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11. 发明授权

US4681615A Silica glass formation process 失效
标题翻译：二氧化硅玻璃形成工艺
公开(公告)号：US4681615A
公开(公告)日：1987-07-21
申请号：US642606
申请日：1984-08-20
申请人： Motoyuki Toki , Sadao Kanbe , Satoru Miyashita , Tetsuhiko Takeuchi
发明人： Motoyuki Toki , Sadao Kanbe , Satoru Miyashita , Tetsuhiko Takeuchi
IPC分类号： C03B8/02 , C03B19/12 , C03C1/00 , C03C3/06 , C03B19/06
CPC分类号： C03C1/006 , C03B19/12 , C03C3/06 , C03C2201/02 , C03C2203/26 , C03C2203/34 , Y02P40/57 , Y10S65/901
摘要： A process for forming monolithic silica glass articles is provided. The process includes the steps of hydrolyzing silicon alkoxide to form a hydrolyzed solution, adding fumed silica to the hydrolyzed silicon alkoxide solution to yield a sol solution, gelling the sol solution to a gel, and drying and sintering the gel to obtain the monolithic silica glass articles.
摘要翻译： PCT No.PCT / JP83 / 00450 Sec。 1984日期1984年8月20日 102（e）日期1984年8月20日PCT提交1983年12月22日PCT公布。第WO84 / 02519号公报日期1984年7月5日。一种用于形成整体式二氧化硅玻璃制品的方法。该方法包括水解硅烷醇以形成水解溶液的步骤，向水解的硅醇盐溶液中加入热解二氧化硅以产生溶胶溶液，将溶胶溶胶凝胶化，并干燥并烧结凝胶以获得单片石英玻璃文章。

12. 发明授权

US07909929B2 Dispersoid having metal-oxygen bonds, metal oxide film, and monomolecular film 有权
标题翻译：具有金属氧键的分散体，金属氧化物膜和单分子膜
公开(公告)号：US07909929B2
公开(公告)日：2011-03-22
申请号：US10533580
申请日：2003-11-12
申请人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
发明人： Nobuo Kimura , Yoshitaka Fujita , Norifumi Nakamoto , Motoyuki Toki , Akiji Higuchi , Kazuo Ono , Tomoya Hidaka , Hiroyuki Takeda
IPC分类号： C01G23/047
CPC分类号： C01B13/32 , C01G23/053 , C23C18/1216 , C23C18/122 , Y10T428/24355
摘要： The invention provides dispersoids having metal-oxygen groups which are suitable for the production of metal oxide thin-films at a low temperature of 200° C. or below and for the production of homogeneous organic-inorganic hybrid materials. The invention also provides metal oxide thin-films and organic-inorganic hybrid materials endowed with various capabilities, particularly organic-inorganic hybrid materials having a high refractive index and high transparency. Use is made of a dispersoid having metal-oxygen bonds which is obtained by mixing a metal compound having at least three hydrolyzable groups with at least 0.5 mole but less than 2 moles of water per mole of the metal compound in an organic solvent, in the absence of an acid, a base and/or a dispersion stabilizer, and at a temperature at or below the temperature at which the metal compound begins to hydrolyze, then raising the temperature to at least the temperature at which hydrolysis begins.
摘要翻译：本发明提供了适用于在200℃或更低的低温下生产金属氧化物薄膜的金属 - 氧基分散体和用于生产均相有机 - 无机混合材料的分散体。本发明还提供具有各种能力的金属氧化物薄膜和有机 - 无机混合材料，特别是具有高折射率和高透明度的有机 - 无机混合材料。使用具有金属 - 氧键的分散体，其通过在有机溶剂中将具有至少三个可水解基团的金属化合物与每摩尔金属化合物混合至少0.5摩尔但小于2摩尔水而获得，不存在酸，碱和/或分散体稳定剂，并且在金属化合物开始水解或在低于金属化合物开始水解的温度的温度下，将温度升至至少水解开始的温度。

