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11. 发明授权

US4584239A Stretched multilayer polypropylene film 失效
标题翻译：拉伸多层聚丙烯薄膜
公开(公告)号：US4584239A
公开(公告)日：1986-04-22
申请号：US753846
申请日：1985-07-11
申请人： Masahiro Kakugo , Yoshiharu Fukui , Kizuku Wakatsuki , Seiichiro Ima , Junichi Kimura
发明人： Masahiro Kakugo , Yoshiharu Fukui , Kizuku Wakatsuki , Seiichiro Ima , Junichi Kimura
IPC分类号： B32B27/00 , B32B27/32 , C09J7/02 , C09J123/08 , C09J123/14
CPC分类号： C09J7/0242 , B32B27/32 , C09J123/0815 , C09J123/142 , Y10S428/91 , Y10T428/2826
摘要： A stretched multilayer polypropylene film is described, comprising a stretched crystalline polypropylene layer and a layer of a composition (Composition B) laminated on at least one side of said polypropylene layer, wherein the composition B comprises a homo- or copolymer composed mainly of ethylene, propylene or butene-1 and having a melting point of 150.degree. C. or less, and a vinylcycloalkane polymer in an amount of 0.05 wt ppm to 10 wt % calculated as a vinylcycloalkane unit. This multilayer film is greatly improved in optical properties such as excellent see-through properties without deteriorating its good heat sealability. Thus it is very useful for wrapping.
摘要翻译：描述了拉伸的多层聚丙烯薄膜，其包含拉伸的结晶聚丙烯层和层压在所述聚丙烯层的至少一侧上的组合物层（组合物B），其中组合物B包含主要由乙烯组成的均聚物或共聚物，丙烯或丁烯-1，熔点为150℃以下，乙烯基环烷烃聚合物的量为0.05重量％〜10重量％，以乙烯基环烷烃单元计算。这种多层膜在透光性方面优异的光学特性大大提高，而不会使其良好的热封性劣化。因此，它是非常有用的包装。

12. 发明授权

US4382065A Fluidized bed apparatus and method of using 失效
标题翻译：流化床装置及其使用方法
公开(公告)号：US4382065A
公开(公告)日：1983-05-03
申请号：US304871
申请日：1981-09-23
申请人： Akinobu Shiga , Masahiro Kakugo , Koji Yamada , Hajime Sadatoshi
发明人： Akinobu Shiga , Masahiro Kakugo , Koji Yamada , Hajime Sadatoshi
IPC分类号： B01J8/34 , B01J8/00 , B01J8/38 , C08F2/38 , C08F10/00 , F27B15/08
CPC分类号： B01J8/386 , B01J8/0065 , C08F10/00
摘要： In a fluidized bed apparatus intended to fluidize solid particles by means of ascending stream gas, the improvement for reducing solid particles entrained from the apparatus, which comprises placing an internal in a free board of the apparatus so that the projected area ratio is not less than 0.8, and the opening proportion to the free board cross-sectional area is within 0.3 to 0.9.
摘要翻译：在旨在通过上升气流使固体颗粒流化的流化床装置中，减少了从装置夹带的固体颗粒的改进，其包括将内部放置在装置的自由板中，使得投影面积比不小于 0.8，与自由板横截面积的开口比例在0.3〜0.9的范围内。

13. 发明授权

US4367322A Process for producing propylene copolymer 失效
标题翻译：制备丙烯共聚物的方法
公开(公告)号：US4367322A
公开(公告)日：1983-01-04
申请号：US291701
申请日：1981-08-10
申请人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Akira Nunose , Masaharu Nishioka
发明人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Akira Nunose , Masaharu Nishioka
IPC分类号： C08F4/64 , C08F210/06
CPC分类号： C08F210/06 , Y10S526/916
摘要： In a process for producing propylene copolymer containing about 80 to 99 mol % propylene and about 1 to 20 mol % ethylene and/or an .alpha.-olefin having 4 to 18 carbon atoms using a Ziegler-Natta catalyst, the improvement which comprises said Ziegler-Natta catalyst comprising:(A) titanium trichloride prepared by reducing titanium tetrachloride with an organoaluminum compound and activating the product; and(B) an organoaluminum compound;with the molar ratio of (B)/(A) being about 20 to 100.
摘要翻译：在使用齐格勒 - 纳塔催化剂的丙烯共聚物的制备方法中，所述丙烯共聚物含有约80-99摩尔％的丙烯和约1-20摩尔％的乙烯和/或具有4-18个碳原子的α-烯烃，其改进包括所述齐格勒 - 纳塔催化剂，其包含：（A）通过用有机铝化合物还原四氯化钛制备的三氯化钛并活化该产物; 和（B）有机铝化合物; （B）/（A）的摩尔比为约20至100。

