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11. 发明申请

US20060011514A1 Coated zeolite catalysts and use for hydrocarbon conversion 有权
公开(公告)号：US20060011514A1
公开(公告)日：2006-01-19
申请号：US10862849
申请日：2004-06-07
申请人： Jannetje van den Berge , Gary Mohr , Kenneth Clem , Wilfried Mortier , Machteld Mertens , Michael Bradford
发明人： Jannetje van den Berge , Gary Mohr , Kenneth Clem , Wilfried Mortier , Machteld Mertens , Michael Bradford
IPC分类号： B01J29/06 , C10G11/04 , C07C15/12 , C07C5/22
CPC分类号： B01J35/023 , B01J29/40 , B01J29/70 , B01J29/80 , B01J37/0246 , B01J2229/12 , B01J2229/26 , B01J2229/42 , B01J2229/62 , C07C2/864 , C07C5/2708 , C07C6/123 , C07C2529/40 , C07C2529/70 , C07C2529/87 , C10G3/45 , C10G3/47 , C10G3/49 , C10G11/05 , C10G35/065 , C10G35/095 , C10G45/64 , C10G2300/1044 , C10G2300/4018 , C10G2300/708 , C10G2400/20 , Y02P20/52 , Y02P30/20 , C07C15/08
摘要： There is provided a coated zeolite catalyst in which the accessibility of the acid sites on the external surfaces of the zeolite is controlled and a process for converting hydrocarbons utilizing the coated zeolite catalyst. The zeolite catalyst comprises core crystals of a first zeolite and a discontinuous layer of smaller size second crystals of a second zeolite which cover at least a portion of the external surface of the first crystals The coated zeolite catalyst finds particular application in hydrocarbon conversion processes where catalyst activity in combination with zeolite structure are important for reaction selectivity, e.g., catalytic cracking, alkylation, disproportional of toluene, isomerization, and transalkylation reactions.

12. 发明申请

US20050197520A1 Chabazite-type molecular sieve, its synthesis and its use in the conversion of oxygenates to olefins 有权
标题翻译：菱沸石型分子筛，其合成及其在含氧化合物转化为烯烃中的应用
公开(公告)号：US20050197520A1
公开(公告)日：2005-09-08
申请号：US11017092
申请日：2004-12-20
申请人： Machteld Mertens , Guang Cao , Hailian Li , Anil Guram , Robert Saxton , Mark Muraoka , Jeffrey Yoder
发明人： Machteld Mertens , Guang Cao , Hailian Li , Anil Guram , Robert Saxton , Mark Muraoka , Jeffrey Yoder
IPC分类号： B01J29/00 , B01J29/70 , C01B37/02 , C01B39/00 , C01B39/02 , C01B39/04 , C01B39/48 , C07C1/00 , C07C1/20
CPC分类号： B01J29/7015 , C01B37/02 , C01B39/48 , C07C1/20 , Y02P20/52 , Y02P30/42 , Y10S423/30 , C07C11/06 , C07C11/04 , C07C11/02
摘要： The synthesis of a crystalline material, in particular a high silica zeolite, having a chabazite-type framework is aided by the addition to the synthesis mixture of seeds of an AEI framework-type material. The chabazite-type product has a relatively small crystal size and exhibits activity and selectivity in the conversion of methanol to lower olefins, especially ethylene and propylene.
摘要翻译：通过添加到AEI骨架型材料的种子的合成混合物来辅助具有菱沸石型骨架的结晶材料，特别是高二氧化硅沸石的合成。菱沸石型产品具有相对较小的晶体尺寸，并且在甲醇转化成低级烯烃，特别是乙烯和丙烯时具有活性和选择性。