13. 发明申请

US20070122631A1 Flexible substrate and coating liquid 审中-公开
标题翻译：柔性基材和涂料液体
公开(公告)号：US20070122631A1
公开(公告)日：2007-05-31
申请号：US10579195
申请日：2004-11-09
申请人： Akiji Higuchi , Kenji Yamada , Rumi Shinagawa , Terumi Ikeda , Motoyuki Toki
发明人： Akiji Higuchi , Kenji Yamada , Rumi Shinagawa , Terumi Ikeda , Motoyuki Toki
IPC分类号： B32B17/06 , B32B17/10 , C08L83/04 , C08G77/00
CPC分类号： B32B27/06 , B32B17/06 , B32B17/10018 , C08L83/04 , Y02P20/582 , Y10T428/31612 , Y10T428/31663
摘要： A flexible substrate 10 of the present invention is formed of a stacked body which is constituted of an inorganic glass layer 110 and polymer layers 120A, 120B, wherein the polymer layers 120A, 120B are formed of a polymer layer which contains polyorganosilsesquioxane as a main component thereof. Due to such a constitution, the flexible substrate 10 of the present invention possesses excellent heat resistance in addition to excellent flexibility, excellent impact resistance and excellent gas barrier properties.
摘要翻译：本发明的柔性基板10由无机玻璃层110和聚合物层120A，120B构成的层叠体形成，其中聚合物层120A，120B由聚合物层形成，聚合物层含有聚有机倍半硅氧烷作为其主要成分。由于这样的结构，本发明的柔性基板10除了具有优异的柔软性，优异的耐冲击性和优异的阻气性外，还具有优异的耐热性。

14. 发明授权

US06255762B1 Ferroelectric element and process for producing the same 失效
标题翻译：铁电元件及其制造方法
公开(公告)号：US06255762B1
公开(公告)日：2001-07-03
申请号：US09117377
申请日：1998-07-29
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： C01B1332
CPC分类号： H01L41/318 , C01G25/006 , C01P2002/34 , C01P2002/72 , C01P2002/77 , C01P2004/02 , H01L41/1876 , Y10T29/42 , Y10T29/49002
摘要： A ferroelectric element comprising a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including a sol-gel process in the presence of a thickener and/or an association preventive from aqueous solutions of respective salts of the metals. The ferroelectric element is advantageous in that the handling of starting compounds and the production of the ferroelectric element are easy, the storage stability of the starting compound solution is good, the cost is low, the ferroelectric element can be formed as a thin layer, particles on the surface of the thin layer are fine and dense, and, hence, the surface smoothness is good. The ferroelectric element is excellent also in piezoelectric properties and therefore can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.
摘要翻译：一种铁电体元件，其包含含有至少两种金属的铁电材料，所述铁电体元件是通过包括溶胶 - 凝胶法在增稠剂存在下和/或与金属的各种盐的水溶液缔合的方法制备的。铁电元件的优点在于，起始化合物的处理和铁电体元素的制备容易，起始化合物溶液的储存稳定性好，成本低，铁电元件可以形成为薄层，颗粒薄层表面细致密集，表面光洁度好。铁电体元件在压电性能方面也是优异的，因此可以有利地用作压电喷墨头中的压电元件。