14. 发明授权

US4355144A Process for producing a propylene-ethylene copolymer having improved stretchability 失效
标题翻译：制备具有改善的拉伸性的丙烯 - 乙烯共聚物的方法
公开(公告)号：US4355144A
公开(公告)日：1982-10-19
申请号：US257431
申请日：1981-04-24
申请人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Seiichiro Ima , Katsuyoshi Yamashita
发明人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Seiichiro Ima , Katsuyoshi Yamashita
IPC分类号： C08F4/00 , C08F2/00 , C08F4/60 , C08F4/64 , C08F10/00 , C08F10/06 , C08F210/00 , C08F210/06 , C08F210/16
CPC分类号： C08F210/06
摘要： In a process for producing polypropylene comprising polymerizing propylene in the presence of hydrogen and a catalyst system comprising (A) titanium trichloride obtained by reducing titanium tetrachloride with an organoaluminum compound and reacting the reduced solid with an ether represented by the formula:R.sup.1 -O-R.sup.2wherein R.sup.1 and R.sup.2 are defined hereinbefore, and a halogen compound selected from the group consisting of (i) halogen or interhalogen compounds of the formula, X.sup.1 X.sup.2.sub.a (wherein X.sup.1, X.sup.2 and a are defined hereinbefore), (ii) titanium halides, and (iii) organic halogen compounds, simultaneously or successively and (B) an organoaluminum compound, the improvement which comprises supplying ethylene together with propylene to the polymerization system such that the ethylene concentration in the vapor phase of the system based on the total amount of propylene, ethylene and hydrogen in the vapor phase of the system is 0.15 to 1.5 mol % to obtain a propylene-ethylene copolymer having an ethylene content of from 0.1 to 1.0 wt % is disclosed. The propylene-ethylene copolymer is improved in stretchability.
摘要翻译：在制备聚丙烯的方法中，包括在氢气存在下聚合丙烯和催化剂体系，所述催化剂体系包含（A）通过用有机铝化合物还原四氯化钛获得的三氯化钛，并将还原的固体与由下式表示的醚反应：R1-O- 其中R 1和R 2如上定义，卤素化合物选自（ⅰ）卤素或下式的卤代化合物：X1X2a（其中X1，X2和a定义如前），（ⅱ）卤化钛和（iii）有机卤素化合物，同时或相继和（B）有机铝化合物，其改进包括将乙烯与丙烯一起供应到聚合体系中，使得基于丙烯总量的体系的气相中的乙烯浓度，系统的气相中的乙烯和氢为0.15〜1.5摩尔％，得到丙烯 - 乙烯共聚物公开了乙烯含量为0.1〜1.0重量％。丙烯 - 乙烯共聚物的拉伸性提高。

15. 发明授权

US4927872A Polypropylene film 失效
标题翻译：聚丙烯膜
公开(公告)号：US4927872A
公开(公告)日：1990-05-22
申请号：US331759
申请日：1989-04-03
申请人： Masahiro Kakugo , Seiichiro Ima
发明人： Masahiro Kakugo , Seiichiro Ima
IPC分类号： B32B27/32 , C08J5/18 , C08K5/00 , C08K5/20
CPC分类号： C08J5/18 , B32B27/32 , C08K5/0008 , C08K5/20 , C08J2323/10 , Y10T428/2826 , Y10T428/31692 , Y10T428/3175 , Y10T428/31797 , Y10T428/31855 , Y10T428/31895 , Y10T428/31913
摘要： A monolayer polypropylene film obtained by melt extrusion from a composition comprising 100 parts by weight of a crystalline polypropylene and, incorporated therein, a slipping agent {A} having a melting point of 100.degree. to 125.degree. C. and a slipping agent {B} having a melting point of 70.degree. to 90.degree. C. in a total amount of 0.05 to 1.0 part by weight, the initial coefficient of friction of said film being 0.7 or below and the coefficient of friction after heating at 60.degree. C. being 1.0 or below; and a multilayer film composed of said polypropylene film layer having said composition and said characteristics and a substrate material layer.

