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11. 发明授权

US06403827B1 Crystal of 2-hydroxynaphthalene-3-carboxylic acid and process for the preparation thereof 有权
标题翻译： 2-羟基萘-3-羧酸的晶体及其制备方法
公开(公告)号：US06403827B1
公开(公告)日：2002-06-11
申请号：US09720994
申请日：2001-01-03
申请人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Hiroyuki Kato
发明人： Ryuzo Ueno , Masaya Kitayama , Nobutaka Izumichi , Hiroyuki Kato
IPC分类号： C07C6334
CPC分类号： C07C65/11 , C07C51/412 , C07C51/43
摘要： The present invention provides crystalline 2-hydroxynaphthalene-3-carboxylic acid (BON) characterized in that the average particle size is equal to or more than 157 &mgr;m and the proportion of the particles of which particle size is less than 74 &mgr;m is equal to or less than 14%. The crystalline composition of the present invention can be prepared by a process comprising the step of recrystallizing BON, especially at a high temperature, or by carrying out the acid precipitation step in the method for preparing BON at a high temperature.
摘要翻译：本发明提供结晶的2-羟基萘-3-羧酸（BON），其特征在于平均粒径等于或大于157μm，粒径小于74μm的颗粒的比例等于或等于小于14％。本发明的结晶组合物可以通过包括重结晶BON的步骤，特别是在高温下或通过在高温下进行BON制备方法进行酸沉淀步骤的方法来制备。

12. 发明授权

US06194608B1 Process for separating and purifying alkali metal salts of hydroxynaphthalenecarboxylic acids 失效
标题翻译：用于分离和纯化羟基萘羧酸的碱金属盐的方法
公开(公告)号：US06194608B1
公开(公告)日：2001-02-27
申请号：US09194019
申请日：1998-11-19
申请人： Ryuzo Ueno , Masaya Kitayama , Kuniyo Yanagawase , Yoshiro Uchiyama , Shigeji Mori
发明人： Ryuzo Ueno , Masaya Kitayama , Kuniyo Yanagawase , Yoshiro Uchiyama , Shigeji Mori
IPC分类号： C07C6334
CPC分类号： C07C51/47 , C07C65/11
摘要： The present invention provides a process for separating and purifying alkali metal salts of hydroxynaphthalenecarboxylic acids, in which alkali metal salt(s) of hydroxynaphthalenecarboxylic acid(s) are separated and purified from a mixture of alkali metal salts of hydroxynaphthalenecarboxylic acids by treating it with a nonionic porous synthetic adsorbent using water or water and water-soluble organic solvent(s).
摘要翻译：本发明提供了一种分离和纯化羟基萘羧酸的碱金属盐的方法，其中羟基萘羧酸的碱金属盐通过用羟基萘羧酸的碱金属盐的混合物与羟基萘羧酸的碱金属盐进行处理而分离和纯化使用水或水的非离子多孔合成吸附剂和水溶性有机溶剂。

13. 发明授权

US6133475A Process for producing 2-hydroxynaphthalene-3,6-dicarboxylic acid 失效
标题翻译： 2-羟基萘-3,6-二羧酸的制备方法
公开(公告)号：US6133475A
公开(公告)日：2000-10-17
申请号：US91289
申请日：1998-06-16
申请人： Ryuzo Ueno , Masaya Kitayama , Yoshiro Uchiyama , Syungo Nara
发明人： Ryuzo Ueno , Masaya Kitayama , Yoshiro Uchiyama , Syungo Nara
IPC分类号： C07C51/15 , C07C65/11
CPC分类号： C07C51/15
摘要： The present invention relates to a process for preparing 2-hydroxynaphthalene-3,6-dicarboxylic acid which comprises reacting potassium 2-naphtholate and carbon dioxide at a temperature 290.degree. C. or higher under a pressure 30 kg/cm.sup.2 (G) or higher. According to this process, 2-hydroxynaphthalene-3,6-dicarboxylic acid can be obtained in high yield.
摘要翻译：本发明涉及一种制备2-羟基萘-3,6-二羧酸的方法，其包括在290℃或更高的温度下在压力为30kg / cm 2（G）或更高的温度下使2-萘酚钠与二氧化碳反应。根据该方法，可以高产率得到2-羟基萘-3,6-二羧酸。

