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    • 17. 发明授权
    • Molecular crystals of controlled size
    • 受控尺寸的分子晶体
    • US06645293B2
    • 2003-11-11
    • US10093979
    • 2002-03-07
    • Allan S. Myerson
    • Allan S. Myerson
    • C30B700
    • B82Y30/00C30B7/00C30B7/005C30B29/54C30B29/605
    • Methods for the crystallization of nano-size crystals of molecular organic compounds while operating at a low supersaturation. The methods are based on controlling the domain size available during the crystallization process. In one exemplary method, microcontacted printed self-assembled monolayers (SAMs) with local domain area sizes ranging up to 2500 &mgr;m2 and fabricated SAMs generated from electron beam lithography, are employed to control the size, orientation, phase, and morphology of the crystal. In another exemplary method, a continuous micro-crystallizer having a vessel diameter of 25 microns or less is used to ensure that that the maximum size of the crystals in at least one dimension, ad preferably two dimensions is constrained by the vessel itself. The methods allow control of supersaturation and growth conditions, as well as manageability over crystallinity and polymorphism, and each method's domain size has the potential for further reduction.
    • 在低过饱和下操作时分子有机化合物的纳米尺寸晶体结晶的方法。 这些方法基于控制结晶过程中可用的结构域尺寸。 在一个示例性方法中,采用微电子印刷的自组装单层(SAM),其具有范围高达2500mum的局域结构域尺寸和由电子束光刻产生的制造的SAM,以控制尺寸,取向,相位和形态 水晶。 在另一示例性方法中,使用容器直径为25微米或更小的连续微结晶器来确保至少一个维度,优选两个维度的晶体的最大尺寸受容器本身约束。 该方法允许控制过饱和和生长条件,以及对结晶度和多态性的可管理性,并且每种方法的结构域尺寸具有进一步还原的潜力。
    • 19. 发明授权
    • Process for treating brass components to substantially eliminate leachabale lead
    • 处理黄铜成分以大幅度消除沥干铅的方法
    • US06197210B1
    • 2001-03-06
    • US09135139
    • 1998-08-17
    • Allan S. Myerson
    • Allan S. Myerson
    • C23F144
    • E03B7/006C23F1/00Y10S148/051
    • A process for the treatment of brass components to reduce leachable lead therefrom when the components are exposed to water which includes the steps of first cleaning the brass components with a cleaning agent in the form of a mineral acid, a mineral acid plus an oxidizing agent, ammonium chloride or ferric chloride and then rinsing to remove the cleaning agent. Thereafter, the brass components are contacted with a lead removal reagent after which the brass components are washed again. It is also possible, in the preferred embodiment, to remove any leachable lead remaining on the surface of the brass components by the additional step of treating the brass components with a water soluble acid and thereafter rinsing the components to leave the components substantially free of the acid. The process as disclosed reduces the leachable lead to well within the most stringent state and/or federal guidelines.
    • 当组分暴露于水时,用于处理黄铜组分以减少可浸出铅的方法,其包括以无机酸,无机酸加氧化剂形式的清洁剂首先清洗黄铜组分的步骤, 氯化铵或氯化铁,然后冲洗以除去清洁剂。 此后,将黄铜组分与除铅试剂接触,然后再次洗涤黄铜组分。 在优选的实施方案中,也可以通过用水溶性酸处理黄铜组分的另外步骤除去残留在黄铜组分表面上的任何可浸出的铅,然后冲洗组分以使组分基本上不含 酸。 所披露的过程将可浸出的铅降低到最严格的状态和/或联邦指南内。