15. 发明授权

US06235260B1 Method for producing In2O3—SnO2 precursor sol 失效
标题翻译：生产In2O3-SnO2前体溶胶的方法
公开(公告)号：US06235260B1
公开(公告)日：2001-05-22
申请号：US09230252
申请日：1999-03-22
申请人： Motoyuki Toki , Toshimi Fukui , Naoko Asakuma , Takamitsu Fujii
发明人： Motoyuki Toki , Toshimi Fukui , Naoko Asakuma , Takamitsu Fujii
IPC分类号： B01F308
CPC分类号： C01G19/00 , C03C17/253 , C03C2217/231 , C03C2218/113 , C04B41/505 , C04B2111/805 , C04B2111/94 , C04B41/0036 , C04B41/0045 , C04B41/4537 , C04B41/4554 , C04B41/5072
摘要： The invention relates to a method for forming a transparent conductive thin film of In2O3—SnO2 on a surface of a plastics substrate of less heat resistance other than that of glass, ceramics, etc. When an In2O3—SnO2 precursor sol is produced by hydrolyzing and polymerizing a solution containing indium alkoxide and tin alkoxide, either tri-s-butoxyindium or tri-t-butoxyindium is used as the indium alkoxide. Water is added to the solution containing indium alkoxide and tin alkoxide at a temperature of not higher than −20° C. The obtained In2O3—SnO2 precursor sol is applied to a surface of a substrate to form a gel film, then the gel film is either irradiated with an ultraviolet beam of which wave length is not longer than 360 nm, or irradiated with an ultraviolet beam of which wave length is not longer than 260 nm and further irradiated with a laser beam of which wave length is not longer than 360 nm, to crystallize the gel forming the thin film, whereby an In2O3—SnO2 thin film having a conductivity is formed on the surface of the substrate.
摘要翻译：本发明涉及在除了玻璃，陶瓷等以外的耐热性低的塑料基板的表面上形成In2O3-SnO2的透明导电性薄膜的方法。当In2O3-SnO2前体溶胶通过水解和使用含有烷氧化铟和锡醇盐的溶液，即三正丁氧基铟或三叔丁氧基铟作为铟醇盐。在不高于-20℃的温度下，向含有烷氧基烷氧化物和锡醇盐的溶液中加入水。将得到的In2O3-SnO2前体溶胶施加到基材的表面，形成凝胶膜，然后将凝胶膜用波长不大于360nm的紫外线照射或用波长不大于260nm的紫外线照射，并进一步用波长不大于360nm的激光束照射使形成薄膜的凝胶结晶，由此在基板的表面上形成具有导电性的In2O3-SnO2薄膜。

16. 发明授权

US4801318A Silica glass formation process 失效
标题翻译：二氧化硅玻璃形成工艺
公开(公告)号：US4801318A
公开(公告)日：1989-01-31
申请号：US8226
申请日：1987-01-29
申请人： Motoyuki Toki , Sadao Kanbe , Satoru Miyashita , Tetsuhiko Takeuchi
发明人： Motoyuki Toki , Sadao Kanbe , Satoru Miyashita , Tetsuhiko Takeuchi
IPC分类号： C03B8/02 , C03B19/12 , C03C1/00 , C03C3/06 , C03B19/06
CPC分类号： C03C1/006 , C03B19/12 , C03C3/06 , C03C2201/02 , C03C2203/26 , C03C2203/34 , Y02P40/57 , Y10S65/901
摘要： In a forming a silica glass at low temperature, a fumed silica is added to a hydrolyzed solution of a metal alcoxide. 0.2-5 mol of fumed silica is added to 1 mol of metal alcoxide. Being uniformly dispersed, the solution is gelled and dried to be dry gel and then sintered to be non-porous. This process allows a practically large sized silica glass to be materialized which has been impossible by the previous sol-gel technology. In addition, a further large silica glass can be prepared by adjusting pH value to 3-6 with addition of base in the sol solution.