14. 发明授权

US6005085A Condensed azo compounds and process for preparing the same 失效
标题翻译：缩合偶氮化合物及其制备方法
公开(公告)号：US6005085A
公开(公告)日：1999-12-21
申请号：US194500
申请日：1998-11-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Katsunori Tanikawa
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Katsunori Tanikawa
IPC分类号： C09B50/00 , C07C245/10 , C07D209/88 , C07D235/26 , C07D249/14 , C07D249/20 , C07D271/10 , C07D271/107 , C07D307/52 , C09B33/147 , C09B62/04 , D06P3/40 , G03G5/06 , C08J3/20 , C09B67/20 , C09D7/12 , C09D11/00
CPC分类号： C07D271/107 , C07C245/10 , C07D209/88 , C07D235/26 , C07D249/14 , C07D249/20 , C07D307/52 , C09B33/147 , C09B62/046 , G03G5/0679 , G03G5/0681 , Y10S8/918
摘要： The present invention provides novel condensed azo compounds using bisamide compounds of 2-hydroxynaphthalene-3,6-dicarboxylic acid, amide, or ester as the couplers, which have excellent properties such as excellent water resistance, chemical resistance, solvent resistance, and heat resistance.
摘要翻译： PCT No.PCT / JP98 / 01166 Sec。 371日期：1998年11月18日 102（e）1998年11月18日日期PCT提交1998年3月19日PCT公布。公开号WO98 / 41580 日期1998年9月24日本发明提供使用2-羟基萘-3,6-二羧酸，酰胺或酯的双酰胺化合物作为成色剂的新颖的缩合偶氮化合物，其具有优异的耐水性，耐化学性，溶剂性电阻和耐热性。

15. 发明授权

US5786523A Naphthol derivatives and process for producing the same 失效
公开(公告)号：US5786523A
公开(公告)日：1998-07-28
申请号：US972480
申请日：1997-11-18
申请人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
发明人： Ryuzo Ueno , Shigeru Ito , Kenji Minami , Masaya Kitayama
IPC分类号： C07C65/11 , C07C65/24 , C07C69/94 , C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07D209/88 , C07D235/26 , C07C39/14
CPC分类号： C07C235/64 , C07C235/66 , C07C275/54 , C07C311/46 , C07C65/11 , C07C65/24 , C07C69/94 , C07D209/88 , C07D235/26 , C07C2103/24
摘要： A naphthol derivative represented by the general formula (I) �wherein Y and Y' indicate --(CONH).sub.n --X or --COR; X is a phenyl group, a naphthyl group, an anthraquinonyl group, a benzimidazolonyl group or a carbazolyl group; R is a hydroxyl group, an alkoxy group having 1 to 6 carbon atoms, a halogen atom, a benzyloxy group, a phenyloxy group or a phenacyloxy group; R.sub.2 is a hydrogen atom, an alkaline metal, an alkyl group having 1 to 6 carbon atoms, an acyl group having 1 to 6 carbon atoms or a phenylalkyl group; Z is a group selected from the group consisting of a hydrogen atom, a halogen atom, a nitro group, a nitroso group and an amino group (Z may be substituted on any ring of the naphthalene ring); and n is an integer of 1 or 2; provided that R.sub.2 and Z do not simultaneously indicate a hydrogen atom when both R simultaneously indicate a hydroxyl group!, and a process for producing the same. This naphthol derivative can be used as raw materials for synthesis, such as dyes, pigments, photosensitive materials and the like. ##STR1##