16. 再颁专利

USRE32542E Molded products of polypropylene 失效
标题翻译：聚丙烯成型产品
公开(公告)号：USRE32542E
公开(公告)日：1987-11-10
申请号：US927219
申请日：1986-11-05
申请人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Seiichiro Ima
发明人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Seiichiro Ima
IPC分类号： C08F10/06 , C08F110/06 , C08F210/06 , C08L23/10 , C08L23/12
CPC分类号： C08F10/06 , C08J5/18 , C08F110/06 , C08F210/06 , C08J2323/12 , C08L23/10 , Y10T428/31899
摘要： A molded product of polypropylene having an isotactic pentad fraction of the boiling heptane insoluble portion of at least about 0.955 and a boiling heptane solubles content of about 2.0 to 9.0% by weight. The molded products include a stretched film, insulating materials for electrical equipment, etc.

17. 发明授权

US4551501A Crystalline propylene polymer composition 失效
标题翻译：结晶丙烯聚合物组合物
公开(公告)号：US4551501A
公开(公告)日：1985-11-05
申请号：US686866
申请日：1984-12-27
申请人： Akinobu Shiga , Masahiro Kakugo , Junpei Kojima , Kizuku Wakatsuki
发明人： Akinobu Shiga , Masahiro Kakugo , Junpei Kojima , Kizuku Wakatsuki
IPC分类号： C08L23/12 , C08F297/08 , C08L7/00 , C08L21/00 , C08L23/00 , C08L23/10 , C08L23/18 , C08L23/20 , C08L23/24 , C08L53/00 , C08L101/00 , C08L23/14
CPC分类号： C08L53/00 , C08F297/08 , C08F297/083 , C08L23/10 , C08L23/20
摘要： A crystalline propylene polymer composition having excellent transparency and rigidity comprising a blend of a crystalline polypropylene with a polymer of a vinyl cycloalkane having at least 6 carbon atoms. The composition contains 0.05 weight ppm to 10,000 weight ppm of the vinyl cycloalkane unit.
摘要翻译：一种结晶丙烯聚合物组合物，其具有优异的透明度和刚度，包括结晶聚丙烯与具有至少6个碳原子的乙烯基环烷烃聚合物的共混物。该组合物含有0.05重量ppm至10,000重量ppm的乙烯基环烷烃单元。

18. 发明授权

US4461881A Process for the production of purified propylene homopolymers or copolymers 失效
标题翻译：制备纯化丙烯均聚物或共聚物的方法
公开(公告)号：US4461881A
公开(公告)日：1984-07-24
申请号：US314344
申请日：1981-10-23
申请人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Takatoshi Suzuki
发明人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Yukio Naito , Takatoshi Suzuki
IPC分类号： C08F6/00 , C08F6/02 , C08F6/06 , C08F10/06 , C08F6/08 , C08F4/64
CPC分类号： C08F6/02 , C08F10/00 , C08F10/06
摘要： In a process for producing a homopolymer or a copolymer of propylene comprising polymerizing propylene or copolymerizing propylene and at least one other unsaturated hydrocarbon monomer in liquid propylene using a catalyst system containing activated titanium trichloride (a) and an organoaluminum compound (b), the activated titanium trichloride (a) being prepared by reducing titanium tetrachloride with an organoaluminum compound followed by activation, to produce a polymer slurry; introducing the polymer slurry produced into the top of a counter-current washing tower; and washing the polymer slurry by counter-currently contacting the polymer slurry with liquid propylene introduced into the bottom of the washing tower, the improvement which comprises purifying the homopolymer or copolymer of propylene by feeding an epoxide in a molar amount of about 1 to about 15 times the molar amount of the total of activated titanium trichloride (a) and organoaluminum compound (b), to a part of said washing tower, thereby deactivating the catalyst and removing the catalyst residue and the homopolymer or copolymer of propylene dissolved in the polymer slurry.
摘要翻译：在使用包含活化的三氯化钛（a）和有机铝化合物（b）的催化剂体系的丙烯均聚物或共聚物的制备方法中，该方法包括聚合丙烯或使液体丙烯中的至少一种其它不饱和烃单体共聚，三氯化钛（a）通过用有机铝化合物还原四氯化钛然后活化而制备，以产生聚合物浆料; 将产生的聚合物浆料引入逆流洗涤塔的顶部; 并且通过将聚合物浆料与引入洗涤塔底部的液态丙烯反向接触来洗涤聚合物浆料，其改进包括通过加入摩尔量为约1至约15的环氧化物纯化丙烯的均聚物或共聚物倍的活化三氯化钛（a）和有机铝化合物（b）的总量的摩尔量与所述洗涤塔的一部分反应，从而使催化剂失活并除去溶解在聚合物浆料中的催化剂残余物和丙烯均聚物或共聚物。