17. 发明申请

US20120015175A1 COATING MATERIALS FOR BISPHENOL A-CONTAINING POLYMERS 审中-公开
标题翻译：含有BISPHENOL A的聚合物涂料
公开(公告)号：US20120015175A1
公开(公告)日：2012-01-19
申请号：US13123597
申请日：2010-06-29
申请人： Toshimi Fukui , Motoyuki Toki
发明人： Toshimi Fukui , Motoyuki Toki
IPC分类号： B32B5/16 , B32B27/00 , B32B27/38 , B32B9/04
CPC分类号： C09D7/67 , C09D5/028 , C09D7/62 , C09D171/02 , Y10T428/25 , Y10T428/31504 , Y10T428/31507 , Y10T428/31511 , Y10T428/3154 , Y10T428/31855
摘要： The present technology provides compositions that may be coated on bisphenol A-containing polymers to provide a coating or film that prevents bisphenol A from leaching from the polymer. Coatings using the present compositions also protect the bisphenol A-containing polymer from degradation by UV rays and other sources. The compositions include one or more matrix polymers having a solubility parameter of about 20 or less; and a plurality of UV-blocking nanoparticles dispersed in the one or more matrix polymers; wherein the composition is substantially free of bisphenol A. Methods of making the compositions and coatings are also provided. The coatings may be used on food and beverage containers made from bisphenol A-containing polymers.
摘要翻译：本技术提供可以涂覆在含双酚A的聚合物上以提供防止双酚A从聚合物中浸出的涂层或膜的组合物。使用本发明组合物的涂料还可以保护含双酚A的聚合物免受紫外线和其它来源的降解。所述组合物包括溶解度参数为约20或更小的一种或多种基质聚合物; 和分散在所述一种或多种基质聚合物中的多个UV-阻聚纳米颗粒; 其中组合物基本上不含双酚A.还提供了制备组合物和涂层的方法。涂料可用于由含双酚A的聚合物制成的食品和饮料容器。

18. 发明申请

US20120003709A1 METHOD AND SYSTEM FOR CELL AND TISSUE CULTIVATION 有权
标题翻译：细胞和组织培养的方法和系统
公开(公告)号：US20120003709A1
公开(公告)日：2012-01-05
申请号：US13131152
申请日：2010-07-01
申请人： Toshimi Fukui , Motoyuki Toki
发明人： Toshimi Fukui , Motoyuki Toki
IPC分类号： C12N13/00 , C12M1/36
CPC分类号： C12N13/00 , C12M23/04 , C12M23/20 , C12M33/00 , C12N11/00
摘要： A cell cultivating platform includes a substrate having a surface, at least one actuator moveable relative to the substrate, and a deformable material layer positioned above at least a portion of the supporting surface and the at least one actuator. The deformable material layer positioned opposite the substrate surface includes a biocompatible supportive surface suitable for supporting cultivated cells. The supportive surface deforms or otherwise deflects in response to activation of the at least one actuator, effectively releasing at least a portion of the cultured cells from the supportive surface. Suitable actuators include piezoelectric actuators that can be selectively energized according to one or more patterns to facilitate separation of cells from the supportive surface. Such activation cycles can be repeated.
摘要翻译：细胞培养平台包括具有表面的基底，可相对于基底移动的至少一个致动器和位于支撑表面和至少一个致动器的至少一部分上方的可变形材料层。与基底表面相对定位的可变形材料层包括适于支撑培养细胞的生物相容支撑表面。支撑表面响应于至少一个致动器的激活而变形或以其它方式偏转，有效地将至少一部分培养细胞从支撑表面释放出来。合适的致动器包括压电致动器，其可以根据一个或多个图案选择性地通电以便于将细胞与支撑表面分离。可以重复这样的激活循环。