16. 发明授权

US07355071B2 Method for preparing 2,6-naphthalene dicarboxylic acid 有权
标题翻译： 2,6-萘二甲酸的制备方法
公开(公告)号：US07355071B2
公开(公告)日：2008-04-08
申请号：US11090054
申请日：2005-03-28
申请人： Masaya Kitayama , Hiroyuki Wakamori
发明人： Masaya Kitayama , Hiroyuki Wakamori
IPC分类号： C07C51/42
CPC分类号： C07C51/09 , C07C63/38
摘要： Disclosed is an improved method for preparing 2,6-naphthalene dicarboxylic acid from di-lower alkyl 2,6-naphthalene dicarboxylate, which is characterized in that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specified amount of water in the presence of specified amount of hydrophobic organic solvent and an additive; that hydrolyzing di-lower alkyl 2,6-naphthalene dicarboxylate in a specific amount of a mixed solvent of non-water miscible alcohol and water; or in that di-lower alkyl 2,6-naphthalene dicarboxylate is hydrolyzed in two steps wherein the 1st step comprises hydrolyzing said ester in a water miscible organic solvent in the presence of a small amount of water, and the 2nd step comprises further hydrolyzing the reaction.
摘要翻译：本发明公开了一种从2,6-二萘基二羧酸二低级烷基酯制备2,6-萘二羧酸的改进方法，其特征在于将2,6-萘二羧酸二低级烷基酯在规定量的水中存在规定量的疏水性有机溶剂和添加剂; 在特定量的非水混溶性醇和水的混合溶剂中水解2,6-萘二甲酸二低级烷基酯; 或者在2,6-二羧酸二低级烷基酯中以两个步骤水解，其中第一步包括在少量水存在下在水混溶性有机溶剂中水解所述酯，第二步包括进一步水解反应。

17. 发明授权

US06984712B2 Liquid-crystal polyester resin 有权
标题翻译：液晶聚酯树脂
公开(公告)号：US06984712B2
公开(公告)日：2006-01-10
申请号：US10496490
申请日：2002-11-25
申请人： Ryuzo Ueno , Masaya Kitayama , Kiichi Kometani , Hiroyuki Kato , Kazunori Ueda
发明人： Ryuzo Ueno , Masaya Kitayama , Kiichi Kometani , Hiroyuki Kato , Kazunori Ueda
IPC分类号： C08G63/06 , C08F20/00 , C09K19/32
CPC分类号： C08G63/605 , C08G63/06 , C08G63/19 , C08G63/20 , C09K19/3809
摘要： The present invention provides a liquid-crystalline polyester resin which comprises monomer units derived from 2-hydroxy-3-naphthoic acid and/or 2-hydroxynaphthalene-3,6-dicarboxylic acid in an amount of 1-5000 mmol % based on the total monomer components of the resin and an alkaline metal compound in an amount of 10-3000 ppm as alkaline metal based on the total monomer components of the resin. The liquid-crystalline polyester resin of the present invention has good colorability, improved heat resistance and good mechanical properties.
摘要翻译：本发明提供一种液晶聚酯树脂，其包含基于总量为1-5000mmol％的来源于2-羟基-3-萘甲酸和/或2-羟基萘-3,6-二羧酸的单体单元树脂的单体组分和碱金属化合物，其量为基于树脂总单体成分的碱金属为10-3000ppm。本发明的液晶聚酯树脂具有良好的着色性，耐热性和良好的机械性能。

