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    • 15. 发明申请
    • Process for Producing Ti and Apparatus Therefor
    • 生产钛的方法及其设备
    • US20100089204A1
    • 2010-04-15
    • US11992162
    • 2006-08-22
    • Tadashi OgasawaraMakoto YamaguchiToru UenishiMasahiko HoriKazuo TakemuraKatsunori Dakeshita
    • Tadashi OgasawaraMakoto YamaguchiToru UenishiMasahiko HoriKazuo TakemuraKatsunori Dakeshita
    • C22B34/12
    • C25C3/28C22B34/1272C22B34/129C22B34/1295C25C3/02C25C7/005C25C7/06
    • A process for producing Ti, comprising a reduction step of reacting TiCl4 with Ca in a CaCl2-containing molten salt having the Ca dissolved therein to thereby form Ti particles, a separation step of separating the Ti particles formed in said molten salt from said molten salt and an electrolysis step of electrolyzing the molten salt so as to increase the Ca concentration, wherein the molten salt increased in Ca concentration in the electrolysis step is introduced into a regulating cell to thereby render the Ca concentration of the molten salt constant and thereafter the molten salt is used for the reduction of TiCl4 in the reduction step. In the present invention, the Ca concentration of the molten salt to be fed to the corresponding reduction vessel can be inhibited from fluctuating and, at the same time, can maintain high concentration levels. Further, a large volume of the molten salt can be treated continuously. Therefore, the reduction reaction of TiCl4 can be efficiently performed, and the process can be effectively utilized in the production of Ti by Ca reduction as a production process for realizing Ti production on an industrial scale.
    • 一种制备Ti的方法,包括在溶解有Ca的含CaCl 2的熔融盐中使TiCl4与Ca反应从而形成Ti颗粒的还原步骤,将在所述熔融盐中形成的Ti颗粒与所述熔融盐分离的分离步骤 以及电解电解步骤,电解所述熔融盐以增加所述Ca浓度,其中将所述电解步骤中的Ca浓度升高的所述熔融盐引入调节池中,从而使所述熔融盐的Ca浓度恒定, 盐在还原步骤中用于还原TiCl4。 在本发明中,可以抑制供给到相应的还原容器的熔融盐的Ca浓度的波动,同时可以保持高浓度水平。 此外,可以连续地处理大量的熔融盐。 因此,可以有效地进行TiCl 4的还原反应,并且通过Ca还原可以有效地利用Ti的制造,作为实现工业规模的Ti生产的制造方法。
    • 17. 发明申请
    • Method for Removing/Concentrating Metal-Fog-Forming Metal Present in Molten Salt, Apparatus Thereof, and Process and Apparatus for Producing Ti or Ti Alloy by use of them
    • 熔融盐中存在的金属成雾金属的除去/浓缩方法及其制备方法以及使用它们生产Ti或Ti合金的方法和装置
    • US20090114546A1
    • 2009-05-07
    • US12224843
    • 2007-03-09
    • Tadashi OgasawaraMakoto Yamaguchi
    • Tadashi OgasawaraMakoto Yamaguchi
    • C25C3/36C25C3/28C25C7/00
    • C22B34/129C22B26/20C22B34/1272C25C3/02C25C3/28
    • The present invention provides a method by which a metal-fog-forming metal dissolved in one portion of “a molten salt mixture consisted of one or more of metal-fog-forming metal containing molten salts” (generally, a molten salt) can be removed and transferred to another portion of the molten salt to increase the concentration thereof. The method can hence be utilized as one of means for treating molten salts in various industrial fields in which metal-fog-forming metal-containing molten salts such as Ca or Na are handled. In particular, when the method is utilized in producing Ti by Ca reduction, the Ca dissolved in the molten salt to be fed to an electrolytic cell can be rapidly removed (recovered) and the Ca formation efficiency during the electrolysis of the molten salt can be enhanced. Consequently, Ca formation and TiCl4 reduction in the electrolysis of the molten salt can be efficiently carried out and a stable operation on a commercial scale is possible. Thus, the method can be efficiently utilized in producing Ti or a Ti alloy by Ca reduction.
    • 本发明提供了一种溶解在由熔融盐形成金属成形金属中的一种或多种熔融盐混合物组成的熔融盐混合物(通常为熔融盐)的一部分中的金属雾形成金属可以是 除去并转移到另一部分熔融盐中以增加其浓度。 因此,该方法可以用作处理含金属成雾金属的熔融盐如Ca或Na的各种工业领域中的熔融盐的一种手段。 特别是当通过Ca还原来制造Ti时,可以迅速除去(回收)溶解在供给电解槽的熔融盐中的Ca,并且熔融盐电解时的Ca生成效率可以为 增强。 因此,可以有效地进行熔融盐的电解中的Ca生成和TiCl 4的还原,从而能够实现商业规模的稳定化。 因此,该方法可以有效地用于通过Ca还原生产Ti或Ti合金。
    • 20. 发明授权
    • High voltage capacitor and magnetron
    • 高压电容器和磁控管
    • US5544002A
    • 1996-08-06
    • US196229
    • 1994-02-24
    • Shouichi IwayaMasahiro YahagiHitoshi KudouShigeru ItouIsao FujiwaraTadashi OgasawaraMakoto MoritaTeruo TaguchiSetuo Sasaki
    • Shouichi IwayaMasahiro YahagiHitoshi KudouShigeru ItouIsao FujiwaraTadashi OgasawaraMakoto MoritaTeruo TaguchiSetuo Sasaki
    • H01G4/224H01G4/35H01G4/38
    • H01G4/35
    • A high voltage capacitor is disclosed that comprises a grounding member (1), two through type capacitors (2 and 3), an insulating case (6) and insulating resin (71 and 72). The grounding member (1) has two raised portions (101 and 102) on which the through type capacitors (2 and 3) are secured. The insulating case (6) has two hollow cylindrical portions (61, 62) spaced apart by a distance D with their upper open ends joined to each other to form a recessed enclosure (63) in line with and following the inner diameter sections (611, 621) of the hollow cylindrical portions (61, 82) and their lower open ends fitted on the outer circumference of the raised portions (101, 102). The insulating resin (71 and 72) is provided around the through type capacitors (2 and 3) within the inner diameter sections (611, 621). It is thus possible to provide a high voltage capacitor with superior mechanical strength and excellent withstand voltage characteristics even in humid environments and that is small in size and inexpensive.
    • PCT No.PCT / JP92 / 01077 Sec。 371日期1994年2月24日 102(e)日期1994年2月24日PCT提交1992年8月26日PCT公布。 出版物WO93 / 04494 日期1993年3月4日公开了一种高压电容器,其包括接地构件(1),两通电容器(2和3),绝缘壳体(6)和绝缘树脂(71和72)。 接地构件(1)具有固定有贯通型电容器(2和3)的两个凸起部分(101和102)。 绝缘壳体(6)具有间隔开距离D的两个中空圆柱形部分(61,62),它们的上开口端彼此连接,以形成与内径部分(611)一致并跟随内凹部分 ,621)和其下开口端嵌合在凸起部分(101,102)的外圆周上。 绝缘树脂(71和72)设置在内径部分(611,621)内的直通型电容器(2和3)周围。 因此,即使在潮湿的环境中也能够提供具有优异的机械强度和优异的耐压特性的高压电容器,并且尺寸小且便宜。