19. 发明授权

US4273905A Process for producing propylene polymer or copolymer 失效
标题翻译：制备丙烯聚合物或共聚物的方法
公开(公告)号：US4273905A
公开(公告)日：1981-06-16
申请号：US1651
申请日：1979-01-08
申请人： Mamoru Asada , Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo
发明人： Mamoru Asada , Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo
IPC分类号： C08F4/00 , C08F4/60 , C08F4/64 , C08F10/06 , C08F4/66
CPC分类号： C08F10/06 , Y10S526/902
摘要： A process for producing a propylene polymer or copolymer which comprises polymerizing (a) propylene or (b) a mixture of propylene and another unsaturated hydrocarbon monomer in liquid propylene in the presence of a catalyst system of(A) a specified titanium trichloride composition obtained by reducing titanium tetrachloride with an organoaluminum compound and activating the product;(B) an organoaluminum compound having the general formulaR.sub.2 AlX wherein R represents an alkyl group or an aralkyl group, each containing up to 18 carbon atoms, and X represents a halogen atom; and(C) an unsaturated carboxylic acid ester; while adjusting the amount of the polymer produced to at least 8,000 g per gram of the titanium trichloride composition.
摘要翻译：一种制备丙烯聚合物或共聚物的方法，其包括在（A）由（A）得到的规定的三氯化钛组合物的催化剂体系的存在下，在液体丙烯中聚合（a）丙烯或（b）丙烯和另一种不饱和烃单体的混合物用有机铝化合物还原四氯化钛并活化产物; （B）具有通式R2AlX的有机铝化合物，其中R表示烷基或芳烷基，各自含有至多18个碳原子，X表示卤素原子; 和（C）不饱和羧酸酯; 同时将生产的聚合物的量调节至每克三氯化钛组合物至少8,000克。

20. 发明授权

US4182852A Process for refining a homopolymer of copolymer of propylene 失效
标题翻译：精制丙烯共聚物均聚物的方法
公开(公告)号：US4182852A
公开(公告)日：1980-01-08
申请号：US881314
申请日：1978-02-27
申请人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Takatoshi Suzuki
发明人： Akinobu Shiga , Kiyoshi Matsuyama , Masahiro Kakugo , Takatoshi Suzuki
IPC分类号： C08F2/00 , C08F2/02 , C08F6/00 , C08F6/02 , C08F6/06 , C08F6/28
CPC分类号： C08F6/02
摘要： In a process for producing a propylene homopolymer or copolymer which comprises polymerizing propylene or copolymerizing propylene and at least one other unsaturated hydrocarbon monomer in liquid propylene using a catalyst comprising activated titanium trichloride and an organo-aluminum compound, the activated titanium trichloride being prepared by reducing titanium tetrachloride with an organo-aluminum compound followed by activation, introducing the polymer slurry produced into the top of a counter-current washing tower, and washing the slurry by bringing the slurry into counter-current contact with liquid propylene which is introduced into the bottom of the washing tower, the improvement which comprises refining the homopolymer or copolymer of propylene by feeding (a) an alcohol having 3 to 8 carbon atoms in a molar amount of about 0.1 to about 10 times the molar amount of the organo-aluminum compound in the slurry, or (b) a mixture of an alcohol having 3 to 8 carbon atoms and an epoxide, the molar amount of the alcohol being about 0.1 to about 10 times the molar amount of the organo-aluminum compound in the slurry and the molar amount of the epoxide compound being about 0.1 to about 3 times the molar amount of the organo-aluminum compound in the slurry, to a part of the washing tower, thereby simultaneously deactivating the catalyst and removing the catalyst and the propylene homopolymer or copolymer dissolved in the polymer slurry.
摘要翻译：在制备丙烯均聚物或共聚物的方法中，包括使用包含活性三氯化钛和有机铝化合物的催化剂聚合丙烯或使丙烯与液体丙烯中的至少一种其它不饱和烃单体共聚，活化的三氯化钛通过还原将四氯化钛与有机铝化合物接触，然后活化，将产生的聚合物浆料引入逆流洗涤塔的顶部，并通过使浆料与导入底部的液体丙烯逆流接触来洗涤浆料的改进，其包括通过将（a）具有3-8个碳原子的醇以摩尔量为有机铝化合物的摩尔量的约0.1至约10倍的量来提炼丙烯的均聚物或共聚物浆料，或（b）具有3至8个碳原子的醇和ep的醇的混合物氧化物，醇的摩尔量为浆料中有机铝化合物的摩尔量的约0.1至约10倍，环氧化合物的摩尔量为有机铝的摩尔量的约0.1至约3倍将该浆料中的化合物加入到洗涤塔的一部分中，从而同时使催化剂失活并除去溶解在聚合物浆料中的催化剂和丙烯均聚物或共聚物。

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