19. 发明授权

US07012036B2 ZrO2-Al2O3 composite ceramic material and production method thereof 失效
标题翻译： ZrO2-Al2O3复合陶瓷材料及其制备方法
公开(公告)号：US07012036B2
公开(公告)日：2006-03-14
申请号：US10621385
申请日：2003-07-18
申请人： Masahiro Nawa , Kouichi Yamaguchi , Motoyuki Toki
发明人： Masahiro Nawa , Kouichi Yamaguchi , Motoyuki Toki
IPC分类号： C04B35/488
CPC分类号： C04B35/4885
摘要： A ZrO2—Al2O3 composite ceramic material having high mechanical strength and toughness as well as excellent wear resistance and hardness is provided. This ceramic material includes a first phase of ZrO2 grains containing 10 to 12 mol % of CeO2 as a stabilizer and having an average grain size of 0.1 μm to 1 μm, and a second phase of Al2O3 grains having an average grain size of 0.1 to 0.5 μm. The ceramic material has a mutual nano-composite structure formed under a condition that a content of the second phase in the ceramic material is within a range of 20 to 60 vol % such that the Al2O3 grains are dispersed within said ZrO2 grains at a first dispersion ratio of 2% or more, and preferably 4% or more, which is defined as a ratio of the number of the Al2O3 grains dispersed within the ZrO2 grains relative to the number of the entire Al2O3 grains dispersed in the ceramic material, and the ZrO2 grains are dispersed within the Al2O3 grains at a second dispersion ratio of 1% or more, which is defined as a ratio of the number of the ZrO2 grains dispersed within the Al2O3 grains relative to the number of the entire ZrO2 grains dispersed in the ceramic material.
摘要翻译：提供具有高机械强度和韧性以及优异的耐磨性和硬度的ZrO 2 -Al 2 O 3 O 3复合陶瓷材料。该陶瓷材料包括含有10〜12摩尔％的CeO 2 N 2作为稳定剂并且平均粒径为0.1〜1μm的ZrO 2 N 2晶粒的第一相，和平均粒度为0.1〜0.5μm的Al 2 O 3 3晶粒的第二相。陶瓷材料具有在陶瓷材料中的第二相的含量在20〜60体积％的范围内形成的相互纳米复合结构，使得Al 2 O _{3％的颗粒以2％以上，优选为4％以上的第一分散比分散在所述ZrO 2 N 2晶粒内，其定义为相对于整个Al 2 O 2的数量分散在ZrO 2 2晶粒内的Al 2 N 3 O 3晶粒，分散在陶瓷材料中的3个/ 3个晶粒，并且ZrO 2/2晶粒分散在Al 2 O 3 3晶粒内 1％或更多的第二分散比，其定义为分散在Al 2 N 3 O 3中的ZrO 2 N 2晶粒的数量的比率，相对于分散在陶瓷材料中的整个ZrO 2 N 2颗粒的数量。}

20. 发明授权

US06343855B1 Ferroelectric element process for producing the same and ink jet head 失效
标题翻译：用于制造相同的铁电元件工艺和喷墨头
公开(公告)号：US06343855B1
公开(公告)日：2002-02-05
申请号：US09011959
申请日：1998-02-23
申请人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
发明人： Shinichi Sakamaki , Yukimi Takahashi , Yorinobu Yamada , Motoyuki Toki , Mamoru Aizawa
IPC分类号： B41J2045
CPC分类号： B41J2/14233 , B41J2202/03 , C23C18/1216 , C23C18/1254 , H01L41/1876 , H01L41/318
摘要： A ferroelectric element, having a ferroelectric material containing at least two metals, the ferroelectric element having been produced by a process including the steps of: providing alkoxides of the respective metals as starting compounds; hydrolyzing the metal alkoxides in the presence of a catalytic amount of a protonic acid to increase the molecular weight; and adding a film-forming polymer material to the sol-like solution prepared in the step of increasing the molecular weight to prepare a sol-like ferroelectric precursor solution. The ferroelectric element can be formed in a thick film form without creating any cracks. It can be advantageously used as a piezoelectric element in a piezoelectric ink jet head.
摘要翻译：具有含有至少两种金属的铁电材料的铁电体元件，所述铁电体元件通过包括以下步骤的方法生产：提供各种金属的醇盐作为起始化合物; 在催化量的质子酸存在下水解金属醇盐以提高分子量; 并将成膜聚合物材料添加到在提高分子量的步骤中制备的溶胶状溶液中以制备溶胶状铁电体前体溶液。铁电元件可以形成为厚膜形式而不产生任何裂纹。它可以有利地用作压电喷墨头中的压电元件。

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