13. 发明申请

US20050154244A1 Chabazite-containing molecular sieve, its synthesis and its use in the conversion of oxygenates to olefins 有权
标题翻译：含有菱沸石的分子筛，其合成及其在含氧化合物转化为烯烃中的应用
公开(公告)号：US20050154244A1
公开(公告)日：2005-07-14
申请号：US11017286
申请日：2004-12-20
申请人： Guang Cao , Machteld Mertens , Karl Strohmaier , Richard Hall , Thomas Colle , Mobae Afeworki , Antonie Bons , Wilfried Mortier , Chris Kliewer , Hailian Li , Anil Guram , Robert Saxton , Mark Murakoa , Jeffrey Yoder
发明人： Guang Cao , Machteld Mertens , Karl Strohmaier , Richard Hall , Thomas Colle , Mobae Afeworki , Antonie Bons , Wilfried Mortier , Chris Kliewer , Hailian Li , Anil Guram , Robert Saxton , Mark Murakoa , Jeffrey Yoder
IPC分类号： C01B37/02 , C01B39/02 , C01B39/46 , C01B39/48 , C10G3/00 , C07C1/00
CPC分类号： C01B39/46 , C01B37/02 , C01B39/023 , C01B39/48 , C10G3/45 , C10G3/49 , C10G3/62 , C10G2300/708 , C10G2300/802 , C10G2400/20 , Y02P30/20 , Y02P30/42
摘要： A crystalline material substantially free of framework phosphorus and comprising a CHA framework type molecular sieve with stacking faults or at least one intergrown phase of a CHA framework type molecular sieve and an AEI framework type molecular sieve, wherein said material, in its calcined, anhydrous form, has a composition involving the molar relationship: (n)X2O3:YO2, wherein X is a trivalent element; Y is a tetravalent element; and n is from 0 to about 0.5. The material exhibits activity and selectivity in the conversion of methanol to lower olefins, especially ethylene and propylene.
摘要翻译：基本上不含骨架磷的结晶物质，其包含具有堆垛层错的CHA骨架型分子筛或CHA骨架型分子筛和AEI骨架型分子筛的至少一个共生相，其中所述材料以其煅烧的无水形式具有涉及摩尔关系的组成：<？in-line-formula description =“In-line Formulas”end =“lead”？>（n）X＆lt; 2＆lt; 3＆lt; 3＆其中X是三价元素;其中X是三价元素;其中X是三价元素; Y是四价元素; 且n为0至约0.5。该材料在甲醇转化为低级烯烃，特别是乙烯和丙烯时具有活性和选择性。

14. 发明申请

US20080045768A1 Novel molecular sieve composition, a method of making and a process of using the same 有权
标题翻译：新型分子筛组合物，制备方法及其使用方法
公开(公告)号：US20080045768A1
公开(公告)日：2008-02-21
申请号：US11827953
申请日：2007-07-13
申请人： Wieslaw Roth , Machteld Mertens , Els De Clerck , Ivy Johnson
发明人： Wieslaw Roth , Machteld Mertens , Els De Clerck , Ivy Johnson
IPC分类号： C07C7/20 , C01B39/00
CPC分类号： B01J29/7038 , B01J29/047 , B01J35/002 , C01B39/06 , C01B39/48 , C07C2/66 , C07C6/123 , C07C29/36 , C07C37/08 , C07C37/11 , C07C37/14 , C07C37/20 , C07C41/06 , C07C57/30 , C07C263/20 , C07C2529/70 , Y02P20/52 , C07C265/14 , C07C39/06 , C07C43/046 , C07C33/20 , C07C39/04 , C07C39/16
摘要： This disclosure relates to a crystalline MCM-22 family molecular sieve composition having, in its as-synthesized form, an X-ray diffraction pattern including a peak at d-spacing maximum of 12.33±0.23 Angstroms, a distinguishable peak at a d-spacing maximum between 12.57 to about 14.17 Angstroms and a non-discrete peak at a d-spacing maximum between 8.8 to 11. Angstroms, wherein the peak intensity of the d-spacing maximum between 12.57 to about 14.17 Angstroms is less than 90% of the peak intensity of the d-spacing maximum at 12.33±0.23 Angstroms. This disclosure also relates to methods of making the crystalline MCM-22 family molecular sieve composition.
摘要翻译：本公开涉及一种结晶MCM-22族分子筛组合物，其以其合成形式具有包括在d间距最大值为12.33±0.23埃处的峰的X射线衍射图，d-间隔处的可区分峰最大值在12.57至约14.17埃之间，并且在8.8至11之间的d间距最大值处的非离散峰。其中，在12.57至约14.17埃之间的d间距最大值的峰值强度小于峰值的90％ d间距最大强度为12.33±0.23埃。本公开还涉及制备结晶MCM-22族分子筛组合物的方法。