18. 发明申请

US20050192442A1 Method for preparing 2-hydroxy-6-ureidocarbonyl naphthalene derivative 失效
标题翻译： 2-羟基-6-脲基羰基萘衍生物的制备方法
公开(公告)号：US20050192442A1
公开(公告)日：2005-09-01
申请号：US11048876
申请日：2005-02-03
申请人： Masaya Kitayama , Hiroyuki Wakamori , Nobuhiro Yonetani
发明人： Masaya Kitayama , Hiroyuki Wakamori , Nobuhiro Yonetani
IPC分类号： C07C275/54 , C07C273/02 , C07C273/06 , C07C273/18 , C07D235/22 , C07C273/00
CPC分类号： C07C273/1827 , C07C275/54
摘要： Disclosed is a method for preparing a 2-hydroxy-6-ureidocarbonyl naphthalene derivative. The method comprises the step of reacting 2-hydroxy-6-aminocarbonyl naphthalene and a isocyanate in an organic solvent at a temperature of 90-200° C. According to the present invention, 2-hydroxy-6-ureidocarbonyl naphthalene derivative can easily be obtained within relatively short time and high yield.
摘要翻译：公开了2-羟基-6-脲基羰基萘衍生物的制备方法。该方法包括在90-200℃的温度下，使2-羟基-6-氨基羰基萘与异氰酸酯在有机溶剂中反应的步骤。根据本发明，2-羟基-6-脲基羰基萘衍生物可容易地在相对较短的时间内获得较高的产量。

19. 发明申请

US20050147909A1 Charge controllers 失效
标题翻译：充电控制器
公开(公告)号：US20050147909A1
公开(公告)日：2005-07-07
申请号：US10511097
申请日：2003-04-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Nobuhiro Yonetani
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Nobuhiro Yonetani
IPC分类号： C07C69/94 , C07C235/46 , C07C235/84 , G03G9/097 , G03G9/00 , C07C23/10
CPC分类号： C07C235/84 , C07C69/94 , G03G9/09733 , G03G9/0975 , G03G9/09775 , G03G9/09783
摘要： The present invention provides a safe charge control agent which exhibits an excellent negative chargeability and excellent dispersibility in and compatibility with binder resins, and is even applicable for col or toners. Specifically, the charge control agent consists of a naphthol derivative of formula [I]: and a salt thereof, and an electrophotographic toner comprising the agent are provided.
摘要翻译：本发明提供一种安全的电荷控制剂，其具有优异的负电荷性和优异的分散性和与粘合剂树脂的相容性，并且甚至可应用于胶体或调色剂。具体地，电荷控制剂由式[I]的萘酚衍生物及其盐组成，并且提供包含该试剂的电子照相调色剂。

20. 发明授权

US06891072B2 Process for production of dimers or aromatic monohydroxyl compounds 失效
标题翻译：二聚体或芳族单羟基化合物的制备方法
公开(公告)号：US06891072B2
公开(公告)日：2005-05-10
申请号：US10433908
申请日：2002-04-18
申请人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Hikari Hirai
发明人： Ryuzo Ueno , Masaya Kitayama , Kenji Minami , Hiroyuki Wakamori , Hikari Hirai
IPC分类号： C07B61/00 , C07C37/11 , C07C39/14 , C07C45/39 , C07C46/08 , C07C49/653 , C07C67/343 , C07C69/94 , C07C231/12 , C07C235/66 , C07C273/18 , C07C275/54 , C07D307/52 , C07C39/12
CPC分类号： C07D307/52 , C07C37/11 , C07C46/08 , C07C67/343 , C07C231/12 , C07C273/1854 , C07C2603/50 , C07C50/10 , C07C50/08 , C07C69/94 , C07C235/66 , C07C275/54 , C07C39/14
摘要： The present invention provides a method for preparing dimer of a monohydroxy aromatic compound. In the method of the present invention, oxidative coupling reaction of a monohydroxy aromatic compound represented by formula [I]: Ar—OH [I] wherein Ar represents an optionally substituted aromatic group is carried out in a nitrogen containing polar solvent in the presence of a copper salt. By the method of the instant invention, dimer of the monohydroxy aromatic compound can be obtained in high yield.
摘要翻译：本发明提供一种制备单羟基芳族化合物的二聚体的方法。在本发明的方法中，由式[I]表示的单羟基芳族化合物的氧化偶联反应：<？in-line-formula description =“In-line Formulas”end =“lead”→Ar-OH [I ]其中Ar表示可以具有取代基的芳族基团，在含铜极性溶剂中，在铜盐存在下进行。通过本发明的方法，可以高产率获得单羟基芳族化合物的二聚体。

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