(公告)号：US4956370A
公开(公告)日：1990-09-11
申请号：US419981
申请日：1989-10-11
申请人： Joachim Ippen , Bernd Baasner , Albrecht Marhold , Ernst Kysela , Klaus Schaller , Miklos von Bittera
发明人： Joachim Ippen , Bernd Baasner , Albrecht Marhold , Ernst Kysela , Klaus Schaller , Miklos von Bittera
IPC分类号： A61K31/505 , A61P31/04 , C07C45/00 , C07C45/46 , C07C45/63 , C07C45/71 , C07C49/84 , C07C205/37 , C07C205/38 , C07D417/12
CPC分类号： C07D417/12 , C07C205/37 , C07C205/38 , C07C45/00 , C07C45/004 , C07C45/46 , C07C45/63 , C07C45/71 , C07C49/84
摘要： A 2-aminothiazole of the formula ##STR1## in which R.sup.1 represents hydrogen or alkyl andR.sup.2 represents a radical of the formula ##STR2## where R.sup.3, R.sup.4, R.sup.5 and R.sup.6 independently of one another in each case represent hydrogen, halogen, nitro, alkyl, alkoxy, alkoxycarbonyl, dialkylamino, alkylthio, alkylsulphinyl, alkylsulphonyl, halogenoalkyl, halogenoalkoxy, halogenoalkylthio, halogenoalkylsulphinyl or halogenoalkylsulphonyl,X represents oxygen, sulphur, sulphinyl or sulphonyl andAr represents an unsubstituted aryl or a substituted aryl radical,and their physiologically tolerable acid addition salts.
摘要翻译：其中R 1表示氢或烷基，R 2表示下式的基团，其中R 3，R 4，R 5和R 6在各种情况下彼此独立地表示氢，卤素，硝基，烷基，烷氧基，烷氧基羰基，二烷基氨基，烷硫基，烷基亚磺酰基，烷基磺酰基，卤代烷基，卤代烷氧基，卤代烷硫基，卤代烷基亚磺酰基或卤代烷基磺酰基，X表示氧，硫，亚磺酰基或磺酰基，Ar表示未取代的芳基或取代的芳基，及其生理上可耐受的酸加成盐。

18. 发明授权

US4549994A Preparation of new fluoropivalic acid fluorides 失效
标题翻译：新氟氟酸氟化物的制备
公开(公告)号：US4549994A
公开(公告)日：1985-10-29
申请号：US630490
申请日：1984-07-13
申请人： Hermann Hagemann , Erich Klauke , Ernst Kysela
发明人： Hermann Hagemann , Erich Klauke , Ernst Kysela
IPC分类号： A01N47/12 , C07C51/00 , C07C51/58 , C07C53/50 , C07C67/00 , C07C239/00 , C07C271/10 , C07C271/14
CPC分类号： C07C53/50 , C07C51/58
摘要： A process for the preparation of a compound according to claim 1, comprising reacting a compound of the formula ##STR1## in which R.sup.3, R.sup.4 and R.sup.5 each independently is CH.sub.3 or CH.sub.2 Cl, at least one of the radicals R.sup.3, R.sup.4 and R.sup.5 being CH.sub.2 Cl,with a metal fluoride at elevated temperature. The products are new and useful as intermediates for making other compounds, especially carbamate insecticide synergists.
摘要翻译：一种制备根据权利要求1的化合物的方法，包括使下式化合物（其中R 3，R 4和R 5各自独立地为CH 3或CH 2 Cl）反应，基团R 3，R 4和R 5中的至少一个为CH 2 Cl ，在高温下用金属氟化物。该产品作为制备其他化合物，特别是氨基甲酸酯杀虫剂增效剂的中间体是新的和有用的。

19. 发明授权

US4351974A Preparation of 3-bromo-4-fluorotoluene 失效
标题翻译： 3-溴-4-氟甲苯的制备
公开(公告)号：US4351974A
公开(公告)日：1982-09-28
申请号：US233413
申请日：1981-02-11
申请人： Bernd Baasner , Erich Klauke , Ernst Kysela
发明人： Bernd Baasner , Erich Klauke , Ernst Kysela
IPC分类号： B01J23/74 , B01J27/00 , C07B61/00 , C07C17/00 , C07C17/12 , C07C25/13 , C07C67/00
CPC分类号： C07C17/12
摘要： In the preparation of 3-bromo-4-fluorotoluene by reacting 4-fluorotoluene with bromine, the improvement which comprises effecting the bromination in glacial acetic acid in the presence of iodine and iron or an iron salt. As a result the proportion of 3-bromo-4-fluorotoluene relative to its 2-bromo-4-fluorotoluene isomer is markedly increased.
摘要翻译：在通过4-氟甲苯与溴反应制备3-溴-4-氟甲苯的过程中，其改进包括在碘和铁或铁盐存在下在冰醋酸中进行溴化。结果，3-溴-4-氟甲苯相对于其2-溴-4-氟甲苯异构体的比例明显增加。

20. 发明授权

US4161593A Process for the preparation of triazines containing a mixture of chlorine and fluorine substituents, and of cyanuric fluoride 失效
标题翻译：制备含有氯和氟取代基的混合物的三嗪和氰尿酰氟的方法
公开(公告)号：US4161593A
公开(公告)日：1979-07-17
申请号：US870601
申请日：1978-01-18
申请人： Erich Klauke , Ernst Kysela , Alfons Dorlars
发明人： Erich Klauke , Ernst Kysela , Alfons Dorlars
IPC分类号： B01J27/00 , C07B61/00 , C07D237/12 , C07D239/30 , C07D251/28
CPC分类号： C07D251/28
摘要： Process for the preparation of triazines containing a mixture of chlorine and fluorine substituents, characterized in that cyanuric chloride is heated with cyanuric fluoride to temperatures from 30.degree.-300.degree. C. in the presence of suitable catalysts.
摘要翻译：用于制备含有氯和氟取代基混合物的三嗪的方法，其特征在于在合适的催化剂存在下，将氰尿酰氯加热至30-300℃。

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