15. 发明申请

US20060292053A1 Process for manufacture of silicoaluminophosphate molecular sieves 有权
标题翻译：硅铝磷酸盐分子筛的制备方法
公开(公告)号：US20060292053A1
公开(公告)日：2006-12-28
申请号：US11442831
申请日：2006-05-30
申请人： Machteld Mertens , An Verberckmoes
发明人： Machteld Mertens , An Verberckmoes
IPC分类号： C01B37/08 , B01J27/182 , C01B25/26
CPC分类号： B01J29/005 , B01J29/85 , C01B37/08 , C01B39/54 , C07C1/20 , C10G2400/20 , Y02P30/20 , C07C11/02
摘要： A process for manufacturing a silicoaluminophosphate molecular sieve comprising at least one intergrown phase of AEI and CHA framework types, the process comprising the steps of (a) combining at least one silicon source, at least one phosphorus source, at least one aluminum source, and at least one structure-directing-agent (R) to form a mixture; and (b) treating the mixture at crystallization conditions sufficient to form the silicoaluminophosphate molecular sieve, wherein the mixture prepared in step (a) has a molar composition of: (n)SiO2/Al2O3/(m)P2O5/(x)R/(y)H2Owherein n ranges from about 0.005 to about 0.6, m ranges from about 0.6 to about 1.2, x ranges from about 0.5 to about 0.99, and y ranges from about 10 to about 40.
摘要翻译：一种制备含有至少一种AEI和CHA骨架类型的共生相的硅铝磷酸盐分子筛的方法，该方法包括以下步骤：（a）将至少一种硅源，至少一种磷源，至少一种铝源和至少一种结构导向剂（R）以形成混合物; （b）在足以形成硅铝磷酸盐分子筛的结晶条件下处理该混合物，其中步骤（a）中制备的混合物的摩尔组成为： “铅”→（n）SiO 2 / Al 2 O 3 /（m）P 2 O （x）R /（y）H 2 O <βin-line-formula description =“In-line Formulas”end =“tail”？>其中 n为约0.005至约0.6，m为约0.6至约1.2，x为约0.5至约0.99，y为约10至约40。

16. 发明申请

US20060079397A1 Catalyst and process for the conversion of oxygenates to olefins 审中-公开
标题翻译：用于将含氧化合物转化为烯烃的催化剂和方法
公开(公告)号：US20060079397A1
公开(公告)日：2006-04-13
申请号：US10964172
申请日：2004-10-12
申请人： Machteld Mertens , Marcel Janssen , Luc Martens , Kenneth Clem
发明人： Machteld Mertens , Marcel Janssen , Luc Martens , Kenneth Clem
IPC分类号： B01J27/182
CPC分类号： B01J29/005 , B01J29/80 , B01J29/85 , C07C1/20 , Y02P30/42 , C07C11/02
摘要： A catalyst composition for use in the conversion of oxygenates to olefins comprises a first molecular sieve comprising a CHA framework type material and a second molecular sieve comprising an AFI framework type material, wherein said second molecular sieve is present in an amount up to 0.75% by weight of said first molecular sieve.
摘要翻译：用于将含氧化合物转化为烯烃的催化剂组合物包括包含CHA骨架型材料的第一分子筛和包含AFI骨架型材料的第二分子筛，其中所述第二分子筛以至多0.75％的量存在，所述第一分子筛的重量。

17. 发明申请

US20050256354A1 Molecular sieve catalyst composition, its making and use in conversion processes 有权
标题翻译：分子筛催化剂组成，其制备和用途在转化过程中
公开(公告)号：US20050256354A1
公开(公告)日：2005-11-17
申请号：US10844168
申请日：2004-05-12
申请人： Luc Martens , Marcel Janssen , Machteld Mertens , An Verberckmoes , Guang Cao
发明人： Luc Martens , Marcel Janssen , Machteld Mertens , An Verberckmoes , Guang Cao
IPC分类号： B01J29/85 , B01J37/00 , C07C1/20 , C10G3/00 , C07C1/00
CPC分类号： C07C1/20 , B01J29/85 , C10G3/49 , C10G3/56 , C10G3/62 , C10G2300/1022 , C10G2400/20 , Y02P30/20 , Y02P30/42 , Y10S423/30 , Y10S502/514 , C07C11/02
摘要： The invention relates to a molecular sieve catalyst composition, to a method of making or forming the molecular sieve catalyst composition, and to a conversion process using the catalyst composition. In particular, the invention is directed to a conversion process for producing olefin(s), preferably ethylene and/or propylene, from a feedstock, preferably an oxygenate containing feedstock in the presence of a molecular sieve having been synthesized in the presence of a flocculant.
摘要翻译：本发明涉及分子筛催化剂组合物，制备或形成分子筛催化剂组合物的方法，以及使用该催化剂组合物的转化方法。特别地，本发明涉及在存在已在絮凝剂存在下合成的分子筛的存在下从原料，优选含氧化合物原料生产烯烃，优选乙烯和/或丙烯的转化方法。

18. 发明授权

US06350428B1 Preparation of zeolite-bound FAU structure type zeolite and use thereof 失效
标题翻译：沸石键合的FAU结构型沸石的制备及其用途
公开(公告)号：US06350428B1
公开(公告)日：2002-02-26
申请号：US09087445
申请日：1998-05-29
申请人： Johannes Petrus Verduijn , by Jannetje Maatje van den Berge , Machteld Mertens
发明人： Johannes Petrus Verduijn , by Jannetje Maatje van den Berge , Machteld Mertens
IPC分类号： C01B3920
CPC分类号： C01B39/205 , B01J20/18 , B01J20/183 , B01J29/08 , B01J29/084 , B01J29/70 , B01J29/80 , B01J2229/26 , B01J2229/42 , C01B39/026 , C01B39/20 , C10G11/05 , C10G35/095 , C10G45/16 , C10G45/64 , C10G47/16 , Y10S423/21
摘要： This invention relates to a process for producing zeolite-bound FAU structure type zeolite having excellent mechanical strength and containing reduced amounts of zeolite P and the use of the zeolite-bound FAU structure type zeolites produced by the process. The zeolite-bound FAU structure type zeolite is prepared by converting the silica of a silica-bound FAU structure type aggregate in an aqueous mixture containing an effective amount of crown ether, e.g., 15-crown-5 and 18-crown-6, to suppress the formation of zeolite P and sufficient hydroxy ions to cause the silica to be converted to the zeolite. The zeolite-bound FAU structure type zeolite finds particular application in adsorption processes and hydrocarbon conversion processes such as catalytic cracking, hydrocracking, and reforming.
摘要翻译：本发明涉及具有优异的机械强度并且含有减少量的沸石P的沸石结合的FAU结构型沸石的制备方法以及通过该方法生产的沸石结合的FAU结构型沸石的用途。沸石键合的FAU结构型沸石通过将二氧化硅结合的FAU结构型骨料的二氧化硅在含有有效量的冠醚例如15-冠-5和18-冠-6的含水混合物中转化成抑制沸石P的形成和足够的羟基离子使二氧化硅转化为沸石。沸石结合的FAU结构型沸石特别适用于吸附过程和烃转化过程如催化裂化，加氢裂化和重整。

19. 发明申请

US20140161717A1 SYNTHESIS OF ZSM-58 CRYSTALS WITH IMPROVED MORPHOLOGY 有权
标题翻译：具有改进形态的ZSM-58晶体的合成
公开(公告)号：US20140161717A1
公开(公告)日：2014-06-12
申请号：US14074881
申请日：2013-11-08
申请人： Ivy D. Johnson , Nadya A. Hrycenko , Barbara Carstensen , Machteld Mertens , Brita Engels
发明人： Ivy D. Johnson , Nadya A. Hrycenko , Barbara Carstensen , Machteld Mertens , Brita Engels
IPC分类号： C01B39/48
CPC分类号： C01B39/04 , B01D53/02 , B01D53/04 , B01D53/0423 , B01D53/0462 , B01D53/047 , B01D53/0473 , B01D69/147 , B01D2253/108 , B01D2256/245 , B01D2257/102 , B01D2257/504 , B01J20/3078 , B01J35/023 , B01J35/026 , C01B37/02 , C01B39/48 , Y02C10/08 , Y02P20/152
摘要： Methods are provided for synthesizing ZSM-58 crystals with an improved morphology and/or an improved size distribution. By controlling the conditions during synthesis of the ZSM-58 crystals, crystals of a useful size with a narrow size distribution can be generated. Additionally, by controlling the ratio of water content to silica content in the synthesis mixture, it has unexpectedly been found that ZSM-58 crystals can be formed with an improved morphology. The improved morphology can result in ZSM-58 crystals with a more uniform size across the various dimensions of the crystal, which allows for more uniform diffusion within the crystal. This is in contrast to conventionally synthesized crystals, where the size of the crystal can vary along different axes of the crystals.
摘要翻译：提供了用于合成具有改进的形态和/或改进的尺寸分布的ZSM-58晶体的方法。通过控制合成ZSM-58晶体的条件，可以产生具有窄尺寸分布的有用尺寸的晶体。另外，通过控制合成混合物中水含量与二氧化硅含量的比例，意外地发现可以形成具有改进的形态的ZSM-58晶体。改进的形态可以导致在晶体的各种尺寸上具有更均匀尺寸的ZSM-58晶体，这允许在晶体内更均匀的扩散。这与传统合成的晶体形成对比，其中晶体的尺寸可以沿晶体的不同轴线变化。

20. 发明申请

US20070100188A1 Metalloaluminophosphate molecular sieves, their synthesis and use 有权
标题翻译：金属铝磷酸盐分子筛，它们的合成和使用
公开(公告)号：US20070100188A1
公开(公告)日：2007-05-03
申请号：US11588669
申请日：2006-10-27
申请人： Machteld Mertens , Karl Strohmaier
发明人： Machteld Mertens , Karl Strohmaier
IPC分类号： C07C1/00 , B01J27/00 , B01J27/182 , C01B39/00
CPC分类号： B01J23/02 , B01J21/10 , B01J29/84 , B01J29/90 , B01J38/02 , B01J38/12 , C01B39/54 , C07C1/20 , C07C2529/84 , C07C2529/85 , Y02P20/584 , Y02P30/42 , Y10S423/30 , C07C11/02
摘要： A process for manufacturing a metalloaluminophosphate molecular sieve, the process comprising the steps of: (a) combining at least one silicon source, at least one metal source, at least one structure-directing-agent (R), at least one phosphorus source, and at least one aluminum source to form a mixture having a molar composition according to formula: (n)Si:Al2:(m)P:(x)R:(y)H2O:(z)M wherein n is in the range of from about 0.005 to about 0.6, m is in the range of from about 1.2 to about 2.4, x is in the range of from about 0.5 to about 2, y is in the range of from about 10 to about 60, and z is in the range of from about 0.001 to 1; and (b) submitting the mixture to crystallization conditions to form the metalloaluminophosphate molecular sieve, wherein the metalloaluminophosphate molecular sieve has an X-ray diffraction pattern having a FWHM greater than 0.10 degree (2θ) and an AEI/CHA framework type ratio of from about 0/100 to about 40/60 as determined by DIFFaX analysis.
摘要翻译：一种制造金属铝磷酸盐分子筛的方法，该方法包括以下步骤：（a）将至少一种硅源，至少一种金属源，至少一种结构导向剂（R），至少一种磷源，和至少一个铝源以形成具有下式的摩尔组成的混合物：<？in-line-formula description =“In-line Formulas”end =“lead”→（n）Si：Al 2 （m）P：（x）R：（y）H 2 O：（z）M <？in-line-formula description =“In-line Formulas”end = “尾”→其中n在约0.005至约0.6的范围内，m在约1.2至约2.4的范围内，x在约0.5至约2的范围内，y在范围内为约10至约60，z在约0.001至1的范围内; 和（b）将混合物提供到结晶条件以形成金属铝磷酸盐分子筛，其中金属铝磷酸盐分子筛具有FWHM大于0.10度（2θ）的X射线衍射图，和来自约 0/100至约40/60，由DIFFaX分析确定。

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